Methods for producing a hollow-core fiber and for producing a preform for a hollow-core fiber
Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that the step of providing and/or arranging the anti-resonant element preforms and/or the process of carrying out a hot-forming process includes a fixation measure and/or a sealing measure using an amorphous SiO 2 particle-containing sealing or joining compound.
1. A method for producing an anti-resonant hollow-core fiber comprising a hollow core extending along a longitudinal axis of the fiber and a sheath region surrounding the hollow core and comprising a plurality of anti-resonance elements, the method comprising:
(a) providing a cladding tube comprising an inner bore of the cladding tube and a longitudinal axis of the cladding tube, along which a cladding tube wall delimited by an inner side and an outer side extends,
(b) providing a number of anti-resonance element preforms composed of a plurality of nested structural elements,
(c) arranging the anti-resonance element preforms at setpoint positions of the inner side of the cladding tube wall to form a primary preform for the hollow-core fiber, which comprises a hollow core region and a sheath region, and
(d) elongating the primary preform to form the hollow-core fiber or further processing the primary preform into a secondary preform from which the hollow-core fiber is drawn, wherein the further processing comprises a single or repeated performance of one or more of the following hot-forming processes:
(i) elongation,
(ii) collapse,
(iii) collapse and simultaneous elongation,
(iv) collapse of additional sheath material,
(v) collapse of additional sheath material and subsequent elongation,
(vi) collapse of additional sheath material and simultaneous elongation,
wherein the provision of the anti-resonance element preforms comprises a fixing measure,
wherein the nested structural elements are fixed with respect to one another using a sealing or bonding compound containing amorphous SiO 2 particles obtained by wet milling grains of high-purity silica glass, and wherein the sealing or bonding compound is vitrified by heating during a hot forming process according to process step (d).
2. The method according to claim 1 , wherein the anti-resonance element preforms are fixed to the inner side of the cladding tube using the sealing or bonding compound.
3. The method according to claim 2 , wherein the anti-resonance element preforms are cylindrical and have two opposite end regions, and that fixing using the sealing or bonding compound takes place exclusively at one of the end regions or exclusively at both end regions.
4. The method according to claim 2 , wherein the arranging of the anti-resonance element preforms on the inner side of the cladding tube comprises fixing by means of a positioning template to be introduced into the inner bore of the cladding tube, which positioning template has multiple radially outward-facing holding elements for positioning the anti-resonance element preforms at the setpoint positions.
5. The method according to claim 4 , wherein the positioning template is used exclusively in the region of the cladding tube end faces, preferably in the region of both cladding tube end faces.
6. The method according to claim 1 , wherein a cladding tube having a circular inner cross-section is provided, and in that a longitudinal structure, preferably a longitudinal groove, is produced on the inner side of the cladding tube wall and has a recess to which or in which the anti-resonance element preforms are fixed.
7. The method according to claim 6 , wherein the sealing or bonding compound is introduced into the recess of the longitudinal structure and that the anti-resonance element preforms, when arranged at the setpoint position according to method step (c), contact the sealing or bonding compound.
8. The method according to claim 6 , wherein the longitudinal structure of the inner side of the cladding tube is produced by means of drilling, sawing, milling, cutting or grinding.
9. The method according to claim 1 , wherein the fixing of cylindrical structural elements using the sealing or bonding compound takes place only at one face end or only at both face ends of the structural elements.
10. The method according to claim 1 , wherein, in order to carry out a process according to method step (d), the preform is bonded to a holder, and the bond between the preform and the holder is produced by means of the sealing or bonding compound.
11. The method according to claim 1 , wherein, in order to carry out a process according to method step (d), the preform is bonded to a gas connection, and the bond between the preform and the gas connection is produced by means of the sealing or bonding compound.
12. The method according to claim 1 , wherein open ends of the anti-resonance element preforms and/or individual structural elements of the anti-resonance element preforms and/or any annular gap between tube elements can be closed by means of the sealing or bonding compound to carry out a process according to method step (d).
13. The method according to claim 1 , wherein the anti-resonance elements are arranged about the hollow core with an odd symmetry.
14. A method for producing a preform for an anti-resonant hollow-core fiber comprising a hollow core extending along a longitudinal axis of the fiber and a sheath region surrounding the hollow core, said sheath region comprising a plurality of anti-resonance elements, with the method comprising:
(a) providing a cladding tube comprising an inner bore of the cladding tube and a longitudinal axis of the cladding tube, along which a cladding tube wall delimited by an inner side and an outer side extends,
(b) providing a number of anti-resonance element preforms composed of a plurality of nested structural elements,
(c) arranging the anti-resonance element preforms in each case at setpoint positions of the inner side of the cladding tube wall to form a primary preform for the hollow-core fiber, which comprises a hollow core region and a sheath region, and
(d) optionally further processing the primary preform into a secondary preform for the hollow-core fiber, wherein the further processing comprises a single or repeated performance of one or more of the following hot-forming processes:
(i) elongation,
(ii) collapse,
(iii) collapse and simultaneous elongation,
(iv) collapse of additional sheath material,
(v) collapse of additional sheath material and subsequent elongation,
(vi) collapse of additional sheath material and simultaneous elongation,
wherein the provision of the anti-resonance element preforms comprises a fixing measure,
wherein the nested structural elements are fixed with respect to one another using a sealing or bonding compound containing amorphous SiO 2 particles obtained by wet milling grains of high-purity silica glass, wherein the sealing or bonding compound is vitrified by heating during a hot forming process according to process step (d).