IP Library › Granted Patent US 10,421,933
Granted Patent B2
US 10,421,933 · App. 15/392,764 · Granted Sep 24, 2019

Solid rinse aid composition and method of making same

Inventors: Xin Sun (Eagan, MN); Derrick Anderson (Vadnais Heights, MN); Kelsey West (St. Paul, MN); Janel Marie Kieffer (Hastings, MN); Victor Fuk-Pong Man (St. Paul, MN); Melissa Hunter (Lakeville, MN)
Assignee: Ecolab USA Inc.
C11D17/0047C11D1/66C11D1/72C11D3/042C11D3/2075C11D3/2082C11D3/2086C11D3/3418C11D3/3463C11D11/0023C11D11/0029C11D11/0035
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Quick Facts
Patent No.
US 10,421,933
App. No.
15/392,764
Granted
Sep 24, 2019
Kind
B2
Abstract

The invention includes a solid rinse aid that is particularly designed for pressed or extrusion solid formation and which is effective for spotless surfaces after rinsing, especially rinsing metals without corrosion. According to the invention, a solid acid is combined with a short-chain alkylbenzene and alkyl naphthalene sulfonate. The short-chain alkylbenzene and alkyl naphthalene sulfonate act as a solidification agent as well as a hydrotrope, and total dissolved solid (TDS) active and are combined with at least one nonionic low foaming surfactant.

Claims (22)

1. A method of making a solid rinse aid composition comprising:

a. admixing a solid acid, nonionic surfactant, and one or more short chain alkyl benzene and/or alkyl naphthalene sulfonates to form a mixture;

b. allowing said mixture to set and thereafter;

c. mixing in any liquid components comprising a preservative, additional surfactant, water, dye, or combination thereof to form a rinse aid mixture;

d. forming a solid rinse aid composition with the rinse aid mixture,

wherein the solid rinse aid composition comprises from about 5 wt. % to about 40 wt. % of the solid acid;

from about 65 wt. % to about 90 wt. % of the one or more short chain alkyl benzene and/or alkyl naphthalene sulfonates, wherein said one or more short chain alkyl benzene and/or alkyl naphthalene sulfonates includes one or more of the following: sodium xylene sulfonate, sodium toluene sulfonate, sodium cumene sulfonate, potassium toluene sulfonate, ammonium xylene sulfonate, calcium xylene sulfonate, sodium C1-C4 naphthalene sulfonate, and sodium butylnaphthalene sulfonate; and

from about 5 wt. % to about 30 wt. % of the nonionic surfactant;

wherein said solid acid does not contain fatty acid or fatty acid salt; and

wherein said solid rinse aid composition provides a use solution with a pH of less than 2.

2. The method of claim 1 wherein said forming a solid is by pressing.

3. The method of claim 1 wherein said forming a solid is by extrusion.

4. The method of claim 1 wherein said mixture is allowed to set for 1 or more days.

5. The method of claim 1 , wherein the solid rinse aid composition further comprises from 0.05 wt. % to about 20 wt. % of a preservative.

6. The method of claim 5 , wherein the preservative comprises 5-chloro-2-methyl-4-isothiazolin-3-one and 2-methyl-4-isothiazolin-3-one.

7. The method of claim 1 , wherein the solid rinse aid composition further comprises from 0.1 wt. % to about 30 wt. % of a chelant.

8. The method of claim 7 , wherein said chelant is an aminocarboxylate.

9. The method of claim 1 , wherein said solid acid is citric acid.

10. The method of claim 1 , wherein said nonionic surfactant is a low foaming surfactant.

11. The method of claim 10 , wherein the solid rinse aid composition is formed by extrusion and wherein said low foaming surfactant is present in an amount of from about 5 wt. % to about 30 wt. %.

12. The method of claim 10 , wherein the solid rinse aid composition is formed by pressing and wherein said low foaming surfactant is present in an amount of from about 5 wt. % to about 20 wt. %.

13. The method of claim 1 , wherein said solid acid is present in an amount of from about 15 wt. % to about 25 wt. %.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 29, 2016
From: SUN, XIN; ANDERSON, DERRICK; WEST, KELSEY; KIEFFER, JANEL MARIE; MAN, VICTOR FUK-PONG; HUNTER, MELISSA
To: ECOLAB USA INC.
Reel/Frame 041210/0713 →
Continuity (3)
Division 14010815 · Aug 27, 2013
Continuation In Part 13530152 · Jun 22, 2012
Related Publication 20170107463A1 · Apr 20, 2017
Cited By (2)
US 12,686,836 US 12,716,044