IP Library Granted Patent US 11,479,375
Granted Patent B2
US 11,479,375 · App. 16/496,128 · Granted Oct 25, 2022

Method of encapsulating liquid products

Inventors: Pierre-Yves Paslier (London, GB); Rodrigo Garcia González (London, GB)
Assignee: NOTPLA LIMITED
B65B3/02A23P20/10B65B9/24B65B61/06B65D65/463B65D65/466
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Quick Facts
Patent No.
US 11,479,375
App. No.
16/496,128
Granted
Oct 25, 2022
Kind
B2
Abstract

The invention relates to a method for encapsulating a liquid product, the method comprising blending together a solution of alginate and a thickener and extruding through an appropriately shaped die to form a membrane, applying a calcium rich ion solution to crosslink the membrane and create a water insoluble membrane, filling the water insoluble membrane with the liquid product; and sealing the membrane around the liquid product, encapsulating the liquid product therein.

Claims (24)

1. A method for encapsulating a liquid product having a viscosity of less than 20000 cP (measured at 20° C. and a shear rate of 10 s −1 ), the method comprising:

blending together a solution of alginate and a thickener and extruding through an appropriately shaped die to form a membrane;

applying a calcium rich ion solution to crosslink the membrane and create a water insoluble membrane;

filling the water insoluble membrane with the liquid product having a viscosity of less than 20000 cP (measured at 20° C. and a shear rate of 10 s −1 ); and

sealing the membrane around the liquid product through a pinch process, encapsulating the liquid product therein, wherein

the pinch process comprises pinching the membrane while crosslinking propagates through the membrane to provide a liquid-tight flat seal in the absence of heat.

2. The method of claim 1 wherein the blending occurs at room temperature.

3. The method of claim 1 , wherein the pinch process further comprises: pinching the membrane at predetermined intervals therealong to individually seal and form a plurality of liquid-based products in series.

4. The method of claim 3 , wherein the method further comprises:

cutting at each seal to separate the products or cutting at predetermined intervals within the series to form distinct chains of encapsulated products.

5. The method of claim 1 , wherein the encapsulated product is rinsed and dried.

6. The method of claim 1 , wherein the solution of alginate is 1-10% alginate.

7. The method of claim 1 , wherein the thickener is xanthan or cellulose gum.

8. The method of claim 1 , wherein the solution of alginate and the thickener is blended with a further plasticizing additive.

9. The method of claim 1 , wherein the calcium rich ion solution has a concentration of 1 to 10%.

10. The method of claim 1 , further comprising an additional pre-step of treating the product with a solution of 0.5 to 10% calcium ions, prior to filling the membrane with the product.

11. The method of claim 1 , further comprising undertaking a membrane reinforcement step in which the encapsulated product is heated to at least 40 degrees C.

12. The method of claim 1 , further comprising undertaking a membrane reinforcement step in which the encapsulated product is heated to at least 80 degrees C.

13. The method of claim 1 , further comprising undertaking a membrane reinforcement step in which the encapsulated product is compressed under a load of 100N or more.

14. The method of claim 1 , further comprising the step of applying a brand, identification or label onto the membrane.

15. The method of claim 1 , wherein the method further comprises:

applying a secondary temporary layer to the membrane of the encapsulated product.

16. The method of claim 15 , wherein the secondary layer is a cross-linked alginate membrane.

17. The method of claim 15 wherein the membrane and the secondary layer are distinguishable from one another by a preformed label or color applied to the membrane and/or to the secondary layer.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 26, 2020
From: PASLIER, PIERRE-YVES; GONZALEZ, RODRIGO GARCIA
To: SKIPPING ROCKS LAB LIMITED
Reel/Frame 052236/0606 →
CHANGE OF NAME Recorded Mar 26, 2020
From: SKIPPING ROCKS LAB LIMITED
To: NOTPLA LIMITED
Reel/Frame 052237/0144 →
Priority Claims (1)
GB 1704547 · Mar 22, 2017 · national
Continuity (1)
Related Publication 20200047927A1 · Feb 13, 2020
Cited By (2)
US 12,286,524 US 12,398,516