IP Library Granted Patent US 12,157,725
Granted Patent B2
US 12,157,725 · App. 17/893,399 · Granted Dec 3, 2024

Conducting reactions in Leidenfrost-levitated droplets

Inventors: Robert Graham Cooks (West Lafayette, IN); Christopher Pulliam (West Lafayette, IN); Ryan M. Bain (West Lafayette, IN)
Assignee: Purdue Research Foundation
C07D213/04C07C45/72C07D209/40C07J41/0005
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,157,725
App. No.
17/893,399
Granted
Dec 3, 2024
Kind
B2
Abstract

The invention generally relates to conducting reactions in Leidenfrost-levitated droplets.

Claims (12)

1. A method for forming a reaction product, the method comprising conducting multiple reactions in multiple separate Leidenfrost-levitated droplets while maintaining a substantially constant volume of each of the multiple separate Leidenfrost-levitated droplets; and

merging the multiple separate Leidenfrost-levitated droplets into a single common Leidenfrost-levitated droplet, thereby forming a reaction product within the single common Leidenfrost-levitated droplet.

2. The method of claim 1 , further comprising collecting the reaction product in the single common Leidenfrost-levitated droplet without evaporating the single common Leidenfrost-levitated droplet.

3. The method according to claim 2 , further comprising analyzing the reaction product.

4. The method according to claim 3 , wherein analyzing is by a mass spectrometry technique.

5. The method according to claim 3 , wherein maintaining the substantially constant volume comprises introducing droplets of a pure solvent or a respective reaction mixture to each of the multiple separate Leidenfrost-levitated droplets.

6. The method according to claim 5 , wherein a rate at which the droplets of the pure solvent or the respective reaction mixture are introduced to each of the multiple separate Leidenfrost-levitated droplets is dependent on an evaporation rate of each of the multiple separate Leidenfrost-levitated droplets.

7. The method according to claim 1 , wherein the multiple reactions are the same.

8. The method according to claim 1 , wherein the multiple reactions are different.

9. The method according to claim 1 , wherein the method is conducted without the use of surfactants.

10. The method according to claim 1 , wherein the multiple separate Leidenfrost-levitated droplets are maintained separately by physical barriers between the multiple separate Leidenfrost-levitated droplets.

11. The method according to claim 10 , wherein the multiple separate Leidenfrost-levitated droplets are merged by removing the physical barriers between the multiple separate Leidenfrost-levitated droplets.

Assignments (2)
CONFIRMATORY LICENSE Recorded May 30, 2023
From: PURDUE UNIVERSITY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 063802/0942 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 23, 2022
From: COOKS, ROBERT GRAHAM; PULLIAM, CHRISTOPHER; BAIN, RYAN M.
To: PURDUE RESEARCH FOUNDATION
Reel/Frame 061864/0689 →
Continuity (5)
Continuation 16993553 · Aug 14, 2020
Continuation 15613520 · Jun 5, 2017
Provisional Application 62346594 · Jun 7, 2016
Provisional Application 62346213 · Jun 6, 2016
Related Publication 20220411373A1 · Dec 29, 2022