IP Library › Granted Patent US 12,540,377
Granted Patent B2
US 12,540,377 · App. 18/163,859 · Granted Feb 3, 2026

Rare earth aluminum alloy powder applicable for additive manufacturing and preparation method thereof

Inventors: Haiyan Gao (Shanghai, CN); Haiyang Lv (Shanghai, CN); Mengmeng Wang (Shanghai, CN); Peng Peng (Shanghai, CN); Yun Wu (Shanghai, CN); Chi Zhang (Shanghai, CN); Min Li (Shanghai, CN); Yufei Wang (Shanghai, CN); Jun Wang (Shanghai, CN); Baode Sun (Shanghai, CN)
Assignee: SHANGHAI JIAO TONG UNIVERSITY
C22C21/00B22F1/05B22F1/065B22F9/082B33Y70/00C22C1/026C22C1/0416C22C21/06B22F2009/0824B22F10/28B22F2301/052B22F2304/10
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Quick Facts
Patent No.
US 12,540,377
App. No.
18/163,859
Granted
Feb 3, 2026
Kind
B2
Abstract

A method for preparing a rare earth aluminum alloy powder applicable for additive manufacturing includes: heating and melting aluminum ingots into an aluminum melt; adding required alloy elements to the aluminum melt to obtain an alloy melt in which the alloy elements are present in the following preset percentages by weight: 1.00% to 10.00% of Ce, 0.05% to 8.00% of Mg, 0.10% to 7.50% of Y, 0.10% to 2.50% of Zr, less than 0.1% of impurities, and the balance aluminum; leading out the alloy melt through a fluid guiding pipe, and impacting the alloy melt with a high-pressure gas flow so that the alloy melt is atomized into fine droplets under an action of surface tension, and solidified into spherical alloy powder; and collecting the spherical alloy powder in a vacuum collector, and screening and drying the spherical alloy powder to obtain the rare earth aluminum alloy powder.

Claims (11)

1 . A method for preparing a rare earth aluminum alloy powder applicable for additive manufacturing, comprising the following steps:

S1, heating and melting aluminum ingots into an aluminum melt at a temperature of 730° C. to 780° C. in presence of a protective atmosphere;

S2, adding required alloy elements to the aluminum melt to obtain an alloy melt: adjusting a proportion of each element with an intermediate alloy, and performing degassing and deslagging so that the alloy elements are present in the following preset percentages by weight: 6.00% to 8.00% of Ce, 0.40% to 1.00% of Mg, 0.10% to 0.25% of Y, 0.10% to 0.25% of Zr, less than 0.1% of impurities, and the balance being aluminum;

S3, leading out the alloy melt through a fluid guiding pipe, and impacting the alloy melt with a gas flow at an outlet of the fluid guiding pipe, so that the alloy melt is atomized into fine droplets under an action of surface tension, and solidified into spherical alloy powder; and

S4, collecting the spherical alloy powder in a vacuum collector, and screening and drying the spherical alloy powder to obtain the rare earth aluminum alloy powder applicable for additive manufacturing.

2 . The method according to claim 1 , wherein in step S3 of leading out the alloy melt through the fluid guiding pipe,

a lead-out temperature of the alloy melt is controlled between 630° C. and 680° C.;

a lead-out velocity of the alloy melt is between 5 kg/min and 10 kg/min;

the fluid guiding pipe is made of zirconium oxide, silicon nitride or titanium nitride; a diameter of the fluid guiding pipe is 2 mm to 6 mm.

3 . The method according to claim 1 , wherein in step S3, the alloy melt is impacted with a high-pressure argon flow or a high-pressure nitrogen flow at a pressure of 6 MPa to 8 MPa.

4 . The method according to claim 1 , wherein the spherical alloy powder has an average particle size of 40 μm to 50 μm and a particle size distribution of 10 μm to 75 μm.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 4, 2023
From: GAO, HAIYAN; LV, HAIYANG; WANG, MENGMENG; PENG, PENG; WU, YUN; ZHANG, CHI; LI, MIN; WANG, YUFEI; WANG, JUN; SUN, BAODE
To: SHANGHAI JIAO TONG UNIVERSITY
Reel/Frame 065757/0087 →
Priority Claims (1)
CN 202011605054.2 · Dec 30, 2020 · national
Continuity (2)
Continuation PCTCN2021114279 · Aug 24, 2021
Related Publication 20230175102A1 · Jun 8, 2023
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