IP Library Granted Patent US 10,059,966
Granted Patent B2
US 10,059,966 · App. 15/604,507 · Granted Aug 28, 2018

Processes for recovering products from a corn fermentation mash

Inventor: Jason Bootsma (Wichita, KS)
Assignee: Flint Hills Resources, LP
C12P7/14C12P19/02C12P19/14C12P2201/00
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Quick Facts
Patent No.
US 10,059,966
App. No.
15/604,507
Granted
Aug 28, 2018
Kind
B2
Abstract

Processes and systems for recovering products from a fermentation mash. In some examples, a process for recovering products from a fermentation mash can include processing a ground corn product to produce a fermentation mash that can include ethanol. At least a portion of the ethanol can be separated from the fermentation mash to produce a whole stillage. The whole stillage can be separated to produce a fiber rich product and a filtrate. The fiber rich product can be hydrolyzed to produce a saccharification mash. The saccharification mash can be processed to produce additional ethanol and a stillage protein product.

Claims (48)

1. A process for recovering products from a fermentation mash, comprising:

processing a ground corn product to produce a fermentation mash comprising ethanol;

separating at least a portion of the ethanol from the fermentation mash to produce a whole stillage;

separating the whole stillage to produce a fiber rich product and a filtrate;

hydrolyzing the fiber rich product to produce a saccharification mash; and

processing the saccharification mash to produce additional ethanol and a stillage protein product comprising about 15 wt % to about 35 wt % of yeast, based on a dry weight of the stillage protein product.

2. The process of claim 1 , wherein the stillage protein product comprises about 20 wt % to about 30 wt % of the yeast, based on the dry weight of the stillage protein product.

3. The process of claim 1 , wherein the stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product.

4. The process of claim 1 , wherein the stillage protein product further comprises protein, fat, ash, neutral detergent fibers, and acid detergent fibers, and wherein the stillage protein product comprises about 47 wt % to about 57 wt % of the protein, about 3 wt % to about 5 wt % of the fat, about 1 wt % to about 3 wt % of the ash, about 4 wt % to about 10 wt % of the neutral detergent fibers, about 5 wt % to about 10 wt % of the acid detergent fibers, and about 20 wt % to about 30 wt % of the yeast, based on the dry weight of the stillage protein product.

5. The process of claim 1 , wherein the fiber rich product has an ethanol potential of at least 90 gallons of ethanol per 1,000 kilograms of the fiber rich product.

6. The process of claim 1 , wherein the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product.

7. The process of claim 1 , wherein greater than 80 wt % of the ground corn product has a particle size of 425 μm or less, as measured according to AOAC 965.22-1966.

8. The process of claim 1 , wherein the fiber rich product is contacted with an acid or a base prior to hydrolyzing the fiber rich product to produce the saccharification mash.

9. The process of claim 1 , wherein:

greater than 80 wt % of the ground corn product has a particle size of 425 μm or less, as measured according to AOAC 965.22-1966,

the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product,

the fiber rich product is contacted with an acid or a base prior to hydrolyzing the fiber rich product to produce the saccharification mash, and

the stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product.

10. A process for recovering products from a fermentation mash, comprising:

processing a ground corn product to produce a fermentation mash comprising ethanol;

separating at least a portion of the ethanol from the fermentation mash to produce a whole stillage;

separating the whole stillage with a fiber filter to produce a fiber rich product and a filtrate;

hydrolyzing the fiber rich product to produce a saccharification mash; and

processing the saccharification mash to produce additional ethanol and a stillage protein product comprising about 15 wt % to about 35 wt % of yeast, based on a dry weight of the stillage protein product.

11. The process of claim 10 , wherein the fiber filter comprises a filter sleeve having openings of about 10 μm to less than 400 μm.

12. The process of claim 10 , wherein the fiber filter comprises a filter sleeve and a rotor disposed within the filter sleeve, and wherein the filter sleeve comprises a woven polymer fabric.

