IP Library Granted Patent US 10,066,290
Granted Patent B1
US 10,066,290 · App. 15/969,958 · Granted Sep 4, 2018

Sintered compact magnesium oxide target for sputtering, and method for producing same

Inventors: Akira Hisano (Ibaraki, JP); Yuichiro Nakamura (Ibaraki, JP)
Assignee: JX Nippon Mining & Metals Corporation
C23C14/3407C04B35/053C04B35/645C23C14/081C23C14/3414C04B2235/442C04B2235/5445C04B2235/721C04B2235/77C04B2235/81C04B2235/9646C04B2235/9661
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Quick Facts
Patent No.
US 10,066,290
App. No.
15/969,958
Granted
Sep 4, 2018
Kind
B1
Abstract

A sintered compact magnesium oxide target for sputtering has a purity of 99.99 wt % or higher excluding C, a density of 3.57 g/cm 3 or higher, and a whiteness of 60% or less. To uniformly deposit a magnesium oxide film, a magnesium oxide target having a higher purity and a higher density is demanded. An object is to provide a target capable of realizing the above and a method for producing such a target. While a magnesium oxide sintered compact sputtering target is produced by hot-pressing a raw material powder, there is a problem in that color shading occurs in roughly φ60 (within a circle having a diameter of 60 mm) at the center part of the target. Conventionally, no particularly attention was given to this problem. However, in recent years, it has become necessary to investigate and resolve this problem in order to improve the deposition quality.

Claims (4)

1. A method for producing a sputtering target comprising a sintered compact of magnesium oxide, comprising the steps of:

adding raw material powder of MgCO 3 in an amount of 5 wt % or more and less than 30 wt % to raw material powder of magnesium oxide (MgO), the raw material powders of magnesium oxide (MgO) and MgCO 3 having a purity of 99.99 wt % or higher excluding C and an average grain size of 0.5 μm or less;

mixing the raw material powder of MgCO 3 with the raw material powder of magnesium oxide (MgO) to produce a mixture; and

hot pressing the mixture at a temperature of 1500° C. or less and an applied pressure of 300 kgf/cm 2 or more to obtain a sintered compact of magnesium oxide having a purity of 99.99 wt % or higher excluding C, a density of 3.57 g/cm 3 or higher, and a whiteness of 60% or less.

Assignments (2)
CHANGE OF ADDRESS Recorded Aug 11, 2021
From: JX NIPPON MINING & METALS CORPORATION
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 057160/0114 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 3, 2018
From: HISANO, AKIRA; NAKAMURA, YUICHIRO
To: JX NIPPON MINING & METALS CORPORATION
Reel/Frame 045707/0823 →
Priority Claims (1)
JP 2011-285757 · Dec 27, 2011 · national
Continuity (1)
Division 14356395
Cited By (1)
US 12,224,166