IP Library › Granted Patent US 12,622,164
Granted Patent B2
US 12,622,164 · App. 18/023,824 · Granted May 5, 2026

Foldable substrates and methods of making

Inventors: Douglas Clippinger Allan (Corning, NY); Matthew John Dejneka (Corning, NY); Yuhui Jin (Painted Post, NY); Xinghua Li (Horseheads, NY); Yousef Kayed Qaroush (Painted Post, NY); Tingge Xu (Santa Clara, CA)
Assignee: CORNING INCORPORATED
H10K77/111H10K2102/311H10K2102/351
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12,622,164
App. No.
18/023,824
Granted
May 5, 2026
Kind
B2
Abstract

Foldable substrates comprise a first outer layer comprising a first major surface, a second outer layer comprising a second major surface, and a core layer positioned therebetween. The core layer may comprise a first central surface area positioned between a first portion and a second portion of the first outer layer, and the core layer comprising a second central surface area positioned between a third portion and fourth portion of the second outer layer. Some foldable substrates comprise a first portion comprising a first depth of compression, a first depth of layer, and a first average concentration. The central portion may comprise a first central depth of compression, a first central depth of layer, and a central average concentration. Methods comprise chemically strengthening a foldable substrate. Some methods comprise etching the foldable substrate and then further chemically strengthening the foldable substrate.

Claims (19)

1 . A foldable substrate comprises:

a substrate thickness defined between a first major surface and a second major surface opposite the first major surface, the substrate thickness is in a range from about 100 micrometers to about 2 millimeters;

a first portion comprising the substrate thickness, the first portion comprises a first average concentration of potassium on an oxide basis, a first compressive stress region extending to a first depth of compression from the first major surface, a second compressive stress region extending to a second depth of compression from the second major surface;

a second portion comprising the substrate thickness, the second portion comprises a second average concentration of potassium on an oxide basis, a third compressive stress region extending to a third depth of compression from the first major surface, a fourth compressive stress region extending to a fourth depth of compression from the second major surface;

a central portion positioned between the first portion and the second portion, the central portion comprises a central thickness defined between a first central surface area and a second central surface area opposite the first central surface area, a central average concentration of potassium on an oxide basis, a first central compressive stress region extending to a first central depth of compression from the first central surface area, the central portion further comprises a second central compressive stress region extending to a second central depth of compression from the second central surface area, wherein the central thickness is in a range from about 25 micrometers to about 80 micrometers, wherein the first central surface area is recessed from the first major surface by a first distance, and an absolute difference between the first average concentration of potassium and the central average concentration of potassium is about 100 parts per million or less.

2 . The foldable substrate of claim 1 , wherein an absolute difference between the first depth of compression as a percentage of the substrate thickness and the first central depth of compression as a percentage of the central thickness is about 1% or less.

3 . The foldable substrate of claim 1 , wherein the substrate thickness is in a range from about 125 micrometers to about 200 micrometers.

4 . The foldable substrate of claim 1 , wherein the second central surface area is recessed from the second major surface by a second distance.

5 . The foldable substrate of claim 4 , wherein the second distance is from about 5% to about 20% of the substrate thickness.

6 . The foldable substrate of claim 4 , wherein the first distance is substantially equal to the second distance.

7 . The foldable substrate of any one of claim 1 , wherein the first compressive stress region comprises a first maximum compressive stress of about 700 MegaPascals or more; the second compressive stress region comprises a second maximum compressive stress; the third compressive stress region comprises a third maximum compressive stress of about 700 MegaPascals or more; the fourth compressive stress region comprises a fourth maximum compressive stress; the first central compressive stress region comprises a first central maximum compressive stress of about 700 MegaPascals or more; the second central compressive stress region comprises a second central maximum compressive stress.

8 . The foldable substrate of claim 1 , further comprising a first tensile stress region of the first portion positioned between the first compressive stress region and the second compressive stress region; the first tensile stress region comprises a first maximum tensile stress; the foldable substrate comprises a second tensile stress region of the second portion positioned between the third compressive stress region and the fourth compressive stress region; the second tensile stress region comprises a second maximum tensile stress; the foldable substrate comprises a central tensile stress region of the central portion positioned between the first central compressive stress region and a second central compressive stress region; the central tensile stress region comprises a central maximum tensile stress; an absolute difference between the central maximum tensile stress and the first maximum tensile stress is about 10 MegaPascals or less.

9 . The foldable substrate of claim 1 , wherein the central portion further comprises a central tensile stress region of the central portion positioned between a portion of the first central surface area and a portion of the second central surface area; the central tensile stress region comprising a central maximum tensile stress; the central portion comprises a first transition portion attaching the first central major surface to the first portion; the first transition portion comprising a first transition tensile stress region comprising a first transition maximum tensile stress; the central portion comprises a second transition portion attaching the first central major surface to the second portion; the second transition portion comprising a second transition tensile stress region comprising a second transition maximum tensile stress; the first transition maximum tensile stress is greater than the central maximum tensile stress.

10 . The foldable substrate of claim 9 , wherein the second transition maximum tensile stress is greater than the central maximum tensile stress.

11 . The foldable substrate of any one of claims 1-10 , wherein the first distance is about 20% to about 45% of the substrate thickness.

