IP Library Granted Patent US 10,912,311
Granted Patent B2
US 10,912,311 · App. 15/547,612 · Granted Feb 9, 2021

Process for treating sweet whey such as to obtain a protein material suitable for hypoallergenic infant formulae

Inventors: Peter Erdmann (Bern, CH); Gustavo Rocha (Freimettigen, CH); Gerard Terpstra (Cordast, CH)
Assignee: Societe des Produits Nestle S.A.
A23C9/146A23C21/00A23J1/205A23J3/08A23L33/18A23L33/19A23L33/40A23V2002/00
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Quick Facts
Patent No.
US 10,912,311
App. No.
15/547,612
Granted
Feb 9, 2021
Kind
B2
Abstract

The invention concerns a process for the treatment of a sweet whey material containing cGMP (caseinoGlycoMacroPeptide), said process comprising the following steps: —Decationising the sweet whey material so as to obtain sweet whey material having a pH value of 1 to 4.5; —Treating said sweet whey in a fluidized bed reactor comprising a specific volume of an anionic resin, at a temperature between 10 and 18° C., wherein said sweet whey contacts said resin for a sufficient amount of time so that the resin absorbs between 52% and 58% of the cGMP present in the sweet whey; and—Recovering a protein material. Advantageously, the protein material is suitable for hypoallergenic infant formulae.

Claims (11)

1. A process for treatment of a sweet whey material containing cGMP (caseinoGlycoMacroPeptide), the process comprising:

decationising the sweet whey material to obtain sweet whey having a pH value of 1 to 4.5;

treating the sweet whey in a fluidized bed reactor comprising a specific volume of an anionic resin at a temperature between 10 and 18° C. and at a ratio of protein over resin of 0.20 to 0.35 kg/L, wherein the sweet whey contacts the anionic resin for a sufficient amount of time, so that the anionic resin absorbs between 52% and 58% of the cGMP present in the sweet whey and at least 90% of anions present in the sweet whey; and

recovering a protein material suitable for hypoallergenic infant formulae, the protein material comprising a tryptophan:threonine ratio between 0.350 and 0.360.

2. The process according to claim 1 , wherein the anionic resin absorbs around 55% of the cGMP.

3. The process according to claim 1 , wherein the anionic resin absorbs at least 90% of anions present in the sweet whey.

4. The process according to claim 3 , wherein the anions are selected from the group consisting of chlorine, phosphorous, citrate, sulphate, lactate, and combinations thereof.

5. The process according to claim 1 , wherein the anionic resin absorbs at least 90% of chlorine and of phosphorous anions present in the sweet whey.

6. The process according to claim 1 comprising treating the sweet whey in the fluidized bed reactor at a ratio of cGMP over resin between 39 and 41 g/L.

7. The process according to claim 1 , wherein the sweet whey material is selected from the group consisting of sweet whey obtained after separation of casein coagulated with rennet, a concentrate of sweet whey, a sweet whey demineralized by electrodialysis, ion exchange, reverse osmosis, electrodeionisation or a combination thereof, a concentrate of sweet whey demineralized by electrodialysis, ion exchange, reverse osmosis, electrodeionisation or a combination thereof, a concentrate of proteins of substantially lactose-free sweet whey obtained by ultrafiltration followed by diafiltration, mother liquors of the crystallization of lactose from sweet whey, a permeate of ultrafiltration of a sweet whey, a product of hydrolysis by a protease of a native casein obtained by acid precipitation of skimmed milk with an inorganic acid or by biological acidification obtained by microfiltration of a skimmed milk, a product of hydrolysis of a caseinate by a protease, and combinations thereof.

8. The process according to claim 1 , wherein the sweet whey has a solid content of about 10 to 30 percent by weight after decationisation.

Assignments (5)
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0001 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT NUMBER 16062921 PREVIOUSLY RECORDED ON REEL 049391 FRAME 0756. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT NUMBER SHOULD HAVE BEEN 16062912. Recorded Jul 3, 2020
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 054082/0165 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ENGLISH TRANSLATION TO SHOW THE FULL AND CORRECT NEW NAME IN SECTION 51. PREVIOUSLY RECORDED AT REEL: 049391 FRAME: 0756. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded Jun 13, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049853/0398 →
MERGER Recorded Jun 6, 2019
From: NESTEC S.A.
To: SOCIÉTÉ DES PRODUITS NESTLÉ S.A.
Reel/Frame 049391/0756 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 17, 2017
From: ERDMANN, PETER; ROCHA, GUSTAVO; TERPSTRA, GERARD
To: NESTEC S.A.
Reel/Frame 044309/0663 →