IP Library Granted Patent US 9,768,047
Granted Patent B2
US 9,768,047 · App. 15/260,152 · Granted Sep 19, 2017

SiC epitaxial wafer and method for producing same, and device for producing SiC epitaxial wafer

Inventors: Yoshiaki Kageshima (Chichibu, JP); Daisuke Muto (Chichibu, JP); Kenji Momose (Chichibu, JP); Yoshihiko Miyasaka (Sanmu, JP)
Assignee: SHOWA DENKO K.K.
H01L21/681C23C16/325C23C16/4401C23C16/52C30B25/02C30B25/12C30B25/16C30B29/36H01L21/0262H01L21/02378H01L21/02433H01L21/02529H01L21/02576H01L29/1608H01L29/34
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Quick Facts
Patent No.
US 9,768,047
App. No.
15/260,152
Granted
Sep 19, 2017
Kind
B2
Abstract

A SiC epitaxial wafer manufacturing method of the present invention includes: manufacturing a SiC epitaxial wafer including a SiC epitaxial layer on a surface of a SiC single crystal wafer while supplying a raw material gas into a chamber using a SiC epitaxial wafer manufacturing apparatus; and manufacturing a subsequent SiC epitaxial wafer after measuring a surface density of triangular defects originating from a material piece of an internal member of the chamber on the SiC epitaxial layer of the previously manufactured SiC epitaxial wafer.

Claims (16)

1. A measurement method of a triangular defect, which is present in a SiC epitaxial layer formed on a SiC single crystal substrate in a SiC epitaxial wafer, by using an optical microscope or an optical surface inspection apparatus using a laser beam, comprising

shifting a position of focus in an optical image from a surface of the SiC epitaxial layer toward an interface between the SiC epitaxial layer and the SiC single crystal substrate, to thereby identify a starting point of the triangular defect, wherein

the triangular defect has a material piece of an internal member of a chamber as the starting point and

the triangular defect is a triangle-shaped defect which has the material piece of the internal member of the chamber as an apex and is formed along a step-flow growth direction in which the apex of a triangle and its opposite side (base) are sequentially arranged.

2. The measurement method according to claim 1 , further comprising: analyzing a composition of the triangular defect by using an energy dispersive X-ray spectroscopy.

3. A SiC epitaxial wafer manufacturing method comprising:

manufacturing a SiC epitaxial wafer including a SiC epitaxial layer on a surface of a SiC single crystal wafer while supplying a raw material gas into a chamber by using a SiC epitaxial wafer manufacturing apparatus;

manufacturing a subsequent SiC epitaxial wafer after a measurement of a surface density of a triangular defect, which has a material piece of an internal member of the chamber as a starting point, in the SiC epitaxial layer of the previously manufactured SiC epitaxial wafer; and

replacing the internal member of the chamber according to a result of the measurement of the surface density of the triangular defect, wherein

the measurement of the surface density of the triangular defect comprises shifting a position of focus in an optical image of an optical microscope or an optical surface inspection apparatus using a laser beam from a surface of the SiC epitaxial layer toward an interface between the SiC epitaxial layer and the SiC single crystal substrate, to thereby identify the starting point of the triangular defect.

4. The SiC epitaxial wafer manufacturing method according to claim 3 , wherein

the SiC epitaxial wafer manufacturing apparatus includes: a susceptor that includes a wafer placement unit on which a wafer is placed; a top plate that is disposed to face an upper surface of the susceptor so that a reaction space is formed between the susceptor and the top plate; and a shielding plate that is disposed to be close to a lower surface of the top plate to such an extent that a deposit is prevented from being attached to the lower surface of the top plate, and

the internal member of the chamber to be replaced is the shielding plate.

5. The SiC epitaxial wafer manufacturing method according to claim 3 , wherein

the SiC epitaxial wafer manufacturing apparatus includes: a susceptor that includes a wafer placement unit on which a wafer is placed; and a top plate that is disposed to face an upper surface of the susceptor so that a reaction space is formed between the susceptor and the top plate, and

the internal member of the chamber to be replaced is the top plate.

Assignments (3)
CHANGE OF ADDRESS Recorded Feb 14, 2024
From: RESONAC CORPORATION
To: RESONAC CORPORATION
Reel/Frame 066599/0037 →
CHANGE OF NAME Recorded Jun 23, 2023
From: SHOWA DENKO K.K.
To: RESONAC CORPORATION
Reel/Frame 064082/0513 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2016
From: KAGESHIMA, YOSHIAKI; MUTO, DAISUKE; MOMOSE, KENJI; MIYASAKA, YOSHIHIKO
To: SHOWA DENKO K.K.
Reel/Frame 040258/0903 →
Priority Claims (1)
JP 2011-157918 · Jul 19, 2011 · national
Continuity (2)
Division 14233289
Related Publication 20160379860A1 · Dec 29, 2016