IP Library › Granted Patent US 12,232,522
Granted Patent B2
US 12,232,522 · App. 17/293,934 · Granted Feb 25, 2025

Method of generating an aerosol having protonated nicotine

Inventors: Connor Bruton (London, GB); Anna Azzopardi (London, GB); Peter Clayton (London, GB)
Assignee: NICOVENTURES TRADING LIMITED
A24F40/10A24B15/167A24F40/30A24F40/42
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Quick Facts
Patent No.
US 12,232,522
App. No.
17/293,934
Granted
Feb 25, 2025
Kind
B2
Abstract

A method of generating an aerosol comprising protonated nicotine, the method comprising the steps of: (i) providing a nicotine formulation comprising nicotine as free base; (ii) providing a carbon dioxide source capable of providing carbon dioxide in situ; (iii) vaporizing or aerosolizing the nicotine formulation; (iv) providing carbon dioxide from the carbon dioxide source, and (v) contacting the carbon dioxide with the vaporized or aerosolized nicotine formulation to thereby protonate nicotine free base and generate an aerosol comprising protonated nicotine.

Claims (21)

1. A method of generating an aerosol comprising protonated nicotine, the method comprising the steps of:

(i) providing a nicotine formulation comprising nicotine as a free base form;

(ii) providing a carbon dioxide source capable of providing carbon dioxide in situ;

(iii) vaporizing or aerosolizing the nicotine formulation;

(iv) providing carbon dioxide from the carbon dioxide source; and

(v) contacting the carbon dioxide with the vaporized or aerosolized nicotine formulation to thereby protonate nicotine free base and generate an aerosol comprising protonated nicotine;

wherein the nicotine formulation contains the carbon dioxide source.

2. The method according to claim 1 , wherein the nicotine formulation contains nicotine substantially in free base form.

3. The method according to claim 1 , wherein the nicotine formulation further comprises a carrier.

4. The method according to claim 3 , wherein the carrier is a solvent.

5. The method according to claim 4 , wherein the solvent is selected from glycerol, propylene glycol, 1,3-propane diol and mixtures thereof.

6. The method according to claim 1 , wherein the nicotine formulation further comprises water.

7. The method according to claim 1 , wherein the nicotine formulation comprises nicotine in an amount of no greater than 2 wt % based on the total weight of the formulation.

8. The method according to claim 1 , wherein the nicotine formulation comprises nicotine in an amount of no greater than 1.8 wt % based on the total weight of the formulation.

9. A nicotine delivery system comprising:

(i) a nicotine formulation comprising nicotine as a free base form; and

(ii) a carbon dioxide source that comprises carbon dioxide in the liquid or gas phase capable of providing carbon dioxide in situ to the nicotine formulation;

wherein the nicotine formulation contains the carbon dioxide source.

10. The nicotine delivery system according to claim 9 , wherein the carbon dioxide source comprises carbon dioxide in the gas phase.

11. The nicotine delivery system according to claim 9 , wherein the carbon dioxide source comprises carbon dioxide in the liquid phase.

12. The nicotine delivery system according to claim 9 , where the nicotine formulation further comprises a carrier that is a solvent selected from glycerol, propylene glycol, 1 , 3 -propane diol and mixtures thereof.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 28, 2022
From: AZZOPARDI, ANNA
To: BRITISH AMERICAN TOBACCO (INVESTMENTS) LIMITED
Reel/Frame 061239/0028 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 28, 2022
From: BRUTON, CONNOR
To: BRITISH AMERICAN TOBACCO (INVESTMENTS) LIMITED
Reel/Frame 061239/0214 →
Priority Claims (1)
GB 1818711 · Nov 16, 2018 · national
Continuity (1)
Related Publication 20220007715A1 · Jan 13, 2022
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