IP Library › Granted Patent US 10,879,035
Granted Patent B2
US 10,879,035 · App. 16/254,965 · Granted Dec 29, 2020

Scanning electron microscope and measurement method for obtaining images of a specimen using an ion beam and an electron beam

Inventors: Noriaki Mizuno (Tokyo, JP); Toshikatsu Kaneyama (Tokyo, JP)
Assignee: JEOL Ltd.
H01J37/222H01J37/28H01J37/3056H01J37/31G01N2001/2873H01J2237/24475H01J2237/24485H01J2237/2804H01J2237/2807
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Quick Facts
Patent No.
US 10,879,035
App. No.
16/254,965
Granted
Dec 29, 2020
Kind
B2
Abstract

A scanning electron microscope includes an FIB column, an SEM column, and a control unit which controls the FIB column and the SEM column. The control unit performs: processing to control the FIB column so that a cross-section of a specimen S is repeatedly exposed at predetermined intervals; processing to perform a first measurement to acquire a first image by irradiating a cross-section of the specimen S with an electron beam each time when a cross-section of the specimen S is exposed; and processing to perform a second measurement to acquire a second image by irradiating a cross-section of the specimen S with an electron beam each time when a cross-section of the specimen S is exposed n times (n is an integer of 2 or more).

Claims (45)

1. A scanning electron microscope comprising:

an ion beam column that irradiates a specimen with an ion beam;

an electron beam column that irradiates the specimen with an electron beam;

a first detector that detects a first signal from the specimen;

a first image generation unit that generates a first image based on a detection signal from the first detector;

a second detector that detects a second signal from the specimen;

a second image generation unit that generates a second image based on a detection signal from the second detector; and

a control unit that controls the ion beam column and the electron beam column,

the control unit performing:

processing to control the ion beam column to cause the specimen to be repeatedly sliced to a predetermined thickness by an ion beam;

processing to perform a first measurement to acquire the first image based on the detection signal from the first detector by irradiating a cross-section of the specimen with the electron beam each time when the specimen is sliced by the ion beam;

processing to perform a second measurement to acquire the second image based on the detection signal from the second detector by irradiating the cross-section of the specimen with the electron beam each time only when the specimen is sliced n times, wherein n is an integer of 2 or more;

wherein a spatial resolution of the first measurement is higher than a spatial resolution of the second measurement; and

wherein measurement conditions of the second measurement to acquire the second image are determined based on:

a difference of the spatial resolution of the first measurement and the spatial resolution of the second measurement; and

a difference of a measurement time of the first measurement and a measurement time of the second measurement.

2. The scanning electron microscope according to claim 1 , further comprising:

an input unit that receives input of an interval of performing the first measurement and input of an interval of performing the second measurement,

wherein the control unit sets the predetermined thickness based on the interval of performing the first measurement, and sets the n based on the interval of performing the second measurement.

3. The scanning electron microscope according to claim 1 , wherein

the control unit sets the predetermined thickness based on a size of an imaging region of the first image and a number of pixels of the first image, and

the control unit sets the n based on a size of an imaging region of the second image and a number of pixels of the second image.

4. The scanning electron microscope according to claim 1 , wherein

in the first measurement, a scanning electron microscope image is acquired by detecting electrons emitted from the specimen, and

in the second measurement, an energy dispersive X-ray spectrometry (EDS) mapping image is acquired by detecting X-rays emitted from the specimen.

5. The scanning electron microscope according to claim 1 , wherein

in the first measurement, a scanning electron microscope image is acquired by detecting electrons emitted from the specimen, and

in the second measurement, an electron back scatter diffraction pattern (EBSD) mapping image is acquired by detecting reflected electrons reflected from the specimen.

6. A measurement method comprising:

slicing a specimen repeatedly to a predetermined thickness;

performing a first measurement to acquire a first image based on a detection signal from a first detector by irradiating a cross-section of the specimen with an electron beam each time when the specimen is sliced; and

performing a second measurement to acquire a second image based on a detection signal from a second detector by irradiating the cross-section of the specimen with the electron beam each time only when the specimen is sliced n times, wherein n is an integer of 2 or more,

wherein a spatial resolution of the first measurement is higher than a spatial resolution of the second measurement; and

wherein measurement conditions of the second measurement to acquire the second image are determined based on:

a difference of the spatial resolution of the first measurement and the spatial resolution of the second measurement; and

a difference of a measurement time of the first measurement and a measurement time of the second measurement.

7. The measurement method according to claim 6 , further comprising:

setting the predetermined thickness based on a size of an imaging region of the first image and a number of pixels of the first image; and

setting the n based on a size of an imaging region of the second image and a number of pixels of the second image.

8. The measurement method according to claim 6 , wherein

in the first measurement, a scanning electron microscope image is acquired by detecting electrons emitted from the specimen, and

in the second measurement, an energy dispersive X-ray spectrometry (EDS) mapping image is acquired by detecting X-rays emitted from the specimen.

9. The measurement method according to claim 6 , wherein

in the first measurement, a scanning electron microscope image is acquired by detecting electrons emitted from the specimen, and

in the second measurement, an electron back scatter diffraction pattern (EBSD) mapping image is acquired by detecting reflected electrons reflected from the specimen.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 23, 2019
From: MIZUNO, NORIAKI; KANEYAMA, TOSHIKATSU
To: JEOL LTD.
Reel/Frame 048107/0964 →
Priority Claims (1)
JP 2018-009998 · Jan 24, 2018 · national
Continuity (1)
Related Publication 20190228948A1 · Jul 25, 2019
Cited By (2)
US 12,500,061 US 12,548,734