IP Library Granted Patent US 10,211,411
Granted Patent B2
US 10,211,411 · App. 15/246,754 · Granted Feb 19, 2019

Thermally activated delayed fluorescent material based on 9,10-dihydro-9,9-dimethylacridine analogues for prolonging device longevity

Inventors: Jian Li (Tempe, AZ); Daijun Feng (Tempe, AZ)
Assignee: Arizona Board of Regents on behalf of Arizona State University
H01L51/0072C07D471/06C07D519/00C07F9/5728C07F9/6561C09K11/06H01L51/0067C09K2211/1007C09K2211/1022C09K2211/1029C09K2211/1044C09K2211/1048C09K2211/1059C09K2211/1096H01L51/5016H01L2051/0063Y02E10/549
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Quick Facts
Patent No.
US 10,211,411
App. No.
15/246,754
Granted
Feb 19, 2019
Kind
B2
Abstract

Thermally activated delayed fluorescent compounds and uses thereof are described. The thermally activated delayed fluorescent compounds are an analogs of 9,10-dihydro-9,9-dimethylacridine compounds.

Claims (41)

1. A thermally activated delayed fluorescent compound represented by Formula I:

wherein:

represents n acceptor moieties A,

where A is a nitrogen-containing heteroaryl group, and n=2 or 3, such that Formula I includes two acceptor moieties (A 1 and A 2 ) or three acceptor moieties (A 1 , A 2 , and A 3 ), and wherein each acceptor moiety is substituted with R q and optionally substituted with one or more R;

L 1 represents —C(R) 2 — or —CO—;

R m , R n , R p , and R q each independently represents a mono-, di-, tri, or tetra-substitution, valency permitting; and

each R, R m , R n , R p , and R q independently represents a hydrogen atom, a deuterium atom, a halogen atom, a hydroxyl group, a thiol group, a nitro group, a cyano group, a substituted or unsubstituted alkyl group, a substituted or unsubstituted haloalkyl group, a substituted or unsubstituted aralkyl group, a substituted or unsubstituted alkenyl group, a substituted or unsubstituted alkynyl group, a substituted or unsubstituted aryl group, a substituted or unsubstituted amino group, a substituted or unsubstituted mono- or dialkylamino group, a substituted or unsubstituted mono- or diarylamino group, a substituted or unsubstituted alkoxy group, a substituted or unsubstituted aryloxy group, a substituted or unsubstituted heteroaryl group, an alkoxycarbonyl group, an acyloxy group, an acylamino group, an alkoxycarbonylamino group, an aryloxycarbonylamino group, a sulfonylamino group, a sulfamoyl group, a carbamoyl group, an alkylthio group, a sulfinyl group, a ureido group, a phosphoramide group, a mercapto group, a sulfo group, a carboxyl group, a hydrazino group, a substituted silyl group, a polymeric group, or a combination thereof.

2. The compound of claim 1 , wherein

represents one of the following structures:

3. The compound of claim 2 , wherein each A n present comprises 1, 2, or 3 nitrogen atoms.

4. The compound of claim 1 , wherein

represents:

wherein U, U 1 , and U 2 each independently represents N or C.

5. The compound of claim 4 , wherein

represents:

6. The compound of claim 1 , wherein n=2 and the compound is represented by Formula V:

7. The compound of claim 1 , wherein n=3, and the compound is represented by Formula VIII:

8. A thermally activated delayed fluorescent compound represented by Formula XV:

wherein:

represents an acceptor moiety A 1 ,

where A 1 is a nitrogen-containing heteroaryl group, wherein A 1 is substituted with R q ;

L 1 represents —C(R) 2 — or —CO—;

