Apparatus and method for analyzing evolved gas
Disclosed is an apparatus and method for analyzing an evolved gas, wherein the precision of detection of a gas component is improved without enlarging the apparatus. The apparatus includes a gas component evolving unit, a detection member for detecting the gas component, and a mixed gas channel for allowing a mixed gas containing the gas component and carrier gas to flow therethrough, and further includes a branch channel branched from the mixed gas channel, an inert gas channel for allowing an inert gas to flow therethrough, a first flow rate regulator for adjusting the flow rate of the carrier gas, a second flow rate regulator for adjusting the flow rate of the inert gas, and a flow rate control unit for controlling the second flow rate regulator such that the flow rate of the mixed gas guided to the detection member is a predetermined value.
1. An apparatus for analyzing an evolved gas, comprising:
a gas component evolving unit configured to evolve a gas component contained in a sample,
a detection member configured to detect the gas component evolved from the gas component evolving unit, and
a mixed gas channel configured to connect the gas component evolving unit and the detection member to each other and to allow a mixed gas comprising the gas component and a carrier gas for guiding the gas component to the detection member to flow therethrough,
and further comprising:
a branch channel branched from the mixed gas channel and open to an outside,
an inert gas channel joined to the detection member downstream of the branch channel such that an inert gas is allowed to flow therethrough to the detection member,
a first flow rate regulator configured to adjust a flow rate F 1 of the carrier gas,
a second flow rate regulator configured to adjust a flow rate F 4 the inert gas flowing through the inert gas channel, and
a flow rate control unit configured to control a split ratio using the second flow rate regulator, thereby controlling a flow rate of the mixed gas guided to the detection member to a predetermined value,
wherein the detection member is a mass spectrometer, and an ion source is provided between the mixed gas channel and the mass spectrometer so as to ionize the gas component of the mixed gas, the inert gas is allowed to flow to the ion source of the spectrometer, and a junction at which the inert gas channel is joined to the mixed gas channel is configured to be open to the outside downstream of the branch channel, the junction comprising a hole in a housing unit of the apparatus that couples a longitudinal end of the mixed gas channel with an end portion of the inert gas channel.
2. The apparatus of claim 1 , wherein a discharge pressure regulator for adjusting a discharge pressure of the mixed gas discharged from the branch channel is provided at a discharge side of the branch channel.
3. The apparatus of claim 1 , wherein the flow rate control unit controls the first flow rate regulator so as to increase the flow rate F 1 when a detection signal from the detection member is less than a predetermined range.
4. The apparatus of claim 2 , wherein the detection member is a mass spectrometer, and an ion source is provided between the mixed gas channel and the mass spectrometer so as to ionize the gas component of the mixed gas, and
the flow rate control unit controls the first flow rate regulator so as to increase the flow rate F 1 when a detection signal from the detection member is less than a predetermined range.
5. The apparatus of claim 3 , further comprising a flow rate measurement instrument for measuring the flow rate of the mixed gas flowing into the detection member or the flow rate of the mixed gas discharged from the branch channel.
6. The apparatus of claim 4 , further comprising a flow rate measurement instrument for measuring the flow rate of the mixed gas flowing into the detection member or the flow rate of the mixed gas discharged from the branch channel.