13. The process of claim 10 , wherein the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product.

14. The process of claim 10 , wherein the stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product.

15. The process of claim 10 , wherein the stillage protein product further comprises protein, fat, ash, neutral detergent fibers, and acid detergent fibers, and wherein the stillage protein product comprises about 47 wt % to about 57 wt % of the protein, about 3 wt % to about 5 wt % of the fat, about 1 wt % to about 3 wt % of the ash, about 4 wt % to about 10 wt % of the neutral detergent fibers, about 5 wt % to about 10 wt % of the acid detergent fibers, and about 20 wt % to about 30 wt % of the yeast, based on the dry weight of the stillage protein product.

16. The process of claim 10 , wherein:

the fiber filter comprises a filter sleeve having openings of about 10 μm to less than 400 μm,

the fiber rich product has an ethanol potential of at least 90 gallons of ethanol per 1,000 kilograms of the fiber rich product, and

the stillage protein product further comprises about 40 wt % to about 80 wt % of protein, about 3 wt % to about 20 wt % of fat, about 1 wt % to about 4 wt % of ash, about 2 wt % to about 30 wt % of neutral detergent fibers, and about 1 wt % to about 15 wt % of acid detergent fibers, based on the dry weight of the stillage protein product.

17. A process for recovering products from a fermentation mash, comprising:

processing a ground corn product to produce a fermentation mash comprising ethanol;

separating at least a portion of the ethanol from the fermentation mash to produce a whole stillage;

separating the whole stillage to produce a fiber rich product and a filtrate, wherein the fiber rich product has an ethanol potential of at least 90 gallons of ethanol per 1,000 kilograms of the fiber rich product,

hydrolyzing the fiber rich product to produce a saccharification mash;

processing the saccharification mash to produce additional ethanol and a stillage protein product comprising about 15 wt % to about 35 wt % of yeast, based on a dry weight of the stillage protein product, and

separating the filtrate to produce a protein rich portion, an oil product, and a clarified stillage.

18. The process of claim 17 , wherein the fiber rich product has an ethanol potential of about 100 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product.

19. The process of claim 17 , wherein the fiber rich product has an ethanol potential of about 135 gallons of ethanol per 1,000 kilograms of the fiber rich product to about 150 gallons of ethanol per 1,000 kilograms of the fiber rich product.

20. The process of claim 17 , wherein greater than 80 wt % of the ground corn product has a particle size of 425 μm or less, as measured according to AOAC 965.22-1966.

21. The process of claim 17 , wherein the whole stillage is separated with a fiber filter to produce the fiber rich product and the filtrate, and wherein the fiber filter comprises a filter sleeve having openings of about 10 μm to about 400 μm.

22. The process of claim 17 , further comprising:

removing water from the protein rich portion to produce a protein rich product; and

removing water from the clarified stillage to produce an evaporated clarified stillage.

23. The process of claim 5 , wherein the whole stillage is separated with a fiber filter to produce the fiber rich product and a filtrate.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2021
From: FLINT HILLS RESOURCES, LP
To: FLINT HILLS RESOURCES GRAIN, LLC
Reel/Frame 057308/0860 →
CHANGE OF NAME Recorded Aug 27, 2021
From: FLINT HILLS RESOURCES GRAIN, LLC
To: POET GRAIN (OCTANE), LLC
Reel/Frame 057339/0312 →
SECURITY INTEREST Recorded Jun 1, 2021
From: FLINT HILLS RESOURCES GRAIN, LLC
To: FHR B&I HOLDINGS, LLC
Reel/Frame 056404/0151 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2017
From: BOOTSMA, JASON
To: FLINT HILLS RESOURCES, LP
Reel/Frame 043426/0362 →
Continuity (6)
Continuation In Part 15529014
Continuation In Part 15604507
Continuation In Part 15529014
Provisional Application 62324159 · Apr 18, 2016
Provisional Application 62260181 · Nov 25, 2015
Related Publication 20170253892A1 · Sep 7, 2017
Cited By (1)
US 12,480,142