IP Library Granted Patent US 12,109,737
Granted Patent B2
US 12,109,737 · App. 18/139,335 · Granted Oct 8, 2024

Nanostructures from laser-ablated nanohole templates

Inventors: William Hudson Hofmeister (Nashville, TN); Alexander Yuryevich Terekhov (Murfreesboro, TN); Jose Lino Vasconcelos da Costa (Tullahoma, TN); Kathleen Stacia Lansford (Manchester, TN); Deepak Rajput (Tullahoma, TN); Lloyd M. Davis (Tullahoma, TN)
Assignee: ULTRA SMALL FIBERS, LLC
B29C41/003B29C33/3842B29C41/02B29C41/38B29C41/42B82Y10/00B82Y40/00C08B3/06C08B5/02C08F110/02C08F120/18C08F120/40C08G63/08C08G63/664C08G77/04G03F7/0002B29K2001/12B29K2001/18B29K2023/06B29K2031/04B29K2033/12B29K2067/04B29K2071/00B29K2083/00B29K2901/10B29K2901/12B29K2907/045B29K2909/00B29K2909/08B29K2909/14B29K2995/0026B29K2995/0094B29L2031/7562Y02P20/582Y10T428/24355Y10T428/24802
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Quick Facts
Patent No.
US 12,109,737
App. No.
18/139,335
Granted
Oct 8, 2024
Kind
B2
Abstract

Solution casting a nanostructure. Preparing a template by ablating nanoholes in a substrate using single-femtosecond laser machining. Replicating the nanoholes by applying a solution of a polymer and a solvent into the template. After the solvent has substantially dissipated, removing the replica from the substrate.

Claims (24)

1. A method for fabricating a nanofiber array, comprising:

providing a mold comprising a surface in which is formed a plurality of nanoholes [,] wherein each nanohole of the plurality is laser-ablated in the surface of the mold;

applying a flowable polymer into the plurality of nanoholes; and

extracting an array of polymer nanofibers from the mold.

2. The method of claim 1 , wherein the nanofibers are not hollow or porous.

3. The method of claim 1 , wherein the nanofibers have an aspect ratio of at least ten-to-one.

4. The method of claim 1 , wherein the nanofibers have a diameter of less than 1000 nanometers.

5. The method of claim 1 , wherein the nanofibers have an aspect ratio of at least ten-to-one and a diameter of less than 1000 nanometers.

6. The method of claim 1 , wherein:

the mold comprises a transparent substrate; and

the surface in which the plurality of nanoholes is formed is on the transparent substrate.

7. The method of claim 1 , wherein the flowable polymer is a polymer solution.

8. The method of claim 1 , wherein the array of polymer nanofibers comprises a plurality of freestanding polymer nanofibers extending from a surface of a polymer substrate.

9. The method of claim 8 , wherein the polymer nanofibers are positioned on the polymer substrate in a non-random, user-defined pattern.

10. The method of claim 1 , wherein said extracting is lifting or peeling the array of polymer nanofibers away from the surface of the mold.

11. The method of claim 1 , wherein applying a flowable polymer into the plurality of nanoholes comprises applying the flowable polymer into the nanoholes until the flowable polymer covers at least a portion of the surface of the mold and connects at least some of the plurality of nanoholes.

12. The method of claim 1 , wherein extracting an array of polymer nanofibers from the mold comprises allowing the flowable polymer to form a continuous film on a portion of the surface of the mold and removing the continuous film from the surface of the mold.

13. The method of claim 1 , wherein:

the flowable polymer includes a polymer capable of forming a continuous film; and

the flowable polymer overflows the plurality of nanoholes and covers at least a portion of the surface of the mold such that the flowable polymer connects at least some of the plurality of nanoholes and forms the continuous film on the portion of the surface of the mold.

14. A method for fabricating a nanofiber array, comprising:

providing a mold comprising a transparent substrate having a surface in which a plurality of nanoholes is laser-ablated;

applying a flowable polymer into the plurality of nanoholes; and

extracting an array of polymer nanofibers from the mold.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 26, 2024
From: HOFMEISTER, WILLIAM HUDSON; TEREKHOV, ALEXANDER YURYEVICH; DA COSTA, JOSE LINO VASCONCELOS; LANSFORD, KATHLEEN STACIA; RAJPUT, DEEPAK; DAVIS, LLOYD M.
To: UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION
Reel/Frame 068096/0871 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 26, 2024
From: UNIVERSITY OF TENNESSEE RESEARCH FOUNDATION
To: ULTRA SMALL FIBERS, LLC
Reel/Frame 068097/0032 →
Continuity (5)
Continuation 17492862 · Oct 4, 2021
Continuation 14560833 · Dec 4, 2014
Continuation 13769575 · Feb 18, 2013
Provisional Application 61599926 · Feb 16, 2012
Related Publication 20230405885A1 · Dec 21, 2023