IP Library › Granted Patent US 11,598,015
Granted Patent B2
US 11,598,015 · App. 17/050,750 · Granted Mar 7, 2023

Fabrication of dendritic structures and tags

Inventors: Michael N. Kozicki (Phoenix, AZ); Yago Gonzalez Velo (Tempe, AZ); Smitha Swain (Tempe, AZ)
Assignee: Arizona Board of Regents on behalf of Arizona State University
C25D3/38A61K9/4891C25D3/46C25D5/48C25D5/605C25D7/00
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Quick Facts
Patent No.
US 11,598,015
App. No.
17/050,750
Granted
Mar 7, 2023
Kind
B2
Abstract

Methods for fabricating dendritic structures and tags include introducing an electrolyte material onto a substrate, into a substrate, or both onto and into a substrate, and applying an electrical potential to at least one pair of electrodes positioned on the substrate to form one or more dendritic structures on the substrate.

Claims (23)

1. A method of forming dendritic structures, the method comprising:

printing an electrically conductive ink on a substrate to form a multiplicity of pairs of electrodes on the substrate;

curing the multiplicity of pairs of electrodes;

immersing the substrate into an electrolytic solution;

applying an electrical potential to the multiplicity of pairs of electrodes to form a multiplicity of dendritic structures on the substrate;

passing the substrate through a rinse bath to remove excess electrolyte;

passing the substrate through a fixing bath to chemically deactivate residual electrolyte material in or on the substrate;

drying the multiplicity of dendritic structures;

oxidizing the multiplicity of dendritic structures;

applying a coating material to the multiplicity of dendritic structures; and

cutting the substrate to yield a multiplicity of substrate pieces, each substrate piece comprising one or more of the multiplicity of dendritic structures.

2. The method of claim 1 , wherein the substrate comprises one or more materials selected from the group consisting of synthetic and non-synthetic paper and card materials, polyethylene, polypropylene, polyester, polystyrene, polyamide, polyolefin, acetate, cellulose acetate, acrylate, vinyl, polyester, and polyethylene terephthalate.

3. The method of claim 1 , wherein the substrate comprises a first structural material and a second adsorbent material.

4. The method of claim 3 , wherein the first structural material comprises at least one of a polymeric material, a paper material, and a cloth material.

5. The method of claim 3 , wherein the second adsorbent material comprises silica.

6. The method of claim 3 , wherein the second adsorbent material is positioned at least partially within a body of the first structural material.

7. The method of claim 3 , wherein the second adsorbent material comprises a gel.

8. The method of claim 1 , wherein the electrical potential is applied to the multiplicity of pairs of electrodes for a period of between 1 second and 30 seconds.

9. The method of claim 1 , wherein each dendritic structure of the multiplicity of dendritic structures is formed between a pair of multiplicity of pairs of electrodes, and a potential difference between the electrodes in each pair of electrodes is between 2 volts and 20 volts.

10. The method of claim 1 , wherein the fixing bath comprises a thiosulfate-based fixing solution.

11. The method of claim 10 , wherein the fixing solution comprises sodium thiosulfate or ammonium thiosulfate.

12. The method of claim 1 , wherein oxidizing the dendritic structures comprises heating the multiplicity of dendritic structures to a temperature of between 90 degrees C. and 100 degrees C.

13. The method of claim 1 , wherein the coating material comprises at least one material selected from the group consisting of cyanoacrylate, polymethylmethacrylate, polyethylene terephthalate, polysiloxane, silicon dioxide, silicon nitride, polyvinylchloride, and cellulose acetate.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 1, 2020
From: KOZICKI, MICHAEL N.; VELO, YAGO GONZALEZ; SWAIN, SMITHA
To: ARIZONA BOARD OF REGENTS ON BEHALF OF ARIZONA STATE UNIVERSITY
Reel/Frame 054505/0900 →
Continuity (2)
Provisional Application 62662979 · Apr 26, 2018
Related Publication 20210230763A1 · Jul 29, 2021
Cited By (3)
US 12,307,323 US 12,447,767 US 12,552,195