IP Library Granted Patent US 11,843,070
Granted Patent B2
US 11,843,070 · App. 17/111,843 · Granted Dec 12, 2023

Photovoltaic devices including doped semiconductor films

Inventors: Anke Abken (Port Hueneme, CA); Markus Gloeckler (Perrysburg, OH); Roger T. Green (St. Charles, MO); Akhlesh Gupta (Sylvania, OH); Upali Jayamaha (Perrysburg, OH); Peter Meyers (Christiansted, VI); Rick C. Powell (Ann Arbor, MI)
Assignee: First Solar, Inc.
H01L31/1828H01L31/02963H01L31/02966H01L31/03042H01L31/073H01L31/18H01L31/1832H01L31/1864H01L31/022466H01L31/1868H01L31/1884Y02E10/50Y02E10/543Y02E10/544Y02P70/50
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,843,070
App. No.
17/111,843
Granted
Dec 12, 2023
Kind
B2
Abstract

A photovoltaic cell can include a dopant in contact with a semiconductor layer.

Claims (38)

1. A method for forming an absorber layer of a photovoltaic cell comprising:

depositing the absorber layer, wherein:

the absorber layer comprises a mixture of CdTe and at least one semiconductor selected from the group consisting of ZnO, ZnS, ZnSe, ZnTe, CdO, CdS, CdSe, MgO, MgS, MgSe, MgTe, HgO, HgS, HgSe, HgTe, MnO, MnS, MnTe, AN, AlP, AlAs, AlSb, GaN, GaP, GaAs, GaSb, InN, InP, InAs, InSb, TlN, TlP, TlAs, and TlSb; and

the absorber layer comprises a Group V dopant;

applying a flux solution to a surface of the absorber layer, wherein the flux solution comprises a chloride compound, and a Group I element;

heat treating the absorber layer with the flux solution, whereby the Group I element is distributed within the absorber layer.

2. The method of claim 1 , wherein the Group I element comprises copper (Cu).

3. The method of claim 1 , wherein the Group I element comprises silver (Ag).

4. The method of claim 1 , wherein the Group I element comprises gold (Au).

5. The method of claim 1 , wherein the Group I element comprises at least one of lithium (Li), sodium (Na), potassium (K), rubidium (Rb), or cesium (Cs).

6. The method of claim 1 , wherein the Group I element comprises at least one of: sodium (Na), potassium (K), or rubidium (Rb).

7. The method of claim 1 , wherein the Group V dopant comprises nitrogen (N).

8. The method of claim 1 , wherein the Group V dopant comprises phosphorus (P).

9. The method of claim 1 , wherein the Group V dopant comprises arsenic (As).

10. The method of claim 1 , wherein the Group V dopant comprises antimony (Sb).

11. The method of claim 1 , wherein the Group V dopant comprises bismuth (Bi).

12. The method of claim 1 , wherein the absorber layer comprises a mixture of CdTe and CdSe.

13. The method of claim 1 , wherein the absorber layer comprises a mixture of CdTe and ZnTe.

14. The method of claim 1 , wherein a concentration of the Group V dopant in the absorber layer is between 0.5 ppma to 500 ppma.

15. The method of claim 1 , wherein the chloride compound comprises cadmium chloride (CdCl 2 ), and wherein the flux solution further comprises a chloride of the Group I element.

16. The method of claim 1 , comprising: depositing a top layer over the semiconductor absorber layer, wherein the top layer comprises a metal nitride, and wherein the metal nitride, includes at least one of: aluminum, molybdenum, chromium, cobalt, nickel, titanium, or tungsten.

17. A method for forming an absorber layer of a photovoltaic cell comprising:

depositing the absorber layer, wherein depositing the absorber layer comprises:

vaporizing a source material to form a semiconductor vapor with a vapor transport deposition system having a distributor;

distributing the semiconductor vapor via the distributor to a deposition chamber, wherein the semiconductor vapor comprises Cd and Te;

applying excess Cd or Te to the semiconductor vapor, whereby:

the vapor is off-stoichiometric compared to CdTe,

a vapor phase overpressure of Cd or Te is introduced to the semiconductor vapor, and

the absorber layer comprises a mixture of CdTe and at least one semiconductor selected from the group consisting of ZnO, ZnS, ZnSe, ZnTe, CdO, CdS, CdSe, MgO, MgS, MgSe, MgTe, HgO, HgS, HgSe, HgTe, MnO, MnS, MnTe, AN, AlP, AlAs, AlSb, GaN, GaP, GaAs, GaSb, InN, InP, InAs, InSb, TlN, TlP, TlAs, and TlSb; and

introducing a Group V dopant into the absorber layer;

applying a flux solution to a surface of the absorber layer, wherein the flux solution comprises a chloride compound, and a Group I element; and

heat treating the absorber layer with the flux solution.

18. The method of claim 1 , wherein the Group V dopant is introduced by a vapor.

19. The method of claim 1 , wherein the Group V dopant is applied to a surface of the absorber layer prior to the step of heat treating the absorber layer with the flux solution.

20. A method for forming an absorber layer of a photovoltaic cell comprising:

depositing the absorber layer, wherein the absorber layer comprises a mixture of CdTe and CdSe, and wherein the absorber layer comprises a Group V dopant at a concentration between 0.5 ppma to 500 ppma;

applying a flux solution to a surface of the absorber layer, wherein the flux solution comprises CdCl 2 , and wherein the flux solution comprises a Group I element; and

heat treating the absorber layer with the flux solution.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Feb 13, 2026
From: JPMORGAN CHASE BANK, N.A.
To: FIRST SOLAR, INC.
Reel/Frame 074858/0364 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 9, 2023
From: POWELL, RICK C.; JAYAMAHA, UPALI; ABKEN, ANKE; GLOECKLER, MARKUS; GUPTA, AKHLESH; GREEN, ROGER T.; MEYERS, PETER
To: FIRST SOLAR, INC.
Reel/Frame 064536/0755 →
SECURITY INTEREST Recorded Jul 10, 2023
From: FIRST SOLAR, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 064237/0462 →
Continuity (5)
Division 16435838 · Jun 10, 2019
Continuation 14994830 · Jan 13, 2016
Division 12262424 · Oct 31, 2008
Provisional Application 60985019 · Nov 2, 2007
Related Publication 20210091250A1 · Mar 25, 2021
Cited By (5)
US 12,238,943 US 12,356,755 US 12,369,426 US 12,520,599 US 12,563,857