R m , R n , R p , and R q each independently represents a mono-, di-, tri, or tetra-substitution, valency permitting; and

each R, R m , R n , R p , and R q independently represents a hydrogen atom, a deuterium atom, a halogen atom, a hydroxyl group, a thiol group, a nitro group, a cyano group, a substituted or unsubstituted alkyl group, a substituted or unsubstituted haloalkyl group, a substituted or unsubstituted aralkyl group, a substituted or unsubstituted alkenyl group, a substituted or unsubstituted alkynyl group, a substituted or unsubstituted aryl group, a substituted or unsubstituted amino group, a substituted or unsubstituted mono- or dialkylamino group, a substituted or unsubstituted mono- or diarylamino group, a substituted or unsubstituted alkoxy group, a substituted or unsubstituted aryloxy group, a substituted or unsubstituted heteroaryl group, an alkoxycarbonyl group, an acyloxy group, an acylamino group, an alkoxycarbonylamino group, an aryloxycarbonylamino group, a sulfonylamino group, a sulfamoyl group, a carbamoyl group, an alkylthio group, a sulfinyl group, a ureido group, a phosphoramide group, a mercapto group, a sulfo group, a carboxyl group, a hydrazino group, a substituted silyl group, a polymeric group, or a combination thereof.

9. A thermally activated delayed fluorescent compound represented by Formula XIX:

wherein:

represents an acceptor moiety A 1 ,

where A 1 is a nitrogen-containing heteroaryl group;

L 1 represents —C(R) 2 — or —CO—;

R m , R n , and R p each independently represents a mono-, di-, tri, or tetra-substitution, valency permitting; and

each R, R m , R n , and R p independently represents a hydrogen atom, a deuterium atom, a halogen atom, a hydroxyl group, a thiol group, a nitro group, a cyano group, a substituted or unsubstituted alkyl group, a substituted or unsubstituted haloalkyl group, a substituted or unsubstituted aralkyl group, a substituted or unsubstituted alkenyl group, a substituted or unsubstituted alkynyl group, a substituted or unsubstituted aryl group, a substituted or unsubstituted amino group, a substituted or unsubstituted mono- or dialkylamino group, a substituted or unsubstituted mono- or diarylamino group, a substituted or unsubstituted alkoxy group, a substituted or unsubstituted aryloxy group, a substituted or unsubstituted heteroaryl group, an alkoxycarbonyl group, an acyloxy group, an acylamino group, an alkoxycarbonylamino group, an aryloxycarbonylamino group, a sulfonylamino group, a sulfamoyl group, a carbamoyl group, an alkylthio group, a sulfinyl group, a ureido group, a phosphoramide group, a mercapto group, a sulfo group, a carboxyl group, a hydrazino group, a substituted silyl group, a polymeric group, or a combination thereof.

10. A light emitting device comprising the thermally activated delayed fluorescent compound of claim 1 .

11. The light emitting device of claim 10 , wherein the light emitting device is an organic light emitting diode.

12. The light emitting device of claim 10 , wherein the device comprises a full color display, a photovoltaic device, a luminescent display device, or a phosphorescent display device.

13. The compound of claim 10 , wherein the compound is:

14. A light emitting device comprising the thermally activated delayed fluorescent compound of claim 10 .

15. The light emitting device of claim 14 , wherein the light emitting device is an organic light emitting diode.

16. The light emitting device of claim 14 , wherein the device comprises a full color display, a photovoltaic device, a luminescent display device, or a phosphorescent display device.

17. A light emitting device comprising the thermally activated delayed fluorescent compound of claim 9 .

18. The light emitting device of claim 17 , wherein the light emitting device is an organic light emitting diode.

19. The light emitting device of claim 17 , wherein the device comprises a full color display, a photovoltaic device, a luminescent display device, or a phosphorescent display device.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 16, 2017
From: LI, JIAN; FENG, DAIJUN
To: ARIZONA BOARD OF REGENTS ON BEHALF OF ARIZONA STATE UNIVERSITY
Reel/Frame 042390/0387 →
Continuity (2)
Provisional Application 62209647 · Aug 25, 2015
Related Publication 20170077420A1 · Mar 16, 2017
Cited By (12)
US 12,193,327 US 12,221,573 US 12,232,411 US 12,302,745 US 12,312,366 US 12,448,405 US 12,492,336 US 12,503,644 US 12,534,462 US 12,545,678 US 12,565,486 US 12,643,919