IP Library Granted Patent US 11,213,927
Granted Patent B2
US 11,213,927 · App. 16/233,943 · Granted Jan 4, 2022

CMP polishing pad conditioner

Inventors: Rajiv K. Singh (Newberry, FL); Deepika Singh (Newberry, FL)
Assignee: ENTREGIS, INC.
B24B53/017B24B37/04B24B37/042B24B37/044B24B53/013B24B53/047B24B53/12
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Quick Facts
Patent No.
US 11,213,927
App. No.
16/233,943
Granted
Jan 4, 2022
Kind
B2
Abstract

A method of processing chemical mechanical polishing (CMP) pad conditioners includes providing the CMP pad conditioner including conditioner substrate that is a metal, ceramic or a metal-ceramic material with a plurality of hard conditioner particles with a Vickers hardness greater than 3,000 Kg/mm 2 bonded to a top surface of the conditioner substrate, and a slurry including an aqueous medium and a plurality of hard slurry particles having a hardness greater than 3,000 Kg/mm 2 . The surface of the pad conditioner is polished in a CMP apparatus using a polishing pad. After the polishing each conditioner particle has at least one exposed facet, and the plurality of hard conditioner particles have a maximum average protrusion-to-protrusion flatness (PPF) difference of 20 microns, and a sharpest edge measured by a value of a cutting edge radius (CER) that lies at an edge of the facet for at least 80% of the facets.

Claims (12)

1. A method of processing a chemical mechanical polishing (CMP) pad conditioner, comprising:

providing said CMP pad conditioner comprising a conditioner substrate including a metal, ceramic or a metal-ceramic material having a patterned surface with a polycrystalline diamond film thereon, and a slurry including an aqueous medium and a plurality of hard slurry particles having a Vickers hardness greater than 3,000 Kg/mm 2 , and

polishing said polycrystalline diamond film in a CMP apparatus using a polishing pad and the slurry,

wherein said polycrystalline diamond film after said polishing includes tallest grains having a height lying in a top 20 percent of a peak-valley range, with at least 80 percent of said tallest grains having an orientation within 20 degrees from a (111) orientation.

2. The method of claim 1 , wherein said plurality of hard slurry particles comprise diamond particles.

3. The method of claim 2 , when an average size of said diamond particles range from 10 micron to 200 microns.

4. The method of claim 2 , wherein a concentration of said diamond particles in said slurry is between 1% and 20% by weight.

5. The method of claim 1 , wherein said polishing pad comprises a metal or a ceramic material with a Vickers hardness greater than 50 kg/m 2 .

6. The method of claim 1 , wherein said polishing pad comprises copper, steel, or a metal alloy including at least two metals.

7. The method in claim 1 , when a viscosity of said slurry ranges from 2 centipoise to 1,500 centipoise.

8. The method of claim 2 , further comprising secondary particles selected from alumina, or silica, with a Vickers hardness less than 3,000 Kg/mm 2 with a size between 10 nm to 10 micron, and a concentration between 1% to 60 weight percent.

9. The method of claim 8 , wherein said plurality of hard slurry particles comprise diamond particles, and wherein a size of said secondary particles is at least 30 percent smaller than a size of said diamond particles.

Assignments (5)
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 060614/0980 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 14, 2020
From: SINMAT, INC.
To: ENTEGRIS, INC.
Reel/Frame 052388/0520 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 27, 2018
From: SINGH, DEEPIKA
To: SINMAT, INC.
Reel/Frame 047862/0043 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 27, 2018
From: SINGH, RAJIV K.
To: UNIVERSITY OF FLORIDA RESEARCH FOUNDATION, INC.
Reel/Frame 047862/0123 →
Continuity (2)
Provisional Application 62611317 · Dec 28, 2017
Related Publication 20190202028A1 · Jul 4, 2019