IP Library Granted Patent US 9,890,160
Granted Patent B2
US 9,890,160 · App. 15/335,751 · Granted Feb 13, 2018

Compounds I

Inventors: Edward Savory (Cambourne, GB); Michael Higginbottom (Caldecote, GB); Kathryn Oliver (Cambridge, GB); Viet-Anh Anne Horgan (Redhill, GB)
Assignee: PROXIMAGEN LIMITED
C07D471/04A61K31/437
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Quick Facts
Patent No.
US 9,890,160
App. No.
15/335,751
Granted
Feb 13, 2018
Kind
B2
Abstract

The present invention relates to compounds of formula (I), and their pharmaceutically acceptable salts, solvates, hydrates, geometrical isomers, tautomers, optical isomers or N-oxides, which are inhibitors of SSAO activity. The invention further relates to pharmaceutical compositions comprising these compounds and to the use of these compounds for the treatment of medical conditions wherein inhibition of SSAO activity is beneficial, such as inflammatory diseases and immune disorders.

Claims (77)

1. A compound of formula (I),

or a pharmaceutically acceptable salt, solvate, hydrate, geometrical isomer, tautomer, optical isomer or N-oxide thereof, wherein:

R 1 is selected from:

(a) hydrogen,

(b) C 1-6 -alkyl, and

(c) —NR 4A R 4B ;

R 2 is selected from:

(a) hydrogen,

(b) C 1-6 -alkyl,

(c) halo-C 1-6 -alkyl,

(d) hydroxy-C 1-6 -alkyl,

(e) C 1-6 -alkoxy-C 1-6 -alkyl,

(f) halo-C 1-6 -alkoxy-C 1-6 -alkyl,

(g) N(R 4A R 4B )—C 1-6 -alkyl,

(h) —C(O)NR 4A R 4B , and

(i) —C(O)O—C 1-6 -alkyl;

R 3 is a heterocyclyl optionally substituted with one or more substituents independently selected from halogen, hydroxy, C 1-4 -alkyl, C 1-4 -alkoxy and —NR 4A R 4B ; and

R 4A and R 4B are each independently selected from:

(a) hydrogen,

(b) C 1-6 -alkyl, and

(c) C 1-6 -acyl.

2. A compound according to claim 1 , wherein R 1 is H.

3. A compound according to claim 1 , wherein R 2 is selected from hydrogen, —C(O)O—C 1-3 -alkyl and —C(O)NR 4A′ R 4B′ , and wherein R 4A′ and R 4B′ are independently selected from hydrogen and C 1-2 -alkyl.

4. A compound according to claim 1 , wherein R 3 is heterocyclyl optionally substituted with one or two substituents independently selected from halogen and C 1-2 -alkyl.

5. A pharmaceutical formulation containing a compound of formula (I),

or a pharmaceutically acceptable salt, solvate, hydrate, geometrical isomer, tautomer, optical isomer or N-oxide thereof, wherein:

R 1 is selected from:

(a) hydrogen,

(b) C 1-6 -alkyl, and

(c) —NR 4A R 4B ;

R 2 is selected from:

(a) hydrogen,

(b) C 1-6 -alkyl,

(c) halo-C 1-6 -alkyl,

(d) hydroxy-C 1-6 -alkyl,

(e) C 1-6 -alkoxy-C 1-6 -alkyl,

(f) halo-C 1-6 -alkoxy-C 1-6 -alkyl,

(g) N(R 4A R 4B )—C 1-6 -alkyl,

(h) —C(O)NR 4A R 4B , and

(i) —C(O)O—C 1-6 -alkyl;

R 3 is a heterocyclyl optionally substituted with one or more substituents independently selected from halogen, hydroxy, C 1-4 -alkyl, C 1-4 -alkoxy and —NR 4A R 4B ; and

R 4A and R 4B are each independently selected from:

(a) hydrogen,

(b) C 1-6 -alkyl, and

(c) C 1-6 -acyl

as active ingredient, in combination with a pharmaceutically acceptable diluent or carrier.

