IP Library Granted Patent US 12,196,109
Granted Patent B2
US 12,196,109 · App. 18/370,648 · Granted Jan 14, 2025

Reactive thermal barrier coating

Inventors: Brian T. Hazel (Avon, CT); Elisa M. Zaleski (Vernon, CT); Kaylan M. Wessels (West Hartford, CT)
Assignee: RTX Corporation
F01D5/282B32B15/04B32B18/00C23C4/11C23C4/134C23C4/18C23C14/06C23C14/08C23C14/081C23C14/082C23C14/083C23C14/086C23C14/088C23C14/22C23C14/28C23C14/30C23C14/34C23C14/3492C23C16/40C23C16/405C23C16/409C23C16/45525C23C28/04C23C28/042C23C28/30C23C28/3215C23C28/345C23C28/3455C23C30/00C23C30/005F01D5/28F01D5/284F01D5/288F01D25/005F01D25/08C04B2237/34C04B2237/343C04B2237/348Y10T428/1259Y10T428/12597Y10T428/12611Y10T428/12618Y10T428/2495Y10T428/24967Y10T428/265
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Quick Facts
Patent No.
US 12,196,109
App. No.
18/370,648
Granted
Jan 14, 2025
Kind
B2
Abstract

A calcium-magnesium-alumino-silicate (CMAS)-reactive thermal barrier coating includes a ceramic coating and a CMAS-reactive overlay coating, wherein the CMAS-reactive overlay coating conforms to a surface of the ceramic coating and comprises a compound that forms a stable high melting point crystalline precipitate when reacted with molten CMAS at a rate that is competitive with CMAS infiltration kinetics into the thermal barrier coating. The ceramic coating phase is stable with the CMAS-reactive overlay coating.

Claims (15)

1. A calcium-magnesium-alumino-silicate (CMAS)-reactive thermal barrier coating comprising:

a ceramic coating comprising a plurality of featherlike columnar grains separated by vertically-oriented gaps open to an outer surface, the ceramic coating comprising stabilized zirconia or stabilized hafnia; and

a CMAS-reactive overlay coating, wherein the CMAS-reactive overlay coating conforms to a surface of the ceramic coating and comprises a pure rare earth oxide, a mixed rare earth oxide, or a rare earth aluminate.

2. The CMAS-reactive thermal barrier coating of claim 1 , wherein the ceramic coating comprises yttrium stabilized zirconia.

3. The CMAS-reactive thermal barrier coating of claim 1 , wherein the ceramic coating comprises gadolinium zirconate.

4. The CMAS-reactive thermal barrier coating of claim 3 , wherein the ceramic coating comprises an outer layer and an inner layer, and wherein the inner layer of the ceramic coating comprises yttrium stabilized zirconia and the outer layer comprises gadolinium zirconate.

5. The CMAS-reactive thermal barrier coating of claim 1 , wherein the CMAS-reactive overlay is a pure rare earth oxide selected from the group of rare earth oxides consisting of Gd 2 O 3 and Y 2 O 3 .

6. The CMAS-reactive thermal barrier coating of claim 1 , wherein the CMAS-reactive overlay is mixed rare earth oxide comprising the elements gadolinium and yttrium.

7. The CMAS-reactive thermal barrier coating of claim 1 , wherein the CMAS-reactive overlay is a rare earth aluminate selected from the group of rare earth aluminates consisting of Y 4 Al 2 O 9 and Y 3 Al 5 O 12 .

8. The CMAS-reactive thermal barrier coating of claim 1 , wherein the ceramic coating comprises a plurality of vertically-oriented gaps and wherein the CMAS-reactive overlay coating extends into the gaps and is deposited on inner walls of the ceramic coating, and wherein the plurality of vertically-oriented gaps remain open.

9. The CMAS-reactive thermal barrier coating of claim 8 , wherein the CMAS-reactive overlay is deposited in pores open to the vertically-oriented gaps.

10. The CMAS-reactive thermal barrier coating of claim 8 , wherein the thickness of the CMAS-reactive overlay ranges from 10 to 500 nanometers.

11. The CMAS-reactive thermal barrier coating of claim 8 , wherein the CMAS-reactive overlay extends into the vertically-oriented gaps to a depth of at least one-third of a thickness of the ceramic coating from an outer surface of the ceramic coating.

12. The CMAS-reactive thermal barrier coating of claim 11 , wherein the CMAS-reactive overlay extends into the vertically-oriented gaps to a depth of at least one-half of a thickness of the ceramic coating from an outer surface of the ceramic coating.

13. The CMAS-reactive thermal barrier coating of claim 1 , wherein the CMAS-reactive overlay has a material composition that will react with molten CMAS to form an oxy-apatite phase.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 20, 2023
From: HAZEL, BRIAN T.; ZALESKI, ELISA M.; WESSELS, KAYLAN M.
To: RAYTHEON TECHNOLOGIES CORPORATION
Reel/Frame 064971/0769 →
CHANGE OF NAME Recorded Sep 20, 2023
From: RAYTHEON TECHNOLOGIES CORPORATION
To: RTX CORPORATION
Reel/Frame 064973/0017 →
Continuity (3)
Continuation 16906298 · Jun 19, 2020
Provisional Application 62864624 · Jun 21, 2019
Related Publication 20240011402A1 · Jan 11, 2024
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