Method to prevent grounding from a silicon rod to a plate in polycrystalline silicon reactor
A method to prevent groundings of polycrystalline silicon rod holders to a reactor plate by the residual polymer in the following manner: first, providing a polycrystalline silicon reactor having a reactor plate with a plurality of silicon rod holders separated from the reactor plate with an insulation; next establishing an electrical circuit from a ground connection on the reactor plate connected to high potential test equipment to a high voltage probe; and finally completing the electrical circuit by contacting the high voltage probe to the holder. By this method any remaining polymer is physically removed as the polymer burns or is ejected by the energetic release caused by mild arcing from the holder to the reactor plate.
1. A process to prevent grounding from a silicon rod to a reactor plate in a polycrystalline reactor comprising:
providing the polycrystalline silicon reactor having the reactor plate with a plurality of silicon rod holders each separated from the reactor plate with an insulation;
establishing an electrical circuit from a ground connection on the reactor plate connected to a potential test equipment further connected to a voltage probe; and
completing the electrical circuit by contacting the high voltage probe to one rod holder of the plurality of rod holders;
wherein any remaining polymer in the polycrystalline silicon reactor deposited completely or partially on the one rod holder or the one rod holder insulation is physically removed as the remaining polymer burns or is ejected by an energetic release caused by arcing from the rod holder to the reactor plate.
2. The process according to claim 1 further comprising setting the potential test equipment in the range of about 5 to 30 milliamperes and about 1,500 to 4,000 volts for delivery of a set amount of milliamperes and volts to the one rod holder.
3. The process according to claim 1 further comprising setting the potential test equipment at about 15 milliamperes and about 2,500 volts for delivery of a set amount of milliamperes and volts to the one rod holder.
4. The process according to claim 3 further comprising completing the electrical circuit on each rod holder of the plurality of rod holders for about 10 seconds to about 90 seconds.
5. The process according to claim 3 further comprising completing the electrical circuit on each rod holder of the plurality of rod holders for about 30 seconds.