IP Library Granted Patent US 11,049,628
Granted Patent B2
US 11,049,628 · App. 16/166,441 · Granted Jun 29, 2021

Target unit with ceramic capsule for producing cu-67 radioisotope

Inventors: David A. Ehst (Downers Grove, IL); James L. Willit (Batavia, IL)
Assignee: UCHICAGO ARGONNE, LLC
G21K5/08B01D7/00G21G1/001G21G1/12H05H6/00G21G2001/0094
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Quick Facts
Patent No.
US 11,049,628
App. No.
16/166,441
Granted
Jun 29, 2021
Kind
B2
Abstract

A target unit for producing Cu67 radioisotope is described herein, and comprises a cage body releasably coupled to a screw-on cap; and a ceramic capsule containing a solid Zn68 target ingot and having one open end and one closed end and defining an interior chamber for the target ingot. The ceramic capsule is releasably contained between the cage body and the screw-on cap with a lid disposed on the open end of the capsule and a washer positioned between the lid and the screw-on cap. The screw-on cap and the washer provide a water-tight seal between the lid and the capsule. The interior of the capsule is in intimate physical contact with the target ingot; and the Zn68 of the target ingot is free of traces of residual oxygen that interfere with contact of the Zn68 to the capsule.

Claims (24)

1. A target unit for producing Cu67 radioisotope comprising:

a cage body releasably coupled to a screw-on cap; and

a ceramic capsule containing a solid Zn68 target ingot and having one open end and one closed end and defining an interior chamber for the target ingot;

wherein the ceramic capsule is releasably contained between the cage body and the screw-on cap with a lid disposed on the open end of the capsule and a washer positioned between the lid and the screw-on cap, wherein the screw-on cap and the washer provide a water-tight seal between the lid and the capsule; the interior of the ceramic capsule is in intimate physical contact with the solid Zn68 target ingot; and the Zn68 of the target ingot is free of traces of residual oxygen that interfere with contact of the Zn68 to the capsule.

2. The target unit of claim 1 , wherein the cage body and the screw-on cap are composed of aluminum.

3. The target unit of claim 1 , wherein the cage body and the screw-on cap are composed of different alloys of aluminum to minimize the possibility of thread galling.

4. The target unit of claim 1 , wherein the cage body and the screw-on cap are each composed of different alloys of aluminum selected from the group consisting of 6061 Al and 2024 Al.

5. The target unit of claim 1 , wherein the cage body includes apertures to allow cooling water to contact the capsule during irradiation thereof to prevent melting or partial melting of the zinc target ingot during the irradiation.

6. The target unit of claim 1 , wherein the ceramic capsule is composed of a material selected from the group consisting of alumina and aluminum nitride.

7. The target unit of claim 1 , wherein the capsule is composed of alumina.

8. A target unit for producing Cu67 radioisotope comprising:

a cylindrical cage body with a threaded open end;

a screw-on cap threaded to mate with the threaded open end of the cage body;

a ceramic capsule having one open end and one closed end, and defining an interior chamber containing a Zn68 target ingot in intimate physical contact with the capsule;

a removable lid covering the open end of the capsule; and

a gasket disposed between the open end of the capsule and the lid;

wherein the ceramic capsule, the lid, and the gasket are arranged within the interior cavity of the cage body with the lid in contact with the screw-on cap when the cage body is mated with the screw-on cap, so that the screw-on cap applies a pressure on the lid and gasket sufficient to form a water-tight seal over the open end of the capsule when the unit is fully assembled for use; and the Zn68 of the target ingot is free of traces of residual oxygen that interfere with contact of the Zn68 to the capsule.

9. The target unit of claim 8 , wherein the cage body and the screw-on cap are composed of aluminum.

10. The target unit of claim 8 , wherein the cage body and the screw-on cap are composed of different alloys of aluminum to minimize the possibility of thread galling.

11. The target unit of claim 8 , wherein the cage body and the screw-on cap are each composed of different alloys of aluminum selected from the group consisting of 6061 Al and 2024 Al.

12. The target unit of claim 8 , wherein the cage body includes apertures to allow cooling water to contact the capsule during irradiation thereof to prevent melting or partial melting of the zinc target ingot during the irradiation.

13. The target unit of claim 8 , wherein the ceramic capsule is composed of a material selected from the group consisting of alumina and aluminum nitride.

14. The target unit of claim 8 , wherein the capsule is composed of alumina.

15. The target unit of claim 8 wherein the gasket is composed of graphite.

Assignments (2)
CONFIRMATORY LICENSE Recorded Jun 21, 2022
From: UCHICAGO ARGONNE, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 060260/0496 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 23, 2018
From: EHST, DAVID A.; WILLIT, JAMES L.
To: UCHICAGO ARGONNE, LLC
Reel/Frame 047281/0616 →
Continuity (4)
Division 15087111 · Mar 31, 2016
Continuation 13399082 · Feb 17, 2012
Provisional Application 61540897 · Sep 29, 2011
Related Publication 20190057791A1 · Feb 21, 2019
Cited By (3)
US 12,340,917 US 12,527,885 US 12,622,984