IP Library Granted Patent US 11,560,397
Granted Patent B2
US 11,560,397 · App. 17/370,722 · Granted Jan 24, 2023

Group VI precursor compounds

Inventors: David M. Ermert (Danbury, CT); Thomas H. Baum (New Fairfield, CT)
Assignee: ENTEGRIS, INC.
C07F11/005C23C16/405
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Quick Facts
Patent No.
US 11,560,397
App. No.
17/370,722
Granted
Jan 24, 2023
Kind
B2
Abstract

The invention provides a facile process for preparing various Group VI precursor compounds, set forth below as Formula (I), useful in the vapor deposition of certain Group VI metals onto solid substrates, especially microelectronic semiconductor device substrates. Also provided is a process for the preparation of such precursor compounds. Additionally, the invention provides a method for vapor deposition of Group VI metals onto microelectronic device substrates utilizing the precursor compounds of the invention.

Claims (12)

1. A compound of the Formula (I)

wherein M is chosen from molybdenum, chromium, and tungsten, X is chosen from fluoro, chloro, bromo, and iodo, and each L 1 and L 2 are dimethyl carbonate.

2. The compound of claim 1 , wherein M is molybdenum.

3. The compound of claim 1 , wherein M is chromium.

4. The compound of claim 1 , wherein M is tungsten.

5. A compound of the Formula (I)

wherein M is chosen from molybdenum, chromium, and tungsten, X is chosen from fluoro, chloro, bromo, and iodo, and each L 1 and L 2 are propylene carbonate.

6. The compound of claim 5 , wherein M is molybdenum.

7. The compound of claim 5 , wherein M is chromium.

8. The compound of claim 5 , wherein M is tungsten.

9. A compound of the Formula (I)

wherein M is chosen from molybdenum, chromium, and tungsten, X is chosen from fluoro, chloro, bromo, and iodo, and each L 1 and L 2 are the same and are chosen from C 1 -C 6 alkyl carbonates.

Assignments (3)
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.; CMC MATERIALS, INC.; INTERNATIONAL TEST SOLUTIONS, LLC; QED TECHNOLOGIES INTERNATIONAL, INC.
To: TRUIST BANK, AS NOTES COLLATERAL AGENT
Reel/Frame 060613/0072 →
SECURITY INTEREST Recorded Jul 8, 2022
From: ENTEGRIS, INC.; ENTEGRIS GP, INC.; POCO GRAPHITE, INC.
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 060614/0980 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 8, 2021
From: ERMERT, DAVID M.; BAUM, THOMAS H.
To: ENTEGRIS, INC.
Reel/Frame 056795/0691 →
Continuity (2)
Provisional Application 63049992 · Jul 9, 2020
Related Publication 20220009953A1 · Jan 13, 2022