IP Library Granted Patent US 12,378,123
Granted Patent B2
US 12,378,123 · App. 17/609,806 · Granted Aug 5, 2025

Chromium-free, iron-based catalyst for water gas shift reaction and methods of use thereof

Inventors: Jian-Ping Shen (Research Triangle Park, NC); Brian Turk (Durham, NC); Pradeepkumar Sharma (Research Triangle Park, NC); David Denton (Mt. Pleasant, SC)
Assignee: Research Triangle Institute
C01B32/50B01J8/24B01J19/0093B01J23/72B01J23/78B01J23/80B01J35/31B01J35/613C01B3/16C01B2203/0283
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Quick Facts
Patent No.
US 12,378,123
App. No.
17/609,806
Granted
Aug 5, 2025
Kind
B2
Abstract

A chromium-free catalyst for use in a fluidized bed reactor is described. The catalyst comprises 45-70 wt % Fe 2 O 3 , 5-15 wt % CuO, 20-35 wt % Al 2 O 3 , 10-20 wt % ZnO, and 1-15 wt % K 2 CO 3 . The catalyst has a Davison Index (DI %) of less than or equal to 15. A method for converting carbon monoxide (CO) into carbon-dioxide (CO 2 ) using the catalyst is described. The method includes introducing H 2 O and CO into a fluidized bed reactor having an operating temperature between about 375° C. and about 450° C. and comprising the chromium free catalyst. The CO conversion is at least 60%.

Claims (15)

1. Fluidizable and attrition-resistant chromium-free catalyst for use in water gas shift reaction in a fluidized bed reactor, comprising

45-70 wt % Fe 2 O 3

5-15 wt % CuO

20-35 wt % Al 2 O 3

10-25 wt % ZnO,

1-15 wt % K 2 CO 3

wherein the catalyst has a Davison Index (DI) of less than or equal to 15.

2. The catalyst of claim 1 , having a BET surface area of about 10-60 m 2 /g.

3. The catalyst of claim 1 , having a density of about 0.8 to about 1.8 g/ml.

4. The catalyst of claim 1 , comprising about 4-6 wt % K 2 CO 3 .

5. The catalyst of claim 1 , comprising about 50-60 wt % Fe 2 O 3 .

6. The catalyst of claim 1 , comprising about 20-25 wt % Al 2 O 3 .

7. The catalyst of claim 1 , comprising about 10-15 wt % ZnO.

8. The catalyst of claim 1 , comprising about 5-10 wt % CuO and optionally 0 to 15 wt % MgO and/or optionally 0 to 15 wt % CeO 2 .

9. The catalyst of claim 1 , wherein the DI is between about 5 and about 7.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 24, 2022
From: RESEARCH TRIANGLE INSTITUTE
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 060173/0546 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 9, 2021
From: SHEN, JIAN-PING; TURK, BRIAN; SHARMA, PRADEEPKUMAR; DENTON, DAVID
To: RESEARCH TRIANGLE INSTITUTE
Reel/Frame 058055/0326 →
Continuity (2)
Provisional Application 62849251 · May 17, 2019
Related Publication 20220219992A1 · Jul 14, 2022
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