IP Library Granted Patent US 12,049,577
Granted Patent B2
US 12,049,577 · App. 18/063,355 · Granted Jul 30, 2024

Dielectric substrate and method of forming the same

Inventors: Jennifer Adamchuk (Marlborough, MA); Dale Thomas (Rochdale, GB); Meghann White (Bedford, NH); Sethumadhavan Ravichandran (Shrewsbury, MA); Gerard T. Buss (Bedford, NH)
Assignee: VERSIV COMPOSITES LIMITED
C09J7/245B32B7/12B32B15/08B32B15/20B32B27/20B32B27/281C09J7/381C09J11/04H05K1/0373H05K1/09B32B2255/10B32B2255/26B32B2264/1021B32B2307/204B32B2307/732B32B2457/08C09J2203/326C09J2301/41C09J2400/166C09J2427/00C09J2427/006H05K2201/0209
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Quick Facts
Patent No.
US 12,049,577
App. No.
18/063,355
Granted
Jul 30, 2024
Kind
B2
Abstract

The present disclosure relates to a dielectric substrate that may include a polymer based core film, and a fluoropolymer based adhesive layer. The polymer based core film may include a resin matrix component, and a ceramic filler component. The ceramic filler component may include a first filler material. The particle size distribution of the first filler material may have a D 10 of at least about 1.0 microns and not greater than about 1.7, a D 50 of at least about 1.0 microns and not greater than about 3.5 microns, and a D 90 of at least about 2.7 microns and not greater than about 6 microns.

Claims (20)

1. A dielectric substrate comprising: a polymer based core film, and a fluoropolymer based adhesive layer, wherein the polymer based core film comprises: a resin matrix component; and a ceramic filler component, wherein the ceramic filler component comprises a first filler material, wherein the first filler material further comprises a mean particle size of not greater than about 10 microns, and a particle size distribution span (PSDS) of not greater than about 5, where PSDS is equal to (D 90 −D 10 )/D 50 , where D 90 is equal to a D 90 particle size distribution measurement of the first filler material, D 10 is equal to a D 10 particle size distribution measurement of the first filler material, and D 50 is equal to a D 50 particle size distribution measurement of the first filler material.

2. The dielectric substrate of claim 1 , wherein the first filler material comprises a mean particle size of not greater than about 10 microns.

3. The dielectric substrate of claim 1 , wherein the first filler material further comprises an average surface area of not greater than about 8 m 2 /g.

4. The dielectric substrate of claim 1 , wherein the fluoropolymer based adhesive layer has an average thickness of at least about 0.2 microns.

5. The dielectric substrate of claim 1 , wherein the fluoropolymer based adhesive layer has an average thickness of not greater than about 7 microns.

6. The dielectric substrate of claim 1 , wherein the fluoropolymer based adhesive layer comprises fluoropolymers (e.g., polytetrafluoroethylene (PTFE), modified polytetrafluoroethylene (mPTFE), co- and terpolymers of tetrafluoroethylene such as fluorinated ethylene-propylene (FEP), perfluoroalkoxy polymer resin (PFA), and modified perfluoroalkoxy polymer resin (mPFA), and derivatives and blends thereof.

7. The dielectric substrate of claim 1 , wherein the fluoropolymer based adhesive layer is a PFA layer.

8. The dielectric substrate of claim 1 , wherein the first filler material comprises a silica based compound.

9. The dielectric substrate of claim 1 , wherein the first filler material comprises silica.

10. The dielectric substrate of claim 1 , wherein the resin matrix comprises a perfluoropolymer.

11. The dielectric substrate of claim 10 , wherein the perfluoropolymer comprises a copolymer of tetrafluoroethylene (TFE); a copolymer of hexafluoropropylene (HFP); a terpolymer of tetrafluoroethylene (TFE); or any combination thereof.

12. The dielectric substrate of claim 10 , wherein the perfluoropolymer comprises polytetrafluoroethylene (PTFE), perfluoroalkoxy polymer resin (PFA), fluorinated ethylene propylene (FEP), or any combination thereof.

13. The dielectric substrate of claim 1 , wherein the content of the resin matrix component is at least about 45 vol. % and not greater than about 63 vol. % for a total volume of the polymer based core film.

14. The dielectric substrate of claim 10 , wherein the content of the perfluoropolymer is at least about 45 vol. % and not greater than about 63 vol. % for a total volume of the polymer based core film.

15. The dielectric substrate of claim 1 , wherein the content of the ceramic filler component is at least about 45 vol. % and not greater than about 57 vol. % for a total volume of the polymer based core film.

16. The dielectric substrate of claim 1 , wherein the content of the first filler material is at least about 80 vol. % and not greater than about 100 vol. % for a total volume of the ceramic filler component.

17. The dielectric substrate of claim 1 , wherein the ceramic filler component further comprises a second filler material.

18. The dielectric substrate of claim 17 , wherein the second filler material comprises a high dielectric constant ceramic material.

19. The dielectric substrate of claim 18 , wherein the high dielectric constant ceramic material has a dielectric constant of at least about 14.

20. A copper-clad laminate comprising: a copper foil layer, and a dielectric substrate overlying the copper foil layer, wherein the dielectric substrate comprises: a polymer based core film, and a fluoropolymer based adhesive layer, wherein the polymer based core film comprises: a resin matrix component; and a ceramic filler component, wherein the ceramic filler component comprises a first filler material, wherein the first filler material further comprises a mean particle size of at not greater than about 10 microns, and a particle size distribution span (PSDS) of not greater than about 5, where PSDS is equal to (D 90 −D 10 )/D 50 , where D 90 is equal to a D 90 particle size distribution measurement of the first filler material, D 10 is equal to a D 10 particle size distribution measurement of the first filler material, and D 50 is equal to a D 50 particle size distribution measurement of the first filler material.

Assignments (3)
CHANGE OF NAME Recorded May 10, 2024
From: SAINT-GOBAIN PERFORMANCE PLASTICS IRELAND LIMITED
To: VERSIV COMPOSITES LIMITED
Reel/Frame 067380/0904 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 24, 2024
From: ADAMCHUK, JENNIFER; THOMAS, DALE; WHITE, MEGHANN; RAVICHANDRAN, SETHUMADHAVAN; BUSS, GERARD T.
To: SAINT-GOBAIN PERFORMANCE PLASTICS CORPORATION
Reel/Frame 067210/0373 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 11, 2024
From: SAINT-GOBAIN PERFORMANCE PLASTICS CORPORATION
To: SAINT-GOBAIN PERFORMANCE PLASTICS IRELAND LIMITED
Reel/Frame 067098/0001 →
Continuity (3)
Continuation 17643446 · Dec 9, 2021
Provisional Application 63126105 · Dec 16, 2020
Related Publication 20230111961A1 · Apr 13, 2023