IP Library Granted Patent US 11,168,377
Granted Patent B2
US 11,168,377 · App. 16/525,473 · Granted Nov 9, 2021

Processes for producing continuous bulk forms of iron-silicon alloys and bulk forms produced thereby

Inventors: Andrew Benjamin Kustas (Albuquerque, NM); Dinakur Sagapuram (Bryan, TX); Kevin Paul Trumble (West Lafayette, IN); Srinivasan Chandrasekar (West Lafayette, IN)
Assignee: Purdue Research Foundation
C21D9/46C21D6/008C21D8/02C21D8/0226C21D8/0273C22C38/002C22C38/02C22C38/04C22C38/06
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Quick Facts
Patent No.
US 11,168,377
App. No.
16/525,473
Granted
Nov 9, 2021
Kind
B2
Abstract

Processes for producing continuous bulk forms of iron-silicon alloys and bulk forms produced thereby. Such a bulk form is continuous in a longitudinal direction thereof and has a continuous cross-sectional form transverse to the longitudinal direction. The bulk form is formed of an Fe—Si alloy and has a crystallographic texture that comprises <111> and {110} fibers that are inclined relative to the longitudinal direction. The bulk form may be produced by a process that includes deforming a solid body formed of an Fe—Si alloy with a cutting tool in a single step to continuously produce a continuous bulk form from material obtained from the solid body.

Claims (24)

1. A bulk form that is a sheet or strip product that has a first direction and has a cross-sectional form transverse to the first direction, the bulk form being formed of an Fe—Si alloy and having a crystallographic texture that comprises <111> and {110} fiber axes that are inclined relative to the first direction.

2. The bulk form of claim 1 , wherein the Fe—Si alloy has a Si content of greater than 3.5 wt. %.

3. The bulk form of claim 1 , wherein the Fe—Si alloy has a Si content of between 4.5 wt. % and 8.5 wt. %.

4. The bulk form of claim 1 , wherein the bulk form was produced by deforming a casting.

5. The bulk form of claim 1 , wherein the product has opposite surfaces parallel to the first direction and the fiber axes are inclined relative to the opposite surfaces.

6. The bulk form of claim 1 , wherein the <111> and {110} fiber axes have a degree of inclination from 0° to 80°.

7. The bulk form of claim 1 , wherein the bulk form has a recrystallized microstructure.

8. The bulk form of claim 1 , wherein the bulk form has a shear texture characterized by an inclination that varies in a thickness direction of the bulk form that is transverse to the first direction.

9. The bulk form of claim 1 , wherein the product is a sheet.

10. The bulk form of claim 1 , wherein the product is a strip.

11. The bulk form of claim 1 , wherein the Fe—Si alloy contains at least one of manganese, phosphorous, sulfur, and aluminum.

12. A process of producing the bulk form of claim 1 , the process comprising:

deforming a solid body formed of the Fe—Si alloy with a cutting tool in a single step to continuously produce the bulk form from material obtained from the solid body.

13. The process of claim 12 , wherein the Fe—Si alloy has a Si content of greater than 3.5 wt. %.

14. The process of claim 12 , wherein the product has opposite surfaces parallel to the first direction and the bulk form travels in the first direction during the deforming step.

15. The process of claim 12 , wherein the <111> and {110} fiber axes have a degree of inclination from 0° to 80°.

16. The process of claim 12 , wherein the bulk form has a recrystallized microstructure as a result of the deforming step.

17. The process of claim 12 , wherein the bulk form comprises a primary shear zone and a secondary shear zone as a result of the deforming step, the process further comprising performing a thermal treatment on the bulk form to preferentially grow grains in the secondary shear zone relative to grains in the primary shear zone.

18. The process of claim 12 , further comprising selectively enhancing frictional shear deformation at an interface between the cutting tool and the bulk form to create a shear texture characterized by an inclination that varies in a thickness direction of the bulk form that is transverse to the first direction.

19. The process of claim 12 , further comprising controlling a degree of inclination of the <111> and {110} fiber axes by controlling a localized deformation temperature, wherein the localized deformation temperature is controlled by controlling:

a deformation velocity (V 0 );

a preheating temperature of the solid body; and

a deformation thickness ratio (λ) equal to t c /t o , where t c is a thickness of the bulk form and t o is the depth of cut of the cutting tool.

20. The process of claim 12 , further comprising installing the bulk form in an electric motor or a power distribution transformer.

Assignments (1)
CONFIRMATORY LICENSE Recorded Oct 2, 2019
From: PURDUE UNIVERSITY
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 050611/0766 →
Continuity (3)
Division 15247322 · Aug 25, 2016
Provisional Application 62209719 · Aug 25, 2015
Related Publication 20190352733A1 · Nov 21, 2019