IP Library › Granted Patent US 12,355,083
Granted Patent B2
US 12,355,083 · App. 18/218,397 · Granted Jul 8, 2025

Conducting coatings for anodes, methods of making and using same, and uses thereof

Inventors: Lynden A. Archer (Ithaca, NY); Jingxu Zheng (Shenzen, CN); Tian Tang (Nanchang, CN); Qing Zhao (Tianjin, CN)
Assignee: Cornell University
H01M4/625H01M4/0452H01M4/134H01M2004/027H01M10/0525H01M10/054
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Quick Facts
Patent No.
US 12,355,083
App. No.
18/218,397
Granted
Jul 8, 2025
Kind
B2
Abstract

Conducting coatings disposed on a metal member. The conducting coatings may have a desired texture and provide homoepitaxial or heteroepitaxial coating of an electrodeposited layer. A conducting coating may be formed by applying a shear force during deposition of the conducting coating. The conducting coatings may be used in anodes of various electrochemical devices. A conducting coating, which may be part of an electrochemical device, may have an electrochemically deposited layer disposed on at least a portion of a surface of the conducting coating. The electrochemically deposited layer may be reversibly electrochemically deposited.

Claims (24)

1. An electrode comprising:

an epitaxial substrate;

an electrodeposited layer disposed on at least a portion of the epitaxial substrate, and a coherent interface having a lattice misfit of less than 15% between the epitaxial substrate and the electrodeposited layer, and wherein:

i) the epitaxial substrate comprises graphene, functionalized graphene, or reduced graphene oxide and the electrodeposited layer comprises Zn;

ii) the epitaxial substrate comprises Au and the electrodeposited layer comprises Al; or

iii) the epitaxial substrate comprises Zr or Ti and the electrodeposited layer comprises Mg.

2. The electrode of claim 1 , wherein the epitaxial substrate comprises an epitaxial templating material chosen from a conducting coating, an FCC metal, an HCP metal, a BCC metal, or any combination thereof, and wherein the epitaxial templating material is chemically inert and/or electrochemically stable under electrochemical cycling conditions.

3. The electrode of claim 1 , wherein the epitaxial substrate comprises a metal member and a conducting coating comprising graphene, functionalized graphene, reduced graphene, Au, Zr, or Ti disposed on at least a portion of the metal member.

4. The electrode of claim 3 , wherein the conducting coating comprises graphene, functionalized graphene, or reduced graphene oxide and the electrodeposited layer comprises Zn.

5. The electrode of claim 1 , wherein the epitaxial substrate comprises Au and the electrodeposited layer comprises Al.

6. The electrode of claim 1 , wherein the epitaxial substrate comprises Zr or Ti and the electrodeposited layer comprises Mg.

7. The electrode of claim 3 , wherein the conducting coating comprises Au and the electrodeposited layer comprises Al.

8. The electrode of claim 3 , wherein the conducting coating comprises Zr or Ti, and the electrodeposited layer comprises Mg.

9. The electrode of claim 1 , wherein the epitaxial substrate comprises a substrate and an aligned coating of a plurality of graphene sheets on at least a portion of the substrate and wherein the graphene sheets are parallel to the substrate.

10. The electrode of claim 1 , wherein the electrodeposited layer comprises an FCC metal selected from Al; or an HCP metal selected from Mg and Zn.

11. The electrode of claim 1 , wherein the coherent interface has a lattice misfit of less than about 10% between the epitaxial substrate and the electrodeposited layer.

12. The electrode of claim 1 , wherein the coherent interface has a lattice misfit of less than about 5% between the epitaxial substrate and the electrodeposited layer.

13. A device comprising one or more electrode(s) of claim 1 .

14. The device of claim 13 , wherein the device is a battery, a supercapacitor, a fuel cell, an electrolyzer, an electrolytic cell, or an electrochemical device.

15. The device of claim 13 , wherein the device is a battery and the battery exhibits one or more of the following:

i). at least 1,000 charging/discharging cycles without failure;

ii). a plating and/or stripping Coulombic efficiency of 95% or greater for at least 1,000 cycles at a rate of 40 mA/cm2 or greater; and/or

iii). at least 1,000 charging/discharging cycles with a Coulombic efficiency of 90% or greater.

16. The electrode of claim 1 , wherein the epitaxial substrate comprises graphene, functionalized graphene, or reduced graphene oxide and the electrodeposited layer comprises Zn.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 15, 2024
From: ARCHER, LYNDEN A.; ZHENG, JINGXU; TANG, TIAN; ZHAO, QING
To: CORNELL UNIVERSITY
Reel/Frame 068902/0238 →
Continuity (3)
Continuation 17604860
Provisional Application 62839485 · Apr 26, 2019
Related Publication 20230361309A1 · Nov 9, 2023
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