IP Library Granted Patent US 11,772,009
Granted Patent B2
US 11,772,009 · App. 17/547,435 · Granted Oct 3, 2023

Systems and methods for rehabilitating alcohol

Inventors: Matthew J. Rubin (Indianapolis, IN); Adam Daniel Ambrecht (Kennesaw, GA); Jessica Clare Halstead (Indianapolis, IN)
Assignee: Trade Secret Chocolates
B01D3/106B01D3/001B01D3/42C07C29/84C12F3/06C12G3/08
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Quick Facts
Patent No.
US 11,772,009
App. No.
17/547,435
Granted
Oct 3, 2023
Kind
B2
Abstract

An assembly for rehabilitating alcohol, including a pressure controllable chamber, a cooler in thermal communication with the pressure controllable chamber, a liquid inlet port in fluidic communication with the pressure controllable chamber, a liquid outlet port in fluidic communication with the pressure controllable chamber, and a gas outlet port in fluidic communication with the pressure controllable chamber. The assembly further includes a partial vacuum source in fluidic communication with the gas outlet port for establishing a partial vacuum in the pressure controllable chamber, and a liquid collection vessel in fluidic communication with the liquid outlet port. The residence time from when a liquid is flowed into the pressure controllable chamber until the liquid exits the chamber is no more than sixty seconds. The partial vacuum is insufficient to evaporate an ethanol solution during residence time in the pressure controllable chamber.

Claims (62)

1. An apparatus for rehabilitating alcohol, comprising:

a pressure vessel defining a pressure controllable chamber;

a water jacket at least partially surrounding the pressure controllable chamber and in thermal communication therewith;

a liquid inlet port in fluidic communication with the pressure controllable chamber;

a gas outlet port in fluidic communication with the pressure controllable chamber;

a vacuum pump in fluidic communication with the gas outlet port;

a collection vessel operationally connected to the pressure vessel;

a liquid outlet port in fluidic communication with the pressure controllable chamber;

wherein the pressure within the pressure controllable chamber is maintained between forty-five Torr and fifteen Torr at ambient temperature and

wherein the pressure vessel defines a distillation-free environment for an ethanol solution.

2. The apparatus of claim 1 and further comprising:

an ethanol solution source operationally connected to the liquid inlet port;

a first liquid pump in fluidic communication with the liquid inlet port and the ethanol solution source; and

a second liquid pump in fluidic communication with the liquid outlet port and the collection vessel.

3. The apparatus of claim 1 and further comprising:

a helical race winding around the pressure controllable chamber a plurality of times from the liquid inlet port to the liquid outlet port.

4. The apparatus of claim 1 and further comprising:

an agitator positioned in the pressure controllable chamber.

5. The apparatus of claim 1 and further comprising at least one sensor operationally connected within the pressure controllable chamber; wherein the at least one sensor is selected from the group comprising pressure sensors, temperature sensors, chemical sensors, and combinations thereof.

6. The apparatus of claim 2 and further comprising:

an electronic controller operationally connected to the respective pumps, the respective ports, and the water jacket.

7. The apparatus of claim 1 wherein the liquid inlet port is a spray head.

8. The apparatus of claim 1 and further comprising a ramp operationally connected to receive liquid from the inlet port, thin the liquid into a sheet, and convey the liquid to the liquid outlet port.

9. The apparatus of claim 1 wherein the pressure vessel is a helically wound tube.

10. An assembly for rehabilitating alcohol, comprising:

a pressure controllable chamber;

a cooler in thermal communication with the pressure controllable chamber;

a liquid inlet port in fluidic communication with the pressure controllable chamber;

a liquid outlet port in fluidic communication with the pressure controllable chamber;

a gas outlet port in fluidic communication with the pressure controllable chamber;

a partial vacuum source in fluidic communication with the gas outlet port for establishing a partial vacuum in the pressure controllable chamber; and

a liquid collection vessel in fluidic communication with the liquid outlet port;

wherein the vacuum source provides a pressure within the pressure controllable chamber of between twenty Torr and forty Torr at 22 degrees Celsius;

wherein residence time from when a liquid is flowed into the pressure controllable chamber until the liquid exits the chamber is no more than sixty seconds;

wherein the partial vacuum is insufficient to evaporate an ethanol solution during residence time in the pressure controllable chamber; and

wherein distillation of an ethanol solution does not occur within the pressure vessel.

11. The assembly of claim 10 wherein the pressure controllable chamber is a helical tube.

12. The assembly of claim 10 and further comprising:

a helical race winding around the pressure controllable chamber a plurality of times from the liquid inlet port to the liquid outlet port.

13. The assembly of claim 10 and further comprising an ethanol solution source operationally connected to the liquid inlet port;

a first liquid pump in fluidic communication with the liquid inlet port and the ethanol solution source; and

a second liquid pump in fluidic communication with the liquid outlet port and the collection vessel.

14. The assembly of claim 13 and further comprising at least one sensor operationally connected within the pressure controllable chamber; wherein the at least one sensor is selected from the group comprising pressure sensors, temperature sensors, chemical sensors, and combinations thereof.

15. The assembly of claim 14 and further comprising:

an electronic controller operationally connected to the respective pumps, the respective ports, and the cooler.

16. The assembly of claim 10 wherein the liquid inlet port is a spray head.

17. A combination for rehabilitating previously distilled alcohol, comprising:

a pressure controllable chamber;

a cooler in thermal communication with the pressure controllable chamber;

a liquid inlet port in fluidic communication with the pressure controllable chamber;

a liquid outlet port in fluidic communication with the pressure controllable chamber;

a gas outlet port in fluidic communication with the pressure controllable chamber;

a partial vacuum source in fluidic communication with the gas outlet port for establishing a partial vacuum of between twenty-five Torr and thirty-five Torr at room temperature in the pressure controllable chamber;

a liquid collection vessel in fluidic communication with the liquid outlet port;

an ethanol solution source operationally connected to the liquid inlet port;

a first liquid pump in fluidic communication with the liquid inlet port and the ethanol solution source;

a second liquid pump in fluidic communication with the liquid outlet port and the liquid collection vessel; and

at least one sensor operationally connected within the pressure controllable chamber, wherein the at least one sensor is selected from the group comprising pressure sensors, temperature sensors, chemical sensors, and combinations thereof; and

an electronic controller operationally connected to the respective pumps, the respective ports, and the cooler;

wherein residence time from when a liquid is flowed into the pressure controllable chamber until the liquid exits the chamber is no more than sixty seconds;

wherein the partial vacuum is insufficient to evaporate an ethanol solution during residence time in the pressure controllable chamber; and

wherein the pressure and temperature defining the environment within the pressure controllable chamber are such that the distillation of an ethanol solution does not occur therein.

Assignments (2)
MERGER Recorded Oct 16, 2023
From: TRADE SECRET CHOCOLATES INC.
To: TRUE ESSENCE FOODS INC.
Reel/Frame 065239/0868 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 24, 2022
From: RUBIN, MATTHEW J; AMBRECHT, ADAM; HALSTEAD, JESSICA C
To: TRADE SECRET CHOCOLATES
Reel/Frame 059089/0632 →
Continuity (2)
Continuation 16939340 · Jul 27, 2020
Related Publication 20220111303A1 · Apr 14, 2022
Cited By (1)
US 12,318,718