IP Library Granted Patent US 11,993,745
Granted Patent B2
US 11,993,745 · App. 18/105,013 · Granted May 28, 2024

Nanoparticle carrier platform and methods for controlled release of subterranean well treatment additives

Inventors: Chao Yan (Sugar Land, TX); Ross Tomson (Houston, TX); Paula Guraieb (Houston, TX); Nasser Ghorbani (The Woodlands, TX)
Assignee: CHAMPIONX LLC
C09K8/536B01J20/08B01J20/28004B01J20/28007B01J20/28016B01J20/3085C09K8/03C09K8/58C09K8/50C09K8/524C09K8/528C09K2208/10C09K2208/20C09K2208/22C09K2208/26C09K2208/28C09K2208/32
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Quick Facts
Patent No.
US 11,993,745
App. No.
18/105,013
Granted
May 28, 2024
Kind
B2
Abstract

Nano-sized mixed metal oxide carriers capable of delivering a well treatment additive for a sustained or extended period of time in the environment of use, methods of making the nanoparticles, and uses thereof are described herein. The nanoparticles can have a formula of: A/[M x 1 M y 2 M z 3 ]O n H m where x is 0.03 to 3, y is 0.01 to 0.4, z is 0.01 to 0.4 and n and m are determined by the oxidation states of the other elements, and M 1 can be aluminum (Al), gallium (Ga), indium (In), or thallium (Tl). M 2 and M 3 are not the same and can be a Column 2 metal, Column 14 metal, or a transition metal. A is can be a treatment additive.

Claims (33)

1. A mixed metal oxide nanoparticle comprising:

M x 1 O n H m ;

M y 2 O n H m ; and

M z 3 O n H m ,

where

M 1 , M 2 , and M 3 are each in the crystal lattice structure of the nanoparticle,

M 1 is a Column 13 element selected from aluminum (Al), gallium (Ga), indium (In), and thallium (Tl),

M 2 and M 3 are each individually a Column 2 metal, a Column 14 metal, or a transition metal, with the proviso that M 2 and M 3 are different,

x is 0.03 to 3, y is 0.01 to 0.40, and z is 0 to 0.40, and

n and m for each of M x 1 O n H m , M y 2 O n H m , and M z 3 O n H m is individually determined by the oxidation states of the metals M 1 , M 2 , and M 3 .

2. The mixed metal oxide nanoparticle of claim 1 , wherein M 2 and M 3 are each independently beryllium (Be), magnesium (Mg), calcium (Ca), strontium (Sr), barium (Ba) and radium (Ra).

3. The mixed metal oxide nanoparticle of claim 1 , wherein M 1 is Al, M 2 is Mg, and M 3 is calcium (Ca).

4. The mixed metal oxide nanoparticle of claim 1 , wherein the nanoparticle has a diameter of 1 nm to 10,000 nm.

5. The mixed metal oxide nanoparticle of claim 4 , wherein the nanoparticle has a diameter of 10 nm to 1000 nm.

6. The mixed metal oxide nanoparticle of claim 5 , wherein the nanoparticle has a diameter of 10 nm to 200 nm.

7. The mixed metal oxide nanoparticle of claim 1 , wherein the nanoparticle further comprises an additive.

8. The mixed metal oxide nanoparticle of claim 7 , wherein the additive is capable of being released from the nanoparticle in a controlled manner over an extended period of time.

9. The mixed metal oxide nanoparticle of claim 7 , wherein the well treatment additive is chemically bound to the nanoparticle through an ionic bond, a covalent bond, a hydrogen bond, a Van der Walls interaction, or by adsorption onto the particle.

10. The mixed metal oxide nanoparticle of claim 7 , wherein the nanoparticle is impregnated with the additive.

11. The mixed metal oxide nanoparticle of claim 7 , wherein the nanoparticle further comprises a coating, and wherein the additive is comprised in the coating.

12. The mixed metal nanoparticle of claim 7 , wherein the additive is a scale inhibitor, a hydrate inhibitor, a clay stabilizer, a bactericide, a salt substitute, a relative permeability modifier, a sulfide scavenger, a corrosion inhibitor, a corrosion inhibitor intensifier, a pH control additive, a surfactant, a breaker, a fluid loss control additive, an asphaltene inhibitor, a paraffin inhibitor, a chelating agent, a foamer, a defoamer, an emulsifier, a demulsifier, an iron control agent, a solvent, or a friction reducer, or any combination thereof.

13. The mixed metal oxide nanoparticle of claim 12 , wherein the additive is a scale inhibitor.

14. The nanoparticle of claim 13 , wherein the scale inhibitor is an organic molecule having a carboxylic acid, a polycarboxylic acid, aspartic acid, maleic acid, sulfonic acid, phosphonic acid, or a phosphate ester group or salts thereof.

15. The nanoparticle of claim 14 , wherein the scale inhibitor is a polymer comprising sulfonated polycarboxylic acid functionality.

16. The mixed metal oxide nanoparticle of claim 12 , wherein the additive is an asphaltene inhibitor.

17. The mixed metal oxide of claim 7 , wherein the additive is a subterranean treatment additive.

18. The mixed metal oxide nanoparticle of claim 17 , wherein the additive is a well treatment additive.

19. The mixed metal oxide nanoparticle of claim 1 , wherein the nanoparticle comprises at least two additives, and wherein the at least two additives are different from each other.

20. A composition comprising a plurality of the nanoparticles of claim 1 .

21. The composition of claim 20 , wherein the composition is a fluid.

22. The composition of claim 20 , wherein the composition is an aqueous liquid, and wherein the plurality of nanoparticles are suspended within the aqueous liquid.

23. The composition of claim 20 , further comprising water.

24. The mixed metal oxide nanoparticle of claim 1 , wherein z is 0.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 3, 2023
From: YAN, CHAO; TOMSON, ROSS; GURAIEB, PAULA; GHORBANI, NASSER
To: TOMSON TECHNOLOGIES LLC
Reel/Frame 062579/0690 →
MERGER Recorded Feb 3, 2023
From: TOMSON TECHNOLOGIES LLC
To: CHAMPIONX LLC
Reel/Frame 062579/0737 →
Continuity (6)
Continuation 17317732 · May 11, 2021
Continuation 16811128 · Mar 6, 2020
Continuation 15897250 · Feb 15, 2018
Division 15593603 · May 12, 2017
Provisional Application 62345568 · Jun 3, 2016
Related Publication 20230374369A1 · Nov 23, 2023