Method for producing n-vinylacetamide and pyrolysis device
A method for producing N-vinylacetamide includes a feeding step of feeding a raw material containing N-(1-methoxyethyl)acetamide (MEA) to an evaporator, an evaporation step of evaporating, by the evaporator, the raw material, to form a vaporized raw material, a superheating step of feeding the vaporized raw material to a superheater, and superheating the vaporized raw material such that a superheating temperature of the vaporized raw material is equal to or more than a temperature higher by 5° C. than a boiling point of the N-(1-methoxyethyl)acetamide (MEA) under an inner pressure of the superheater and equal to or less than 200° C., and a thermal decomposition step of feeding the superheated vaporized raw material to a thermal decomposition reactor, to thermally decompose the superheated vaporized raw material, and a content of the N-(1-methoxyethyl)acetamide in the raw material is from 80 to 100 mass %.
1 . A method for producing N-vinylacetamide, comprising:
a feeding step of feeding a raw material containing N-(1-methoxyethyl)acetamide (MEA) to an evaporator,
an evaporation step of evaporating, by the evaporator, the raw material, to form a vaporized raw material,
a superheating step of feeding the vaporized raw material to a superheater, and superheating the vaporized raw material such that a superheating temperature of the vaporized raw material is equal to or more than a temperature higher by 5° C. than a boiling point of the N-(1-methoxyethyl)acetamide under an inner pressure of the superheater and equal to or less than 200° C., and
a thermal decomposition step of feeding the superheated vaporized raw material to a thermal decomposition reactor, to thermally decompose the superheated vaporized raw material, wherein a content of the N-(1-methoxyethyl)acetamide in the raw material is from 80 to 100 mass %.
2 . A method for producing N-vinylacetamide, comprising:
a feeding step of feeding a raw material containing N-(1-methoxyethyl)acetamide (MEA) to an evaporator,
an evaporation step of evaporating, by the evaporator, the raw material, to form a vaporized raw material,
a superheating step of feeding the vaporized raw material to a superheater, and giving an amount of heat of 1.0 KJ/mol or more to the vaporized raw material to superheat the vaporized raw material, and
a thermal decomposition step of feeding the superheated vaporized raw material to a thermal decomposition reactor, to thermally decompose the superheated vaporized raw material, wherein a content of the N-(1-methoxyethyl)acetamide in the raw material is from 80 to 100 mass %.
3 . The method for producing N-vinylacetamide according to claim 1 , wherein the evaporation step is performed under reduced pressure.
4 . The method for producing N-vinylacetamide according to claim 1 , wherein the thermal decomposition step is performed under reduced pressure.
5 . The method for producing N-vinylacetamide according to claim 1 , wherein the evaporator is a falling film evaporator.
6 . The method for producing N-vinylacetamide according to claim 1 , wherein the evaporator is a forced film evaporator.
7 . The method for producing N-vinylacetamide according to claim 1 , wherein a downstream end of the evaporator is connected to an upstream end of the superheater via a first piping, and
a downstream end of the first piping is at the highest position in the first piping.
8 . The method for producing N-vinylacetamide according to claim 1 , wherein a downstream end of the superheater is connected to an upstream end of the thermal decomposition reactor via a second piping, and
an upstream end of the second piping is at the highest position in the second piping.
9 . The method for producing N-vinylacetamide according to claim 1 , further comprising, between the evaporation step and the thermal decomposition step, a collection step of collecting, from the raw material fed to the evaporator, a liquid raw material that is not vaporized and a liquid raw material comprising a part of the vaporized raw material that is liquefied,
the collection step being a step of collecting the liquid raw material by a raw material collection device provided between the evaporator and the thermal decomposition reactor.
10 . The method for producing N-vinylacetamide according to claim 9 , wherein a downstream end of the evaporator is joined to an upstream end of the raw material collection device.
11 . The method for producing N-vinylacetamide according to claim 9 , wherein a downstream end of the raw material collection device is joined to an upstream end of the superheater.
12 . The method for producing N-vinylacetamide according to claim 10 , wherein the vaporized raw material is fed through the raw material collection device to the thermal decomposition reactor.
13 . The method for producing N-vinylacetamide according to claim 9 , wherein the raw material collection device comprises:
a cylindrical part through which the vaporized raw material is distributed,
a collecting section with which a flow of the vaporized raw material flowing through the cylindrical part partially or entirely collides, and which collects, from the raw material fed to the evaporator, the liquid raw material that is not vaporized and the liquid raw material comprising a part of the vaporized raw material that is liquefied, and
a discharge piping through which the liquid raw material collected by the collecting section is discharged to outside the cylindrical part.
14 . The method for producing N-vinylacetamide according to claim 9 , wherein the superheated vaporized raw material is fed through the raw material collection device to the thermal decomposition reactor.