IP Library Granted Patent US 10,179,108
Granted Patent B2
US 10,179,108 · App. 15/366,900 · Granted Jan 15, 2019

Compositions for treatment of attention deficit hyperactivity disorder

Inventors: David Lickrish (Camana Bay, KY); Feng Zhang (Pflugerville, TX)
Assignee: IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.
A61K9/2866A61K9/0053A61K9/4808A61K9/5015A61K9/5026A61K9/5042A61K9/5047A61K9/5073A61K9/5084A61K31/137A61K31/4458A61K9/5078
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Quick Facts
Patent No.
US 10,179,108
App. No.
15/366,900
Granted
Jan 15, 2019
Kind
B2
Abstract

Therapeutic compositions and methods for treatment of attention deficit disorder (ADD) or attention deficit hyperactivity disorder (ADHD) and other CNS stimulant responsive conditions include dosage forms that deliver a therapeutic amount of active drug in a delayed and controlled release formulation. The dosage form can be administered at night and drug release is delayed for from 5 to 8 hours or longer, followed by an extended release.

Claims (12)

1. A solid, oral pharmaceutical composition comprising coated particles:

said particles comprising:

(a) a core comprising dextroamphetamine or a pharmaceutical salt thereof;

(b) a sustained release layer enclosing the core, wherein the sustained release layer comprises a water-insoluble and water-permeable polymer, a water soluble polymer, a hydrophobic plasticizer, and a hydrophobic binder; and

(c) a delayed release layer enclosing the sustained release layer, wherein the delayed release layer comprises a pH dependent polymer or copolymer that is insoluble in aqueous medium at pH lower than 5.5; wherein the formulation provides at least an 8 hour lag time during which the formulation releases no more than 10% of the total dextroamphetamine or a pharmaceutical salt thereof, followed by a sustained release period of 10-12 hours when the composition is placed in 700 ml aqueous solution of 0.1N HC 1 pH 1.1 for up to 2 hours, followed by 4 hours in sodium phosphate buffer at pH 6.0, followed by 14 hours in sodium phosphate buffer, pH 7.2 at 37° C.±.0.5° C., as measured by the USP Apparatus I.

2. The composition of claim 1 , wherein the core comprises dextroamphetamine sulfate.

3. The composition of claim 1 , wherein the sustained release layer comprises ethyl cellulose, hydroxypropyl cellulose, dibutyl sebacate and a metal stearate.

4. The composition of claim 1 , wherein the sustained release layer comprises ethyl cellulose, hydroxypropyl cellulose, dibutyl sebacate and magnesium stearate.

5. The composition of claim 1 , wherein the pH dependent copolymer is methacrylic acid copolymer Type B.

6. The composition of claim 1 , further comprising mono- and diglycerides, dibutyl sebacate and polysorbate 80.

7. The composition of claim 1 , contained in a single dosage form containing 1 mg to 80 mg of dextroamphetamine or a pharmaceutical salt thereof.

8. The composition of claim 1 , wherein the sustained release layer comprises ethyl cellulose and hydroxypropyl cellulose in a ratio of about 1:3 to 1:5, dibutyl sebacate and from 25% to 50% by weight magnesium stearate.

Assignments (9)
SECURITY INTEREST Recorded Dec 23, 2025
From: COLLEGIUM PHARMACEUTICAL, INC.; BIODELIVERY SCIENCES INTERNATIONAL, INC.; IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.
To: TRUIST BANK, A NORTH CAROLINA CHARTERED BANK
Reel/Frame 073302/0334 →
RELEASE OF SECURITY INTEREST Recorded Dec 23, 2025
From: BIOPHARMA CREDIT PLC
To: IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.
Reel/Frame 073308/0416 →
RELEASE OF SECURITY INTEREST Recorded Dec 5, 2025
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION
To: IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.; HIGHLAND THERAPEUTICS INC.; NORTH SOUND PHARMACEUTICALS, INC.; IRONSHORE PHARMACEUTICALS INC.
Reel/Frame 073133/0245 →
PATENT SECURITY AGREEMENT Recorded Sep 3, 2024
From: IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.
To: BIOPHARMA CREDIT PLC
Reel/Frame 068826/0711 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 13, 2017
From: ZHANG, FENG
To: FORMULATION TECHNOLOGIES, LLC DBA PHARMAFORM
Reel/Frame 041239/0710 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 13, 2017
From: HIGHLAND THERAPEUTICS, INC.
To: IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.
Reel/Frame 041240/0075 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 13, 2017
From: LICKRISH, DAVID
To: IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.
Reel/Frame 041240/0169 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 13, 2017
From: FORMULATION TECHNOLOGIES LLC DBA PHARMAFORM
To: HIGHLAND THERAPEUTICS INC.
Reel/Frame 041695/0172 →
SECURITY INTEREST Recorded Jan 23, 2017
From: IRONSHORE PHARMACEUTICALS & DEVELOPMENT, INC.; HIGHLAND THERAPEUTICS INC.; NORTH SOUND PHARMACEUTICALS, INC.; IRONSHORE PHARMACEUTICALS INC.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 041048/0299 →
Continuity (10)
Continuation 15076253 · Mar 21, 2016
Continuation 14841428 · Aug 31, 2015
Continuation 14255529 · Apr 17, 2014
Continuation In Part 14230053 · Mar 31, 2014
Continuation In Part 14230067 · Mar 31, 2014
Continuation In Part 13429292 · Mar 23, 2012
Continuation In Part 13429292 · Mar 23, 2012
Provisional Application 61561763 · Nov 18, 2011
Provisional Application 61466684 · Mar 23, 2011
Related Publication 20170079937A1 · Mar 23, 2017
Cited By (1)
US 12,383,506