IP Library › Granted Patent US 12,415,757
Granted Patent B2
US 12,415,757 · App. 18/296,552 · Granted Sep 16, 2025

Method of making a sprayable setting type compound

Inventors: Rafael Bury (Wheeling, IL); Joseph W. Schlude (Deerfield, IL); David D. Pelot (Chicago, IL); Naveen Punati (Kildeer, IL); Tyler Kincaid (Wheaton, IL); Juan Ignacio Huitzil (Puebla, MX)
Assignee: KNAUF GIPS KG
C04B28/14C04B14/10C04B22/10C04B22/142C04B22/16C04B41/009C04B41/4543C04B41/5085C04B41/65C04B2103/12C04B2103/22C04B2103/44C04B2111/00172C04B2111/00681
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Quick Facts
Patent No.
US 12,415,757
App. No.
18/296,552
Granted
Sep 16, 2025
Kind
B2
Abstract

A method of making a setting type compound by injecting an activator compound into a plaster compound wherein the activator compound tube is coaxial and within the plaster compound tube, each at the same flowrate, the same pressure and the same viscosity. The cross sectional transverse areas of an annulus containing the plaster compound and the hole in the annulus containing the activator compound are the same.

Claims (53)

1. A method of making a setting type compound comprising:

feeding a plaster compound and injecting an activator compound into a T-connector, wherein the T-connector has a first leg having a first inlet opening in communication with a first tube, the first tube comprising a second leg of the T-connector and a third leg of the T-connector, the second leg and the third leg being aligned, the second leg having a second inlet opening, the third leg having a discharge opening, the second inlet opening and the discharge opening being opposed;

wherein feeding the plaster compound comprises pumping the plaster compound through the first leg into the first tube where the second leg meets the third leg at a specified first pressure and flowing the plaster compound at a specified first flowrate through the third leg of the first tube,

injecting an activator compound at a specified second pressure and specified second flowrate through a second tube located within said second leg and extending into the third leg, the activator compound discharging from an exit at a downstream portion of the second tube located within and coaxial with the second leg of the first tube to contact the plaster compound; wherein the exit is upstream of the discharge opening of the first tube;

wherein an annulus between the first tube and second tube at the exit has a first cross-sectional transverse area,

wherein the second tube at the exit defines an inner second cross-sectional transverse area,

wherein the first cross-sectional transverse area is equal to or greater than the second cross-sectional transverse area, and

mixing the plaster compound with the activator compound in about a 1:1 to 10:1 volume ratio in a static mixer downstream of the exit to yield the setting type compound;

wherein a ratio of the inner cross-sectional transverse area of the second tube to cross-sectional transverse area of an annulus between the first tube and the second tube is 0.25:1 to 1:1;

wherein the specified first rate of flow and the specified second rate of flow are each in a range of 0.5-4 gpm,

wherein the viscosity of the plaster compound is between 2,500 and 28,000 cps,

wherein the viscosity of the activator compound is between 2,500 and 28,000 cps,

wherein the viscosity of the activator compound, and the viscosity of the plaster compound and the viscosity of the setting type compound are equal;

wherein the viscosity of the setting type compound is between 2,500 and 28,000 cps,

wherein each of the specified first pressure and the specified second pressure is in a range from 1000 to 3500 psi.

2. The method according to claim 1 , further comprising spraying the setting type compound on a drywall, concrete, brick and mortar, textured substrates and other conventional substrates.

3. The method according to claim 1 ,

wherein the plaster compound comprises in weight percent on a dry basis:

plaster at about 20-about 99 wt. % of the plaster compound,

attapulgite clay at 0.05-about 2 wt. % of the plaster compound,

thickening agent at 0-about 2 wt. % of the plaster compound,

retarder at 0-about 2 wt. % of the plaster compound,

chelator at about 0.05-about 5 wt. % of the plaster compound, wherein the chelator is selected from tetra sodium pyrophosphate or tetra potassium pyrophosphate,

an optional second chelator at about 0.05-about 5 wt. % of the plaster compound,

preservative at 0-about 2 wt. % of the plaster compound, and

water at about 5-about 75 wt. % of the plaster compound on a wet basis.