6. A method for the treatment of a mammal, including man, having inflammation, an inflammatory disease, an immune or an autoimmune disorder associated with SSAO inhibition, which comprises administering to the mammal, including man, an effective amount of a compound of formula (I),

or a pharmaceutically acceptable salt, solvate, hydrate, geometrical isomer, tautomer, optical isomer or N-oxide thereof, wherein:

R 1 is selected from:

(d) hydrogen,

(e) C 1-6 -alkyl, and

(f) —NR 4A R 4B ;

R 2 is selected from:

(j) hydrogen,

(k) C 1-6 -alkyl,

(l) halo-C 1-6 -alkyl,

(m) hydroxy-C 1-6 -alkyl,

(n) C 1-6 -alkoxy-C 1-6 -alkyl,

(o) halo-C 1-6 -alkoxy-C 1-6 -alkyl,

(p) N(R 4A R 4B )—C 1-6 -alkyl,

(q) —C(O)NR 4A R 4B , and

(r) —C(O)O—C 1-6 -alkyl;

R 3 is a heterocyclyl optionally substituted with one or more substituents independently selected from halogen, hydroxy, C 1-4 -alkyl, C 1-4 -alkoxy and —NR 4A R 4B ; and

R 4A and R 4B are each independently selected from:

(d) hydrogen,

(e) C 1-6 -alkyl, and

(f) C 1-6 -acyl.

7. The method according to claim 6 , wherein the inflammation or inflammatory disease or immune or autoimmune disorder is arthritis (including rheumatoid arthritis, juvenile rheumatoid arthritis, osteoarthritis and psoriatic arthritis), synovitis, vasculitis, a condition associated with inflammation of the bowel (including Crohn's disease, ulcerative colitis, inflammatory bowel disease and irritable bowel syndrome), atherosclerosis, multiple sclerosis, Alzheimer's disease, vascular dementia, a pulmonary inflammatory disease (including asthma, chronic obstructive pulmonary disease and acute respiratory distress syndrome), a fibrotic disease (including idiopathic pulmonary fibrosis, cardiac fibrosis and systemic sclerosis (scleroderma)), an inflammatory disease of the skin (including contact dermatitis, atopic dermatitis and psoriasis), systemic inflammatory response syndrome, sepsis, an inflammatory and/or autoimmune condition of the liver (including autoimmune hepatitis, primary biliary cirrhosis, alcoholic liver disease, sclerosing cholangitis, and autoimmune cholangitis), diabetes (type I or II) and/or the complications thereof, chronic heart failure, congestive heart failure, an ischemic disease (including stroke and ischemia-reperfusion injury) or myocardial infarction and/or the complications thereof.

8. The method according to claim 6 , wherein the inflammatory disease is vasculitis.

9. The method according to claim 7 , wherein the inflammatory disease is arthritis.

10. The method according to claim 9 , wherein the inflammatory disease is osteoarthritis.

11. The method according to claim 9 , wherein the inflammatory disease is rheumatoid arthritis.

12. The method according to claim 6 , wherein the inflammatory disease is psoriasis.

13. The compound of claim 1 , wherein R 3 is tetrahydrofuranyl.

14. The compound of claim 13 , wherein the tetrahydrofuranyl is optionally substituted with one or two substituents independently selected from halogen and C 1-2 -alkyl.

15. The compound of claim 1 that is (3S)-Tetrahydrofuran-3-yl (4S)-4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c]-pyridine-5-carboxylate, or a pharmaceutically acceptable salt thereof.

16. The compound of claim 1 that is (3R)-1-methylpyrrolidin-3-yl 4-isopropyl-1,4,6,7-tetrahydro-5H-imidazo[4,5-c] pyridine-5-carboxylate, or a pharmaceutically acceptable salt thereof.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 15, 2022
From: BENEVOLENTAI CAMBRIDGE LIMITED
To: PROXIMAGEN, LLC
Reel/Frame 059265/0350 →
CHANGE OF ADDRESS Recorded Mar 22, 2019
From: BENEVOLENTAI CAMBRIDGE LIMITED
To: BENEVOLENTAI CAMBRIDGE LIMITED
Reel/Frame 048676/0176 →
CHANGE OF NAME Recorded Dec 17, 2018
From: PROXIMAGEN LIMITED
To: BENEVOLENTAI CAMBRIDGE LIMITED
Reel/Frame 047799/0165 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 27, 2016
From: SAVORY, EDWARD; HIGGINBOTTOM, MICHAEL; OLIVER, KATHRYN; HORGAN, VIET-ANH ANNE
To: PROXIMAGEN LIMITED
Reel/Frame 040149/0608 →
Priority Claims (1)
SE 0801979 · Sep 16, 2008 · national
Continuity (6)
Continuation 14684813 · Apr 13, 2015
Continuation 14062969 · Oct 25, 2013
Continuation 13567146 · Aug 6, 2012
Division 13062318
Provisional Application 61106734 · Oct 20, 2008
Related Publication 20170044157A1 · Feb 16, 2017