IP Library Granted Patent US 11,884,641
Granted Patent B2
US 11,884,641 · App. 17/263,141 · Granted Jan 30, 2024

Method for decomposing flavonoid glycoside and method for producing flavonoid

Inventors: Motohiro Arifuku (Tokyo, JP); Yoshiaki Kurihara (Tokyo, JP); Masato Kaneeda (Tokyo, JP)
Assignee: RESONAC CORPORATION
C07D311/40C07D311/30
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Quick Facts
Patent No.
US 11,884,641
App. No.
17/263,141
Granted
Jan 30, 2024
Kind
B2
Abstract

Provided is a method for decomposing a flavonoid glycoside, wherein a flavonoid glycoside-containing raw material is hydrothermally treated to decompose a flavonoid glycoside into a flavonoid.

Claims (21)

1. A method for decomposing flavonoid glycosides, comprising

performing a hydrothermal treatment on a raw material containing flavonoid glycosides to decompose the flavonoid glycosides into flavonoids,

wherein the flavonoid glycosides include sudachitin glycoside wherein the raw material is Citrus sudachi , and/or demethoxysudachitin glycoside, and

the hydrothermal treatment is performed under conditions of a temperature of 180° C. to 300° C. for 0.5 to 20 hours.

2. The method for decomposing flavonoid glycosides according to claim 1 ,

wherein the hydrothermal treatment is performed in a sealed container containing the raw material.

3. The method for decomposing flavonoid glycosides according to claim 2 ,

wherein the hydrothermal treatment is performed by heating a reaction solution containing the raw material and water in the sealed container.

4. The method for decomposing flavonoid glycosides according to claim 3 ,

wherein the content of the flavonoid glycosides in the reaction solution with respect to a total amount of the reaction solution is 0.01 to 3 mass %.

5. The method for decomposing flavonoid glycosides according to claim 3 ,

wherein the content of an inorganic acid in the reaction solution with respect to a total amount of the reaction solution is 1 mass % or less.

6. The method for decomposing flavonoid glycosides according to claim 2 ,

wherein the hydrothermal treatment is performed by supplying water vapor into the sealed container from the outside.

7. The method for decomposing flavonoid glycosides according to claim 1 ,

wherein the raw material further contains flavonoids.

8. The method for decomposing flavonoid glycosides according to claim 1 , wherein the raw material is a dry powder obtained from the pericarp of Citrus sudachi.

9. A method for producing flavonoids, comprising

a decomposition process in which the flavonoid glycosides are decomposed by the method for decomposing flavonoid glycosides according to claim 1 ; and

an extraction process in which flavonoids are extracted from a decomposition product obtained in the decomposition process.

10. The method for decomposing flavonoid glycosides according to claim 1 , wherein the hydrothermal treatment is performed under conditions of a temperature of 190° C. to 300° C. for 0.5 to 20 hours.

Assignments (3)
CHANGE OF ADDRESS Recorded Feb 9, 2024
From: RESONAC CORPORATION
To: RESONAC CORPORATION
Reel/Frame 066547/0677 →
CHANGE OF NAME Recorded Apr 23, 2023
From: SHOWA DENKO MATERIALS CO., LTD.
To: RESONAC CORPORATION
Reel/Frame 063410/0085 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 26, 2021
From: ARIFUKU, MOTOHIRO; KURIHARA, YOSHIAKI; KANEEDA, MASATO
To: SHOWA DENKO MATERIALS CO., LTD.
Reel/Frame 055025/0231 →