IP Library › Granted Patent US 11,428,681
Granted Patent B2
US 11,428,681 · App. 16/673,893 · Granted Aug 30, 2022

Gas sensors based upon metal carbon complexes

Inventors: Timothy M. Swager (Newton, MA); Sophie Liu (Cambridge, MA); Graham Sazama (Chestnut Hill, MA); Alexander R. Petty (Allston, MA); Jan M. Schnorr (Boston, MA)
Assignee: Massachusetts Institute of Technology
G01N33/0047G01N27/127Y10T436/21Y10T436/216
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Quick Facts
Patent No.
US 11,428,681
App. No.
16/673,893
Granted
Aug 30, 2022
Kind
B2
Abstract

A sensor can include a conductive region in electrical communication with at least two electrodes, the conductive region including a conductive material and an alkene-interacting metal complex.

Claims (19)

1. A sensor comprising:

a conductive region including a carbon nanotube in electrical communication with at least two electrodes, the conductive region including a conductive material and an alkene-interacting metal complex, wherein the alkene-interacting metal complex includes a metal macrocycle complex including a non-coordinating anion capable of forming a stable complex by reaction with an alkene and reacts with the alkene to produce a chemiresistive response in the conductive region.

2. The sensor of claim 1 , wherein the conductive material includes graphite.

3. The sensor of claim 1 , wherein the conductive material includes graphene.

4. The sensor of claim 1 , wherein the conductive material is the alkene-interacting metal complex.

5. The sensor of claim 1 , wherein the conductive material includes a conductive polymer.

6. The sensor of claim 1 , wherein the conductive material includes a metal oxide.

7. The sensor of claim 1 , wherein the conductive material includes an inorganic semiconductor.

8. The sensor of claim 1 , wherein the macrocycle complex includes a phthalocyanine.

9. The sensor of claim 1 , wherein the macrocycle complex includes a porphyrin.

10. The sensor of claim 1 , wherein the metal of the macrocycle complex includes Mn, Re, Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pd, Cu, Ag, Au, or Hg.

11. The sensor of claim 1 , wherein the metal of the macrocycle complex includes a cobalt ion.

12. The sensor of claim 1 , wherein the metal of the macrocycle complex includes an iridium ion.

13. The sensor of claim 1 , wherein the metal macrocycle complex includes a 5, 10, 15, 20-tetraphenylporphyrinato cobalt.

14. The sensor of claim 1 , wherein the metal macrocycle complex includes a 5, 10, 15, 20-tetrakis(pentafluorophenyl)porphyrinato cobalt.

15. The sensor of claim 1 , wherein the anion includes Cl − , ClO 4 − , BF 4 − , RSO 3 − where R is CF 3 , CH 3 , an aryl, an alkyl, or an oxygen bound arylor alkyl group, PF 6 − , or BAr 4 − , where Ar is an aromatic group.

16. The sensor of claim 1 , wherein the alkene-interacting metal complex includes a palladium ion.

17. The sensor of claim 1 , wherein the alkene-interacting metal complex includes palladium(II) trifluoroacetate or palladium(II) acetate.

18. The sensor of claim 1 , wherein the alkene-interacting metal complex further reacts to regenerate the metal complex that reacts with an additional alkene.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 7, 2020
From: SWAGER, TIMOTHY M.; LIU, SOPHIE; SAZAMA, GRAHAM; PETTY, ALEXANDER R.; SCHNORR, JAN M.
To: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Reel/Frame 051430/0275 →
Continuity (3)
Continuation 14635995 · Mar 2, 2015
Provisional Application 61946872 · Mar 2, 2014
Related Publication 20200225201A1 · Jul 16, 2020