IP Library Granted Patent US 10,981,117
Granted Patent B2
US 10,981,117 · App. 15/742,661 · Granted Apr 20, 2021

Blended potting resins and use thereof

Inventors: Ganapathysubramanian Iyer (Woburn, MA); Cha Doh (Sudbury, MA)
Assignee: ENTEGRIS, INC.
B01D63/023B01D63/022C08J5/24C08L23/06C08L23/26C08J2323/06C08J2423/26C08J2477/00C08L2023/44C08L2205/025C08L2205/16C08L2207/04C08L2207/062
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Quick Facts
Patent No.
US 10,981,117
App. No.
15/742,661
Granted
Apr 20, 2021
Kind
B2
Abstract

A thermoplastic blended potting resin, a blended resin potted membrane, a membrane separation module, a fluid separation device, a method of making and a method of using the membrane separation module and the fluid separation device are described herein. The blended thermoplastic potting resin comprises at least one polar membrane having two end regions and a middle region; and a blended resin comprising a non-polar thermoplastic polymer and a polar thermoplastic polymer; wherein at least one of the two ends regions is coated with the blended potting resin to form a fluid-tight seal between the end regions and the open middle region, and wherein the polar thermoplastic polymer is 1% or greater by weight of blended resin.

Claims (30)

1. A blended resin potted membrane, comprising:

at least one membrane constructed of a first material and having a first end region, a second end region, and a middle region; and

a thermoplastic blended potting resin comprising a thermoplastic polymer modified with polar groups,

wherein the polar groups are about 0.1% or greater by weight of the total weight of the modified thermoplastic polymer,

wherein the polar groups are amides, alcohols, acid anhydrides, cyanides, sulfates, sulfonates, carboxylic acids, aldehydes, amines or ammonium groups, and

wherein at least one of the first end region and the second end region are encapsulated with the thermoplastic blended potting resin and bonded by the thermoplastic blended potting resin to a housing constructed of a second material, wherein the first material and the second material are physically or chemically incompatible.

2. The blend resin potted membrane of claim 1 , wherein the modified thermoplastic polymer comprises polar groups from about 0.05% to about 75% by weight of the total weight of the modified thermoplastic polymer.

3. The blended resin potted membrane of claim 1 , wherein the at least one membrane is a hollow fiber, a flat sheet, or a pleated sheet.

4. The blended resin potted membrane of claim 3 , wherein the at least one membrane is a hollow fiber.

5. The blended resin potted membrane of claim 1 , wherein the at least one membrane is a plurality of membranes.

6. The blended resin potted membrane of claim 1 , wherein the at least one membrane is a polyamide, a polyimideamide, a polyimide, a polysulfone, a cellulose acetate, a polyvinyl alcohol or a polyacrylate.

7. A membrane separation module, comprising:

at least one membrane constructed of a first material,

wherein the at least one membrane has a first potted end region, a second potted end region, and an open middle region, and

wherein the first potted region and the second potted region encapsulated in a thermoplastic blended potting resin comprising a thermoplastic polymer modified with polar groups, wherein the polar groups are about 0.1% or greater by weight of the total weight of the modified thermoplastic polymer, and wherein the polar groups are amides, alcohols, acid anhydrides, cyanides, sulfates, sulfonates, carboxylic acids, aldehydes, amines or ammonium groups; and

a housing constructed of a second material sealingly bonded to the membrane by the thermoplastic blended potting resin;

wherein the first material and the second material are physically or chemically incompatible; and

wherein the two potted end regions are encapsulated with the thermoplastic blended potting resin to form a fluid-tight seal between the two potted end regions and the open middle region.

8. The membrane separation module of claim 7 , wherein the at least one membrane is a hollow fiber, a flat sheet, or a pleated sheet.

9. The membrane separation module of claim 7 , wherein: (1) the first material is a polar material and the second material is a non-polar material; or (2) the first material is a non-polar material and the second material is a polar material.

10. A fluid separation device, comprising:

a housing having:

a first end and a second end;

a separation element contained within the housing to divide the interior of the housing into first and second volumes, the separation element comprising the membrane separation module of claim 7 and a series of flow passages upstream and downstream of said membrane module, and wherein the membrane module is bonded to the housing by the blended resin;

a first connector at the first end for introducing a fluid feed to the interior of the housing;

a second connector for removing a permeate from the interior of the housing;

a central conduit attached to the first connector and extending longitudinally within the housing to the second end so as direct all of the flow between the first connector and the second end;

wherein the second end is in fluid communication with the first volume,

wherein the second volume is in fluid communication with the second connector, and

wherein a fluid fed into the first connector is processed by the separation element to form the permeate collected and removed by the second connector.

Assignments (4)
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
ASSIGNMENT OF PATENT SECURITY INTEREST RECORDED AT REEL/FRAME 048811/0679 Recorded Nov 5, 2019
From: GOLDMAN SACHS BANK USA
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 050965/0035 →
SECURITY INTEREST Recorded Nov 13, 2018
From: ENTEGRIS, INC.; SAES PURE GAS, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 048811/0679 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 19, 2018
From: IYER, GANAPATHYSUBRAMANIAN; DOH, CHA
To: ENTEGRIS, INC.
Reel/Frame 047233/0116 →
Continuity (2)
Provisional Application 62190617 · Jul 9, 2015
Related Publication 20180200676A1 · Jul 19, 2018
Cited By (1)
US 12,378,514