Furnace system and method of use
A sintering furnace can include an outer shell defining an internal volume a reactive agent inlet configured to introduce a reactive agent into the internal volume; an insulation chamber within the outer shell; and a retort configured to retain an object. A method of operating a sintering furnace can include sintering a part precursor within a retort arranged within a chamber, wherein the chamber defines an intermediate volume between the retort and the chamber, wherein a sintering byproduct is oxidized within the intermediate volume.
1. A method for operating a sintering furnace, comprising,
in a retort, sintering a part precursor at a sintering temperature to form a finished part, wherein the retort defines a retort volume, wherein the retort is arranged within a chamber defining an intermediate volume between the retort and the chamber, wherein a sintering byproduct is oxidized within the intermediate volume, wherein an inert gas is injected into the retort volume and wherein an oxidizing agent is injected into the intermediate volume, wherein an oxidizing agent concentration within the intermediate volume is at most approximately 1000 parts per million (ppm).
2. The method of claim 1 , wherein a carbon content of an environment within the retort volume is approximately equal to a carbon content of the finished part.
3. The method of claim 1 , wherein the sintering byproduct flows out of the retort volume into the intermediate volume.
4. The method of claim 1 , wherein an inert gas flow rate is greater than an oxidizing agent flow rate.
5. The method of claim 1 , further comprising, before sintering the part precursor, debinding the part precursor at a debinding temperature below the sintering temperature.
6. The method of claim 5 , wherein the oxidizing agent is injected into the intermediate volume during debinding the part precursor.
7. The method of claim 1 , further comprising, measuring a carbon dioxide level, wherein an oxidizing agent flow rate is determined based on the carbon dioxide level.
8. The method of claim 1 , wherein the inert gas is preheated within a tortuous chamber of the retort before the inert gas is injected into the retort volume.
9. The method of claim 1 , wherein an oxidizing agent concentration within the retort volume is at most approximately 100 ppm.
10. A method for operating a sintering furnace, comprising,
in a retort, sintering a part precursor at a sintering temperature to form a finished part, wherein the retort defines a retort volume, wherein the retort is arranged within a chamber defining an intermediate volume between the retort and the chamber, wherein a sintering byproduct is oxidized within the intermediate volume, wherein an inert gas is injected into the retort volume and wherein an oxidizing agent is injected into the intermediate volume; and
measuring a carbon dioxide level, wherein an oxidizing agent flow rate is determined based on the carbon dioxide level.
11. The method of claim 10 , wherein a carbon content of an environment within the retort volume is approximately equal to a carbon content of the finished part.
12. The method of claim 10 , wherein the sintering byproduct flows out of the retort volume into the intermediate volume.
13. The method of claim 10 , wherein an inert gas flow rate is greater than the oxidizing agent flow rate.
14. The method of claim 10 , further comprising, before sintering the part precursor, debinding the part precursor at a debinding temperature below the sintering temperature.
15. The method of claim 14 , wherein the oxidizing agent is injected into the intermediate volume during debinding the part precursor.
16. A method for operating a sintering furnace, comprising, in a retort, sintering a part precursor at a sintering temperature to form a finished part, wherein the retort defines a retort volume, wherein the retort is arranged within a chamber defining an intermediate volume between the retort and the chamber, wherein a sintering byproduct is oxidized within the intermediate volume, wherein an inert gas is injected into the retort volume and wherein an oxidizing agent is injected into the intermediate volume, wherein the inert gas is preheated within a tortuous chamber of the retort before the inert gas is injected into the retort volume.
17. The method of claim 16 , wherein a carbon content of an environment within the retort volume is approximately equal to a carbon content of the finished part.
18. The method of claim 16 , wherein the sintering byproduct flows out of the retort volume into the intermediate volume.
19. The method of claim 16 , wherein an inert gas flow rate is greater than an oxidizing agent flow rate.
20. The method of claim 16 , further comprising, before sintering the part precursor, debinding the part precursor at a debinding temperature below the sintering temperature.
21. The method of claim 20 , wherein the oxidizing agent is injected into the intermediate volume during debinding the part precursor.