IP Library Granted Patent US 10,723,641
Granted Patent B2
US 10,723,641 · App. 16/108,369 · Granted Jul 28, 2020

Sodium nitrite oxidation of hydrogen sulfide

Inventors: Jack G. Frost (Duncan, OK); Kenneth J. Snyder, Jr. (Addington, OK)
Assignee: United Laboratories International, LLC
C02F1/72C02F1/20C02F1/66C02F2101/101C02F2103/365
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Quick Facts
Patent No.
US 10,723,641
App. No.
16/108,369
Granted
Jul 28, 2020
Kind
B2
Abstract

A method for treating hydrogen sulfide in a solution includes providing the solution containing hydrogen sulfide. The method also includes adding sodium nitrite to the solution in an amount suitable to react with the hydrogen sulfide and treat the hydrogen sulfide.

Claims (24)

1. A method for removing hydrogen sulfide comprising:

providing a solution comprising hydrogen sulfide;

adding sodium nitrite to the solution comprising hydrogen sulfide; and

adding a pH buffer to the solution to maintain a pH of the solution between about 7.0 to about 9.0, wherein the pH buffer removes free ammonia from the solution.

2. The method of claim 1 , wherein the concentration of hydrogen sulfide in the solution is about 2,000 mg/liter to about 25,000 mg/liter.

3. The method of claim 1 , wherein the sodium nitrite is added at a weight ratio to the hydrogen sulfide from about 0.676:1 to about 5:1.

4. The method of claim 1 , wherein the pH buffer comprises an acidic buffering chemical.

5. The method of claim 1 , wherein the solution further comprises water.

6. The method of claim 1 , wherein the adding of the sodium nitrite is performed at a temperature of from about ambient temperature to about a boiling temperature of the solution.

7. The method of claim 1 , wherein the adding of sodium nitrite is performed at a temperature of from about 40° C. to about 70° C.

8. The method of claim 1 , wherein a reaction between the hydrogen sulfide and the sodium nitrite produces ammonia.

9. A method for removing hydrogen sulfide comprising:

providing a solution comprising hydrogen sulfide, wherein the solution is disposed in a vessel;

adding sodium nitrite to the solution comprising hydrogen sulfide; and

adding a pH buffer to the solution to maintain a pH of the solution between about 7.0 to about 9.0, wherein the pH buffer removes free ammonia from the solution.

10. The method of claim 9 , wherein the concentration of hydrogen sulfide in the solution is about 2,000 mg/liter to about 25,000 mg/liter.

11. The method of claim 9 , wherein the sodium nitrite is added at a weight ratio to the hydrogen sulfide from about 0.676:1 to about 5:1.

12. The method of claim 9 , wherein the pH buffer comprises an acidic buffering chemical.

13. The method of claim 9 , wherein the solution further comprises water.

14. The method of claim 9 , wherein a reaction between the hydrogen sulfide and the sodium nitrite produces ammonia in the vessel.

15. The method of claim 9 , further comprising introducing a gas into the vessel.

16. The method of claim 15 , wherein the gas is nitrogen.

17. The method of claim 15 , wherein the gas is air.

18. The method of claim 15 , wherein the introducing of the gas into the vessel removes ammonia.

Assignments (4)
MERGER Recorded Mar 15, 2025
From: CR3 ZYMEFLOW, INC.
To: ZYMEFLOW, INC.
Reel/Frame 070523/0169 →
MERGER Recorded Mar 13, 2025
From: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
To: CR3 ZYMEFLOW, INC.
Reel/Frame 070508/0396 →
MERGER Recorded Mar 12, 2025
From: UNITED LABORATORIES INTERNATIONAL, LLC
To: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
Reel/Frame 070491/0243 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 28, 2020
From: FROST, JACK G.; SNYDER, KENNETH J., JR.
To: UNITED LABORATORIES INTERNATIONAL, LLC
Reel/Frame 052779/0243 →
Continuity (4)
Continuation 15623112 · Jun 14, 2017
Continuation 14197034 · Mar 4, 2014
Continuation 12415283 · Mar 31, 2009
Related Publication 20180354825A1 · Dec 13, 2018
Cited By (1)
US 12,391,588