IP Library › Granted Patent US 12,269,774
Granted Patent B2
US 12,269,774 · App. 17/505,892 · Granted Apr 8, 2025

Penetrating prime emulsion

Inventors: James Barnat (Tulsa, OK); Joel Coates (Tulsa, OK)
Assignee: ArrMaz Products Inc.
C04B26/26C04B24/123C09K17/34E01C7/36E01C19/16E01C21/00C04B2103/40C04B2111/00741C04B2111/0075E01C19/48
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Quick Facts
Patent No.
US 12,269,774
App. No.
17/505,892
Granted
Apr 8, 2025
Kind
B2
Abstract

A bituminous emulsion that is capable of being used as a penetrating prime emulsion. The penetrating prime emulsion may be capable of penetrating compacted soil without the use of solvent, and may toughen quickly to allow early application of a paved layer on the surface. The bituminous emulsion may comprise bituminous material and an emulsifier comprising octylphenol ethoxylates, and optionally further comprising tallow diamine betaines or other betaines.

Claims (41)

1. A bituminous emulsion comprising:

binding material;

emulsifier, the emulsifier comprising octylphenol ethoxylates at a rate of 0.05% to 10% by weight of the bituminous emulsion; and

a second emulsifier at a rate of 0.05% to 10% by weight of the bituminous emulsion wherein the second emulsifier comprises tallow diamine betaine.

2. The bituminous emulsion of claim 1 where the tallow diamine betaines is methylated tallow alkyl diamine betaine.

3. The bituminous emulsion of claim 1 where the tallow diamine betaines is ethoxylated or polyethoxylated tallow alkyl diamine betaine.

4. The bituminous emulsion of claim 1 where the bituminous emulsion is solvent free.

5. A method of creating and using a penetrating prime emulsion, the method comprising:

selecting a binding material;

producing an aqueous phase, the aqueous phase comprising:

an emulsifier, the emulsifier comprising octylphenol ethoxylates at a rate of 0.05% to 10% by weight of the penetrating prime emulsion; and

a second emulsifier at a rate of 0.05% to 10% by weight of the penetrating prime emulsion wherein the second emulsifier comprises tallow diamine betaine; and

emulsifying the binding material in a range of 5% to 75% binding material phase and 10% to 95% aqueous phase to produce the penetrating prime emulsion.

6. The method of claim 5 where the tallow diamine betaines is methylated tallow alkyl diamine betaine.

7. The method of claim 5 where the tallow diamine betaines is ethoxylated or polyethoxylated tallow alkyl diamine betaine.

8. The method of claim 5 where the penetrating prime emulsion is solvent free.

9. The method of claim 5 further comprising applying the penetrating prime emulsion to a surface.

10. The method of claim 9 further comprising:

waiting three days; and

then applying a paved layer to the surface.

11. The method of claim 9 further comprising:

waiting one day; and

then applying a paved layer to the surface.

12. The method of claim 9 further comprising:

waiting 8 hours; and

then applying a paved layer to the surface.

13. The method of claim 9 further comprising:

waiting one hour; and

then applying a paved layer to the surface.

14. The method of claim 5 further comprising testing the penetrating prime emulsion by applying it to a compacted soil specimen.

15. The method of claim 14 further comprising first creating the compacted soil specimen by:

separating the aggregate to 100% passing the #8 sieve;

adding 5% water to assist compaction;

compacting at 100-135 psi or higher;

drying out the sample overnight at +100 C; and

cooling to room temperature.

16. A method of dust control, the method comprising:

applying a bituminous emulsion to a surface, the bituminous emulsion comprising binding material, emulsifier, and a second emulsifier, the emulsifier comprising octylphenol ethoxylates at a rate of 0.05% to 10% by weight of the bituminous emulsion and the second emulsifier at a rate of 0.05% to 10% by weight of the bituminous emulsion and where the second emulsifier comprises tallow diamine betaine.

17. The bituminous emulsion of claim 16 where the tallow diamine betaines is methylated tallow alkyl diamine betaine.

18. The bituminous emulsion of claim 16 where the tallow diamine betaines is ethoxylated or polyethoxylated tallow alkyl diamine betaine.

19. The bituminous emulsion of claim 16 where the bituminous emulsion is solvent free.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 20, 2021
From: BARNAT, JAMES; COATES, JOEL
To: ARRMAZ PRODUCTS INC.
Reel/Frame 057846/0780 →
Continuity (2)
Provisional Application 63093896 · Oct 20, 2020
Related Publication 20220119312A1 · Apr 21, 2022
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