IP Library Granted Patent US 12,090,480
Granted Patent B2
US 12,090,480 · App. 18/362,530 · Granted Sep 17, 2024

Partition-based method of analysis

Inventors: Donald A. Masquelier (Tracy, CA); Kevin D. Ness (Pleasanton, CA); Benjamin J. Hindson (Livermore, CA); Billy W. Colston, Jr. (San Ramon, CA)
Assignee: Bio-Rad Laboratories, Inc.
B01L3/50273B01F23/41B01F33/3011B01F33/813B01L3/502B01L3/502784B01L3/52B01L9/527C12Q1/686B01F25/14B01F25/23B01F33/3021B01L3/502761B01L2200/025B01L2200/0636B01L2200/0647B01L2200/0673B01L2200/14B01L2200/16B01L2300/0609B01L2300/0681B01L2300/0816B01L2300/0829B01L2300/0861B01L2400/049G01N35/08
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Quick Facts
Patent No.
US 12,090,480
App. No.
18/362,530
Granted
Sep 17, 2024
Kind
B2
Abstract

Methods of partition-based analysis. In an exemplary method, a device having a port fluidically connected to a chamber may be selected. A sample-containing fluid may be placed into the port. The sample-containing fluid may be moved from the port to the chamber. Partitions of the sample-containing fluid may be formed. A monolayer of the partitions in the chamber may be created. At least a portion of the monolayer may be imaged.

Claims (23)

1. A method for quality control in digital PCR, the method comprising the steps of:

preparing a reaction mixture comprising a target nucleic acid, a first dye, a second dye, and nucleic acid amplification reagents;

generating a plurality of partitions comprising the reaction mixture; and

assessing the first dye or and the second dye to indicate variation among the partitions, the first dye providing a test signal and the second dye providing a reference signal and indicating a partition volume of the partitions.

2. The method of claim 1 , wherein the assessing step comprises colorimetric measurement of the first dye or the second dye.

3. The method of claim 1 , wherein at least one of the partitions does not contain the reaction mixture.

4. The method of claim 1 , wherein the assessing step comprises assessing a partition volume for members of the plurality.

5. The method of claim 1 , further comprising the step of identifying a member of the plurality below a predefined partition volume.

6. The method of claim 1 , wherein reference signal indicates amplification of a control nucleic acid target.

7. A method for quality control in a digital PCR, the method comprising:

distributing a reaction mixture comprising a target nucleic acid, a first dye, a second dye, and nucleic acid amplification reagents into a plurality of partitions; and

assessing the first dye or and the second dye to indicate presences of the reaction mixture within members of the plurality, the first dye providing a test signal and the second dye providing a reference signal and indicating a partition volume of the partitions.

8. The method of claim 7 , wherein the assessing step comprises colorimetric measurement of the first dye or the second dye.

9. The method of claim 7 , wherein at least one of the partitions does not contain the reaction mixture.

10. The method of claim 7 , wherein the dye or the second dye is indicative of a volume of the reaction mixture in members of the plurality.

11. The method of claim 7 , wherein the assessing step comprises assessing a partition volume for members of the plurality.

12. The method of claim 7 , further comprising the step of identifying a member of the plurality of partitions below a predetermined partition volume.

13. The method of claim 7 , wherein the reference signal indicates amplification of a control nucleic acid target.

14. The method of claim 1 , wherein the dye or the second dye is indicative of a volume of the reaction mixture in members of the plurality.

15. The method of claim 1 , wherein the second dye is not coupled to an amplification reaction and provides a passive reference.

16. The method of claim 1 , further comprising transforming the test signal based on the reference signal to reduce variation.

17. The method of claim 7 , wherein the second dye is not coupled to an amplification reaction and provides a passive reference.

18. The method of claim 7 , further comprising transforming the test signal based on the reference signal to reduce variation.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 1, 2024
From: COLSTON, BILLY WAYNE, JR.; HINDSON, BENJAMIN JOSEPH; NESS, KEVIN DEAN; MASQUELIER, DONALD ARTHUR; MILANOVICH, FRED PAUL; MODLIN, DOUGLAS; RIOT, VINCENT; BURD, SAMUEL; MAKAREWICZ, ANTHONY JOSEPH, JR.; BELGRADER, PHILLIP; BRIGHT, ISAAC J.; LUCERO, MICHAEL Y.
To: QUANTALIFE, INC.
Reel/Frame 071380/0338 →
MERGER Recorded Jul 1, 2024
From: QUANTALIFE, INC.
To: BIO-RAD QL, INC.
Reel/Frame 067880/0623 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 1, 2024
From: BIO-RAD QL, INC.
To: BIO-RAD LABORATORIES, INC.
Reel/Frame 068065/0601 →
Continuity (93)
Continuation 17486667 · Sep 27, 2021
Continuation 16667811 · Oct 29, 2019
Continuation 15707908 · Sep 18, 2017
Continuation 15351354 · Nov 14, 2016
Continuation In Part 12954634 · Nov 25, 2010
Continuation In Part 13400030 · Feb 17, 2012
Continuation In Part 14020742 · Sep 6, 2013
Continuation In Part 14159410 · Jan 20, 2014
Continuation In Part 14201752 · Mar 7, 2014
Continuation In Part 14848311 · Sep 8, 2015
Continuation In Part 12586626 · Sep 23, 2009
Continuation In Part 12862542 · Aug 24, 2010
Continuation In Part 12890550 · Sep 24, 2010
Continuation In Part 13245575 · Sep 26, 2011
Continuation In Part 13945661 · Jul 18, 2013
Continuation In Part 12962507 · Dec 7, 2010
Continuation In Part 12962511 · Dec 7, 2010
Continuation In Part 12962502 · Dec 7, 2010
Continuation In Part 12963523 · Dec 8, 2010
Continuation In Part 13039233 · Mar 2, 2011
Continuation In Part 12976827 · Dec 22, 2010
Continuation In Part 13341669 · Dec 30, 2011
Continuation In Part 13341678 · Dec 30, 2011
Continuation In Part 13072673 · Mar 25, 2011
Continuation In Part 13341688 · Dec 30, 2011
Continuation In Part 13287120 · Nov 1, 2011
Continuation In Part 13424304 · Mar 19, 2012
Continuation In Part 13548062 · Jul 12, 2012
Continuation In Part PCTUS2012048198 · Jul 25, 2012
Continuation In Part 13562198 · Jul 30, 2012
Continuation In Part 13287095 · Nov 1, 2011
Continuation In Part 12586626 · Sep 23, 2009
Continuation 12586626 · Sep 23, 2009
Continuation In Part 13251016 · Sep 30, 2011
Continuation In Part 13245575 · Sep 26, 2011
Continuation 12586626 · Sep 23, 2009
Continuation 12976827 · Dec 22, 2010
Continuation 12586626 · Sep 23, 2009
Continuation 12586626 · Sep 23, 2009
Continuation 12586626 · Sep 23, 2009
Continuation PCTUS2011030101 · Mar 25, 2011
Continuation PCTUS2011030077 · Mar 25, 2011
Continuation In Part 12586626 · Sep 23, 2009
Continuation PCTUS2011030097 · Mar 25, 2011
Continuation In Part 12976827 · Dec 22, 2010
Division 13385277 · Feb 9, 2012
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