IP Library Granted Patent US 11,141,714
Granted Patent B2
US 11,141,714 · App. 14/946,453 · Granted Oct 12, 2021

Selective alkane activation with single-site atoms on amorphous support

Inventors: Adam S. Hock (Chicago, IL); Neil M. Schweitzer (Evanston, IL); Jeffrey T. Miller (Naperville, IL); Bo Hu (Chicago, IL)
Assignee: UChicago Argonne, LLC
B01J23/755B01J21/08B01J23/06B01J23/08B01J23/72B01J23/745B01J23/75B01J35/002B01J35/023B01J35/1019B01J35/1047B01J37/0201B01J37/0203B01J37/0209B01J37/0238B01J37/035B01J37/06B01J37/18C07C5/322C07C5/3332C10G49/02C07C2521/08C07C2523/06C07C2523/08C07C2523/72C07C2523/745C07C2523/75C07C2523/755C10G2300/1081C10G2400/20Y02P20/52
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Quick Facts
Patent No.
US 11,141,714
App. No.
14/946,453
Granted
Oct 12, 2021
Kind
B2
Abstract

The present invention relates generally to catalysts and methods for use in olefin production. More particularly, the present invention relates to novel amorphously supported single-center, Lewis acid metal ions and use of the same as catalysts.

Claims (9)

1. A catalyst for use in olefin production comprising one or more single-atom Lewis acid metal ions selected from the group consisting of Zn tetrahedrally coordinated on the surface of an amorphous silica support in which a tetrahedrally coordinated Zn(II) ion is bonded at a corner vacancy of SiO2 of the amorphous silica support wherein said catalyst selectively cleaves C—H bonds over C—C bonds in the conversion of alkanes to alkenes.

2. The catalyst of claim 1 , wherein the catalyst is a heterogeneous, single-site Zn(II) catalyst, in which the tetrahedrally coordinated Zn(II) ion is bonded to the silica support at 3-membered ring siloxane sites.

3. The catalyst of claim 1 , wherein the catalyst is not redox-active.

4. The catalyst of claim 1 , wherein the catalyst has a selectivity of greater than 75% for C—H activation.

5. The catalyst of claim 1 , wherein the catalyst has a selectivity of greater than 90% for C—H activation.

6. The catalyst of claim 1 , wherein the catalyst has a selectivity of greater than 95% for C—H activation.

7. The catalyst of claim 1 , wherein the catalyst retains catalytic activity for longer than 1 hour.

8. The catalyst of claim 1 , wherein the catalyst retains catalytic activity for longer than 12 hours.

9. The catalyst of claim 1 , wherein the catalyst retains catalytic activity for longer than 24 hours.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 28, 2019
From: SCHWEITZER, NEIL M.; MILLER, JEFFREY T.
To: UCHICAGO ARGONNE, LLC
Reel/Frame 048724/0895 →
CONFIRMATORY LICENSE Recorded Jan 15, 2016
From: UCHICAGO ARGONNE, LLC
To: ENERGY, UNITED STATES DEPARTMENT OF
Reel/Frame 037565/0134 →
Continuity (2)
Division 13830320 · Mar 14, 2013
Related Publication 20160074838A1 · Mar 17, 2016