Electron microscope
The objective of the present invention is to simultaneously achieve image observations at a high resolution using an electron microscope, and X-ray analysis at a high energy-resolution using a microcalorimeter. An X-ray detector is disposed at a position where the intensity of the magnetic field from an objective lens is weaker than the critical magnetic field of a material used in a thermal insulation shield for a superconducting transition-edge sensor or a microcalorimeter. In addition, an optical system for transmitting X-rays to the detector is inserted between a sample and the detector. Alternatively, a magnetic field shield for shielding the X-ray detector is used.
1. An electron microscope comprising:
an electron source that generates an electron beam;
an objective lens that focuses the electron beam on a sample;
an X-ray detector that detects X-rays generated from the sample and performs energy spectroscopy; and
an X-ray optical system that transmits X-rays generated from the sample to the X-ray detector such that the X-rays are transmitted far away from a tip of a magnetic path of the objective lens,
wherein the X-ray detector is disposed in a space where the intensity of a magnetic field formed from the objective lens is weaker than a predetermined intensity of the magnetic field.
2. The electron microscope according to claim 1 ,
wherein the x-ray detector includes a superconducting transition-edge sensor.
3. The electron microscope according to claim 2 ,
wherein the predetermined intensity of the magnetic field is the intensity of the critical magnetic field in which a superconducting state of the superconducting transition-edge sensor is destroyed.
4. The electron microscope according to claim 2 ,
wherein the X-ray detector has a thermal insulation shield made of a superconducting material, and
wherein the predetermined intensity of the magnetic field is the intensity of the critical magnetic field in which a superconducting state of the thermal insulation shield is destroyed.
5. The electron microscope according to claim 1 ,
wherein the X-ray detector is a microcalorimeter.
6. The electron microscope according to claim 1 ,
wherein the X-ray optical system is a poly-capillary lens.
7. The electron microscope according to claim 1 ,
wherein the X-ray optical system is disposed between an upper magnetic path and a lower magnetic path of the objective lens.
8. The electron microscope according to claim 1 ,
wherein the X-ray optical system is disposed on the electron source side from the upper magnetic path of the objective lens in a magnetic field formed by the upper magnetic path.
9. The electron microscope according to claim 1 ,
wherein the X-ray optical system is disposed on the sample side from the lower magnetic path of the objective lens in a magnetic field formed by the lower magnetic path.
10. The electron microscope according to claim 1 ,
wherein a lower magnetic path of the objective lens is disposed to be parallel to the sample.
11. An electron microscope comprising:
an electron source that generates an electron beam;
an objective lens that focuses the electron beam on a sample;
an X-ray detector that detects X-rays generated from the sample and performs energy spectroscopy; and
a magnetic field shield that shields the X-ray detector from a magnetic field formed from the objective lens,
wherein the X-ray detector is disposed in a space where the intensity of a magnetic field formed from the objective lens due to the magnetic field shield is weaker than a predetermined intensity of the magnetic field; and
wherein at least a part of the X-ray detector is disposed between an upper magnetic path and a lower magnetic path of the objective lens.
12. The electron microscope according to claim 11 ,
wherein the x-ray detector includes a superconducting transition-edge sensor.
13. The electron microscope according to claim 12 ,
wherein the predetermined intensity of the magnetic field is the intensity of the critical magnetic field in which a superconducting state of the superconducting transition-edge sensor is destroyed.
14. An electron microscope comprising:
an electron source that generates an electron beam;
an objective lens that focuses the electron beam on a sample;
an X-ray detector that detects X-rays generated from the sample and performs energy spectroscopy; and
a magnetic field shield that shields the X-ray detector from a magnetic field formed from the objective lens,
wherein the X-ray detector is disposed in a space where the intensity of a magnetic field formed from the objective lens due to the magnetic field shield is weaker than a predetermined intensity of the magnetic field;
wherein the x-ray detector includes a superconducting transition-edge sensor; and
wherein the X-ray detector has a thermal insulation shield made of a superconducting material, and
wherein the predetermined intensity of the magnetic field is the intensity of the critical magnetic field in which a superconducting state of the thermal insulation shield is destroyed.