IP Library Granted Patent US 11,522,252
Granted Patent B2
US 11,522,252 · App. 17/590,394 · Granted Dec 6, 2022

Separators for electrochemical cells

Inventors: Steven A. Carlson (Cambridge, MA); Ifenna Kingsley Anakor (Allston, MA); Greg Robert Farrell (Sudbury, MA)
Assignee: LG Energy Solution, Ltd.
H01M50/446C04B14/303C04B24/00C04B24/023C04B26/06C04B38/0074H01M50/409H01M50/411H01M50/431C04B2111/00612C04B2111/00801C04B2111/00853Y02E60/10Y10T29/49115
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Quick Facts
Patent No.
US 11,522,252
App. No.
17/590,394
Granted
Dec 6, 2022
Kind
B2
Abstract

Provided are separators for use in an electrochemical cell comprising (a) an inorganic oxide and (b) an organic polymer, wherein the inorganic oxide comprises organic substituents. Also provided are electrochemical cells comprising such separators.

Claims (34)

1. An electrochemical cell comprising:

(a) an anode;

(b) a cathode;

(c) a porous separator comprising a free-standing inorganic oxide layer, and wherein said free-standing inorganic oxide layer comprises:

a hydrated aluminum oxide; and

an organic polymer that is covalently bonded to at least a portion of said hydrated aluminum oxide; and

(d) an electrolyte selected from a group consisting of liquid organic electrolytes, gel polymer electrolytes, and solid polymer electrolytes,

wherein the separator is 6 μm to 25 μm thick.

2. The electrochemical cell of claim 1 , wherein the separator has an elastic modulus of 15,000 kg/cm 2 to 50,000 kg/cm 2 .

3. The electrochemical cell of claim 1 , wherein the separator has a tensile strength between 100 kg/cm 2 to 500 kg/cm 2 at 2 percent elongation.

4. The electrochemical cell of claim 1 , wherein an average pore diameter of said inorganic oxide layer of said separator is 30 nm to 50 nm.

5. The electrochemical cell of claim 1 , wherein said hydrated aluminum oxide comprises boehmite.

6. The electrochemical cell of claim 1 , wherein said hydrated aluminum oxide is of a formula Al 2 O 3 .xH 2 O, wherein x is in a range of 0.8 to less than 1.0.

7. The electrochemical cell of claim 1 , wherein said hydrated aluminum oxide is of a formula Al 2 O 3 .xH 2 O, wherein x is in a range of 1.0 to 1.5.

8. The electrochemical cell of claim 1 , wherein a anode comprises lithium as the anode active material.

9. The electrochemical cell of claim 1 , wherein the separator does not melt at temperatures below 300° C.

10. The electrochemical cell of claim 1 , wherein the organic polymer is present in an amount of 5 percent to 35 percent of the weight of the hydrated aluminum oxide.

11. An electrochemical cell comprising:

(a) an anode;

(b) a cathode;

(c) a porous separator comprising a free-standing inorganic oxide layer, and wherein said free-standing inorganic oxide layer comprises:

a hydrated aluminum oxide; and

an organic polymer that is covalently bonded to at least a portion of said hydrated aluminum oxide; and

(d) an electrolyte selected from a group consisting of liquid organic electrolytes, gel polymer electrolytes, and solid polymer electrolytes,

wherein an average pore diameter of said inorganic oxide layer of said separator is 30 nm to 50 nm.

12. The electrochemical cell of claim 11 , wherein the separator has a tensile strength between 100 kg/cm 2 to 500 kg/cm 2 at 2 percent elongation.

13. The electrochemical cell of claim 11 , wherein said inorganic oxide layer has a % porosity of 48% to 62%.

14. The electrochemical cell of claim 11 , wherein said hydrated aluminum oxide is of a formula Al 2 O 3 .xH 2 O, wherein x is in a range of 0.8 to less than 1.0.

15. The electrochemical cell of claim 11 , wherein said hydrated aluminum oxide is of a formula Al 2 O 3 .xH 2 O, wherein x is in a range of 1.0 to 1.5.

16. The electrochemical cell of claim 11 , wherein the separator has an elastic modulus of 15,000 kg/cm 2 to 50,000 kg/cm 2 .

17. The electrochemical cell of claim 11 , wherein the anode comprises lithium as a anode active material.

18. The electrochemical cell of claim 11 , wherein the separator does not melt at temperatures below 300° C.

19. The electrochemical cell of claim 11 , wherein the organic polymer is present in an amount of 5 percent to 35 percent of the weight of the hydrated aluminum oxide.

20. The electrochemical cell of claim 11 , wherein the separator has a percent elongation at break at least 10%.

Assignments (1)
NUNC PRO TUNC ASSIGNMENT Recorded May 24, 2022
From: OPTODOT CORPORATION
To: LG ENERGY SOLUTION, LTD.
Reel/Frame 060000/0089 →
Continuity (8)
Continuation 17406515 · Aug 19, 2021
Continuation 17019584 · Sep 14, 2020
Continuation 16657257 · Oct 18, 2019
Continuation 15799449 · Oct 31, 2017
Continuation 14534991 · Nov 6, 2014
Continuation 11652948 · Jan 12, 2007
Provisional Application 60773487 · Feb 15, 2006
Related Publication 20220158302A1 · May 19, 2022