Apparatus and method for solvent recovery from drying process
Method and apparatus for condensing a majority of the solvent in a process gas stream at low temperatures, e.g., below the freezing point of water, ca. −5° C. The gas stream exiting the condenser step may be further processed in one or more emission control devices, such as a single or multi-step series of concentrator devices, such as zeolite concentrator devices. One or more emission control operations can be carried out downstream of the single or multi-step concentrators. The aforementioned condensing process enables the one or more concentrators to operate in a favorable temperature range for removal of 99% or more of VOC, thereby meeting or exceeding strict environmental regulations.
1. A method for conditioning a circulation air laden with at least one condensable fluid, comprising:
a. introducing the circulation air at a first volume flow and intake temperature level above 0° C. to a main condenser with at least one main condensation chamber;
b. gradually cooling the circulation air to a main temperature level of 0° C. or less inside the main condensation chamber;
c. splitting the volume flow of the circulation air into a high volume re-circulating flow and low volume off-gas side stream after reaching a second temperature level; and
d. providing the high-volume re-circulating flow to a circulation air intake of a dryer,
the method further comprising providing a condenser to cool the circulation air according to step b), which comprises at least one cooling coil containing a cooling medium, and whereby the cooling medium enters the cooling coil at a far end side of a circulation air entry with entry temperature of 0° C. or less and is heated while traveling through the cooing coil in a counter-flow direction to the circulation air, the cooling coil having coil tube and finned surface and
wherein the rate of cooling is maintained at less than 0.30 C degrees per millisecond, while the gas flow travels the distance between the condensing coil tubes and finned surfaces.
2. The method according to claim 1 , wherein the rate of cooling is maintained at between 0.15 and 0.22 C degrees per millisecond.
3. The method according to claim 1 , further comprising:
a. feeding the circulation air at the first volume flow to a pre-condenser upstream of said main condenser with a pre-condensing temperature level below a first temperature level and above said main temperature level;
b. gradually cooling the circulation air to said pre-condensing temperature level in the pre-condenser; and
c. providing the cooled circulation air to an intake of said main condenser.
4. The method according to claim 2 , further comprising:
a. feeding the circulation air at the first volume flow to a pre-condenser upstream of said main-condenser with a pre-condensing temperature level below a first temperature level and above said main condensing temperature;
b. gradually cooling the circulation air to said pre-condensing temperature level in the pre-condenser; and
c. providing the cooled circulation air to an intake of said main condenser.
5. The method according to claim 1 , further comprising pre-cooling said circulation air upstream of said main condenser.
6. The method according to claim 1 , further comprising re-heating said circulation air downstream of said main condenser.
7. The method according to claim 3 , further comprising re-heating said circulation air downstream of said main condenser.
8. The method according to claim 1 , further comprising:
a. feeding the off-gas side stream to an at least two-stage air pollution control device;
b. collecting and increasing the concentration of residual condensable fluid in an adsorptive concentrator as a first pollution control stage;
c. subsequently treating a remaining off gas stream in a second air pollution control device as a second stage further downstream of the first stage to a level of concentration of residual condensable in the air well below a predetermined limit.
9. The method of claim 8 , wherein said predetermined limit is 1 mg/Nm 3 .
10. The method according to claim 8 , wherein said second air pollution control device is a second adsorptive concentrator.
11. The method according to claim 8 , wherein said second air pollution control device is a filtration device.
12. The method according to claim 11 , wherein said filtration device comprises an active carbon filter.
13. The method of claim 1 , further comprising adding humidity to said circulation air prior to gradually cooling the circulation air.
14. The method according to claim 13 , further comprising sensing the dew point of said circulation air prior to its provision to said main condenser, and sensing the temperature of said high volume re-circulating flow, wherein the amount of humidity added to said circulation air is based on the sensed temperature of said high volume re-circulating flow.
15. The method of claim 13 , further comprising sensing a dew point temperature value of said circulation air prior to introduction of said circulation air into said main condenser; sensing the temperature of fluid exiting said at least one main condenser, and controlling the introduction of humidity in response to the sensed dew point temperature and the sensed temperature of fluid exiting said at least one main condenser.
16. The method of claim 13 , further comprising analyzing a solvent concentration of fluid in circulation air exhausted from said main condenser; sensing humidity of the fluid in said circulation air exhausted from said main condenser; calculating a mole fraction of water in said air exhausted from said main condenser; and introducing humidity into said circulating air entering said main condenser in response to when said mole fraction is lower than a predetermined value.