12 . The foldable substrate of claim 1 , wherein the substrate achieves an effective bend radius of 5 millimeters.

13 . A foldable apparatus comprising the foldable substrate of claim 1 , the foldable apparatus further comprises an adhesive comprising a first contact surface and a second contact surface opposite the first contact surface, wherein at least a portion of the adhesive is positioned in a recess defined between the second central surface area and a second plane defined by the second major surface.

14 . A foldable apparatus comprises the foldable substrate of claim 1 , the foldable apparatus further comprises a polymer-based portion positioned in a recess defined between the second central surface area and a second plane defined by the second major surface, wherein the foldable apparatus comprises an adhesive comprising a first contact surface and a second contact surface opposite the first contact surface.

15 . The foldable apparatus of claim 14 , wherein the polymer-based portion comprises a strain at yield in a range from about 5% to about 10%, and wherein a magnitude of a difference between an index of refraction of the foldable substrate and an index of refraction of the polymer-based portion is about 0.1 or less.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2023
From: ALLAN, DOUGLAS CLIPPINGER; DEJNEKA, MATTHEW JOHN; JIN, YUHUI; LI, XINGHUA; QAROUSH, YOUSEF KAYED; XU, TINGGE
To: CORNING INCORPORATED
Reel/Frame 062824/0832 →
Continuity (1)
Related Publication 20230309368A1 · Sep 28, 2023
References Cited (43)
US 9321677B2 · Chang · 2016 [cited by examiner]
US 9578150B2 · Xie et al. · 2017 [cited by applicant]
US 9779190B2 · Ahmed et al. · 2017 [cited by applicant]
US 10545537B2 · Ahn et al. · 2020 [cited by applicant]
US 20100167059A1 · Hashimoto et al. · 2010 [cited by applicant]
US 20150043174A1 · Han · 2015 [cited by examiner]
US 20150110990A1 · Chou et al. · 2015 [cited by applicant]
US 20150210588A1 · Chang · 2015 [cited by examiner]
US 20150210589A1 · Chang et al. · 2015 [cited by applicant]
US 20150227172A1 · Namkung et al. · 2015 [cited by applicant]
US 20160214889A1 · Garner et al. · 2016 [cited by applicant]
US 20160224069A1 · Chang et al. · 2016 [cited by applicant]
US 20170309843A1 · Kim · 2017 [cited by applicant]
US 20180009706A1 · Luo et al. · 2018 [cited by applicant]
US 20180224894A1 · Namkung et al. · 2018 [cited by applicant]
US 20190106353A1 · Rai et al. · 2019 [cited by applicant]
US 20190161401A1 · Kuang et al. · 2019 [cited by applicant]
US 20200006683A1 · Kim · 2020 [cited by applicant]
US 20200264669A1 · Namkung · 2020 [cited by examiner]
US 20210107251A1 · Chen et al. · 2021 [cited by applicant]
US 20210107829A1 · Chen et al. · 2021 [cited by applicant]
US 20210230057A1 · Kuang et al. · 2021 [cited by applicant]
US 20220212446A1 · Harris et al. · 2022 [cited by applicant]
US 20220274871A1 · Allan et al. · 2022 [cited by applicant]
US 20220291712A1 · Baby et al. · 2022 [cited by applicant]
CN 104347000A · 2015 [cited by applicant]
CN 104724917A · 2015 [cited by applicant]
CN 104835415A · 2015 [cited by applicant]
CN 107305906A · 2017 [cited by applicant]
CN 108328939A · 2018 [cited by applicant]
CN 111433167A · 2020 [cited by applicant]
GB 1253284A · 1971 [cited by applicant]
KR 1020160058792A · 2016 [cited by applicant]
KR 102068685B1 · 2020 [cited by applicant]
KR 102068729B1 · 2020 [cited by applicant]
KR 102069040B1 · 2020 [cited by applicant]
Chinese Patent Application No. 202080106831.0 , Office Action dated May 31, 2024, 5 pages (English Translation only), Chinese Patent Office. [cited by applicant]
International Search Report and Written Opinion of the International Searching Authority; PCT/US2020/048492 Mailed on May 21, 2021, 16 pages; European Patent Office. [cited by applicant]
Sun et al., “A Study On Ion-Exchanged, Soda-Lime Glass's Residual Stress Relationship With K+/Na+ Concentration”, Int. J. Appl Glass Sci., vol. 11, 2020, pp. 134-146. [cited by applicant]
Tandia et al., “Elasticity of Ion Stuffing in Chemically Strengthened Glass”, Journal of Non-Crystalline Solids, vol. 358, 2012, pp. 1569-1574. [cited by applicant]
Chinese Patent Application No. 202080106831.0, Office Action dated Mar. 7, 2025, 5 pages (English Translation only), Chinese Patent Office. [cited by applicant]
Korean Patent Application No. 10-2023-7010332, Notice of Allowance dated Aug. 28, 2025, 3 pages (English Translation only), Korean Patent Office. [cited by applicant]
Li et al., “China Die & Mould Design Canon”, Design of Moulds for Light Industry, vol. 2, 2003, 8 pages (2 pages of English Translation and 6 pages of Original Document). [cited by applicant]