IP Library Granted Patent US 11,891,470
Granted Patent B2
US 11,891,470 · App. 17/612,674 · Granted Feb 6, 2024

Method for producing chloroprene-based-polymer latex

Inventors: Yuki Miura (Yokohama, JP); Yuji Hashimoto (Yokohama, JP); Keiichi Nakamura (Kawasaki, JP)
Assignee: Resonac Corporation
C08F36/18C08F6/003
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Quick Facts
Patent No.
US 11,891,470
App. No.
17/612,674
Granted
Feb 6, 2024
Kind
B2
Abstract

A method for producing a chloroprene-based polymer latex which can efficiently remove a residual volatile organic substance from the chloroprene-based polymer latex while suppressing the deposition of agglomerates is provided. In the method for producing a chloroprene-based polymer latex of the present invention, when the residual volatile organic substance comprised in the latex is volatilized and removed, a mixed fluid of one or more gases selected from the group consisting of inert gases and air, and water is contacted with the latex at a gas pressure higher than the saturated water vapor pressure, and a temperature of the mixed fluid is a temperature lower than a boiling point of water at the gas pressure.

Claims (11)

1. A method for producing a chloroprene-based polymer latex,

wherein when a residual volatile organic substance comprised in the latex is volatilized and removed, a mixed fluid of one or more gases selected from inert gases and air, and water is contacted with the latex at a gas pressure higher than a saturated water vapor pressure at a liquid temperature of the latex,

a temperature of the mixed fluid is a temperature lower than a boiling point of water at the gas pressure, and

the temperature of the latex contacted with the mixed fluid is 10 to 60° C.

2. The method for producing a chloroprene-based polymer latex according to claim 1 , wherein the temperature of the mixed fluid contacted with the latex is 10 to 60° C.

3. The method for producing a chloroprene-based polymer latex according to claim 1 , wherein the mixed fluid is contacted with the latex by blowing the mixed fluid into the latex liquid.

4. The method for producing a chloroprene-based polymer latex according to claim 1 , wherein a concentration of the residual volatile organic substance comprised in the latex before the latex is contacted with the mixed fluid is 150 to 10000 ppm by mass based on a total mass of the latex.

5. The method for producing a chloroprene-based polymer latex according to claim 1 , wherein the concentration of the residual volatile organic substance comprised in the latex is reduced to less than 150 ppm by mass based on the total mass of the latex.

6. The method for producing a chloroprene-based polymer latex according to claim 1 , wherein the residual volatile organic substance is a residual monomer in polymerization reaction in production of the latex.

7. The method for producing a chloroprene-based polymer latex according to claim 1 , wherein the inert gases are selected from noble gases and nitrogen gas.

8. The method for producing a chloroprene-based polymer latex according to claim 1 , wherein the inert gases are selected from argon and nitrogen gas.

Assignments (3)
CHANGE OF ADDRESS Recorded Feb 9, 2024
From: RESONAC CORPORATION
To: RESONAC CORPORATION
Reel/Frame 066547/0677 →
CHANGE OF NAME Recorded Jun 23, 2023
From: SHOWA DENKO K.K.
To: RESONAC CORPORATION
Reel/Frame 064082/0513 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 2, 2021
From: MIURA, YUKI; HASHIMOTO, YUJI; NAKAMURA, KEIICHI
To: SHOWA DENKO K.K.
Reel/Frame 058270/0438 →