IP Library Granted Patent US 11,191,290
Granted Patent B2
US 11,191,290 · App. 15/106,403 · Granted Dec 7, 2021

Process for supplying magnesium and/or calcium enriched water based beverage and associated manufacturing apparatus

Inventors: Eric Marchal (Vittel, FR); Renaud Sublet (Vittel, FR)
Assignee: Societe des Produits Nestle S.A.
A23L2/54A23L2/38A23L2/52A23L33/16B01F3/04439B01F3/04808A23V2002/00B01F2003/049B01F2003/04943
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Quick Facts
Patent No.
US 11,191,290
App. No.
15/106,403
Granted
Dec 7, 2021
Kind
B2
Abstract

The invention relates to a process for producing magnesium and/or calcium-enriched drinking water based beverage, comprising: —preparing a concentrated aqueous solution of magnesium and/or calcium bicarbonate by, a) providing a powder of magnesium and/or calcium compound in a reactor (4); b) adding an aqueous liquid in said reactor; and c) injecting carbon dioxide (CO 2 ) into said reactor; —adding at least part of the concentrated aqueous solution of magnesium and/or calcium bicarbonate into a flowing circuit comprising an aqueous liquid. The invention also relates to the associated manufacturing apparatus comprising a reactor.

Claims (22)

1. A process for producing a calcium-enriched drinking water based beverage, the process comprising:

preparing a concentrated aqueous solution of calcium bicarbonate using an apparatus comprising a closed reactor, a line of an open flow circuit comprising a first outlet line, a first inlet line feeding into the closed reactor, and a second outlet line feeding from the closed reactor through a second inlet line into the line of the open flow circuit, wherein the first outlet line, the first inlet line, and the second outlet line are connected to each other at a three-way junction, the preparing of the concentrated aqueous solution comprises:

providing a powder of a calcium compound in the closed reactor, wherein the calcium compound is selected from the group consisting of calcium oxide, calcium hydroxide, calcium carbonate, and mixtures thereof;

adding an aqueous liquid from the first outlet line through the first inlet line into the closed reactor; and

injecting carbon dioxide into the closed reactor to form the concentrated aqueous solution of calcium bicarbonate, into the open flow circuit comprising the aqueous liquid; and

adding at least part of the concentrated aqueous solution of calcium bicarbonate from the closed reactor through the second outlet line, to the second inlet line, and into the line of the open flow circuit, wherein the first inlet line feeding into the closed reactor is common with the second outlet line feeding from the closed reactor.

2. The process according to claim 1 wherein the powder further comprises a magnesium compound selected from the group consisting of magnesium oxide, magnesium hydroxide, magnesium carbonate, and magnesium hydroxide carbonate.

3. The process according to claim 1 , comprising measuring the electrical conductivity of the concentrated aqueous solution in the closed reactor.

4. The process according to claim 1 , wherein the pressure of carbon dioxide atmosphere in the closed reactor is maintained in the range of 1 atm to 10 atm.

5. The process according to claim 1 , wherein the solubility of the calcium compound is increased by increasing the pressure of the carbon dioxide atmosphere in the closed reactor.

6. The process according to claim 1 , wherein the closed reactor is fed with the calcium compound using a solid dosing pump.

7. The process according to claim 1 , wherein the concentrated aqueous solution of calcium bicarbonate is added into the open flow circuit comprising the aqueous liquid to form the calcium-enriched drinking water based beverage using a liquid dosing pump.

8. The process according to claim 1 wherein the closed reactor is automatically agitated.

9. The process according to claim 2 wherein the concentration of magnesium in the concentrated aqueous solution is between 1 g/l and 25 g/l.

10. The process according to claim 1 wherein the concentration of calcium in the concentrated aqueous solution is between 1 g/l and 75 g/l.

11. The process according to claim 2 wherein the concentration of magnesium in the drinking water based beverage is at least 55 mg/l.

12. The process according to claim 1 wherein the concentration of calcium in the drinking water based beverage is 150 mg/l.

13. The process according to claim 7 , wherein a further component is incorporated into the calcium enriched drinking water based beverage through the second inlet line, and the second inlet line is downstream of the liquid dosing pump which adds the concentrated aqueous solution of calcium bicarbonate in the aqueous liquid.

14. The process according to claim 13 , wherein the further component is selected from the group consisting of salt, mineral, health-promoting material, and taste or flavor rendering material.

15. The process according to claim 1 further comprising mixing the concentrated aqueous solution of calcium bicarbonate with an agitator within the closed reactor, and

mixing the concentrated aqueous solution with water in a static mixer.

16. The process according to claim 1 further comprising keeping the concentrated aqueous solution of calcium bicarbonate under a pressure of a carbon dioxide atmosphere of at least 1 atm to 10 atm in the closed reactor during the process.

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0165 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ENGLISH TRANSLATION TO SHOW THE FULL AND CORRECT NEW NAME IN SECTION 51. PREVIOUSLY RECORDED AT REEL: 049391 FRAME: 0756. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded Jun 13, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049853/0398 →
MERGER Recorded Jun 6, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049391/0756 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 14, 2017
From: MARCHAL, ERIC; SUBLET, RENAUD
To: NESTEC S.A.
Reel/Frame 043336/0438 →
Priority Claims (1)
EP 13197968 · Dec 18, 2013 · regional
Continuity (1)
Related Publication 20170000164A1 · Jan 5, 2017