4. The method according to claim 1 , wherein the activator compound comprises in weight percent on a dry basis:

calcium carbonate at 0-about 99 wt. % of the activator compound, attapulgite clay at 0-about 2 wt. % of the activator compound,

zinc sulfate monohydrate at about 0.1-about 99 wt. % of the activator compound,

thickening agent at 0-about 2 wt. % of the activator compound,

preservative at 0-about 2 wt. % of the activator compound, and

water at about 5-75 wt. % of the activator compound on a wet basis.

5. The method according to claim 1 ,

wherein the specified first rate of flow and the specified second rate of flow are each 1-2 gpm,

wherein the viscosity of the plaster compound is between 4000 and 5600 cps,

wherein the viscosity of the activator compound is between 4000 and 5600 cps,

wherein the viscosity of the setting type compound is between 4000 and 5600 cps,

wherein each of the specified first pressure and the specified second pressure is in a range from above 2000 to 3500 psi, and the specified first pressure and the specified second pressure are equal;

wherein the first rate of flow and the second rate of flow are equal.

6. The method according to claim 1 , wherein each of the specified first pressure and the specified second pressure is 2000-3000 psi, and the specified first pressure and the specified second pressure are equal.

7. The method according to claim 1 , wherein the setting type compound has about 55 to about 88 wt. % solids, wherein the activator compound and the plaster compound have the same weight percent solids.

8. The method according to claim 1 , wherein the mixing step has a 1:1 volume ratio of the plaster compound to the activator compound.

9. The method according to claim 1 , wherein the setting type compound has about 69 to about 78 wt. % solids.

10. The method according to claim 1 , wherein the setting type compound has about 72 to about 78 wt. % solids.

11. The method according to claim 1 , wherein the viscosity of the plaster compound is between 4,000-5,600 cps,

wherein the viscosity of the activator compound is between 4,000-5,600 cps, and

wherein the viscosity of the setting type compound is between 4,000-5,600 cps.

12. The method according to claim 1 , wherein the setting type compound consists essentially of the activator compound and the plaster compound.

13. The method according to claim 1 , wherein the specified first pressure is about equal of the specified second pressure.

14. The method according to claim 1 , wherein the specified first flowrate is equal to the specified second flowrate.

15. The method according to claim 1 , wherein the spraying is through a nozzle on a spray gun.

16. The method according to claim 1 , wherein each of the specified first pressure and the specified second pressure is 1500-3000 psi, and the specified first pressure and the specified second pressure are equal.

17. The method of claim 1 , wherein the feeding of the plaster compound and injecting of the activator compound are provided by a single pump.

Assignments (4)
CORRECTIVE ASSIGNMENT TO CORRECT THE THE PROPERTY SECTION BY REMOVING THE FOLLOWING NUMBERS: US APPLICATION NOS. 17815628, 17816462, 63476769, 18482718, 63480055, 18219467, 63508313, 18643391, 63511370, 18625779, AND PCT APPLICATION NOS. US2328362, US2328846, US2384176, US2410391, US2432338, US2433943 PREVIOUSLY RECORDED ON REEL 69170 FRAME 414. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT . Recorded Nov 20, 2024
From: UNITED STATES GYPSUM COMPANY
To: KNAUF GIPS KG
Reel/Frame 069560/0147 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 15, 2024
From: UNITED STATES GYPSUM COMPANY
To: KNAUF GIPS KG
Reel/Frame 069170/0414 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 22, 2023
From: BURY, RAFAEL; SCHLUDE, JOSEPH W.; PELOT, DAVID D.; PUNATI, NAVEEN; KINCAID, TYLER; HUITZIL, JUAN IGNACIO
To: UNITED STATES GYPSUM COMPANY
Reel/Frame 064999/0125 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 7, 2023
From: BURY, RAFAEL; SCHLUDE, JOSEPH W.; PELOT, DAVID D.; PUNATI, NAVEEN; KINCAID, TYLER; HUITZIL, JUAN IGNACIO
To: UNITED STATES GYPSUM COMPANY
Reel/Frame 063255/0486 →
Continuity (2)
Provisional Application 63377497 · Sep 28, 2022
Related Publication 20240101479A1 · Mar 28, 2024
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