IP Library Granted Patent US 12,486,481
Granted Patent B2
US 12,486,481 · App. 18/410,960 · Granted Dec 2, 2025

Systems and methods for stillage fractionation

Inventor: Jason Alan Bootsma (Sioux Falls, SD)
Assignee: POET Research, Inc.
C12F3/10A23K10/38A23K20/163A23K50/10C10L1/026C11B1/00C12M41/26C12M43/00C12M47/10C12M47/14Y02P60/87
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Quick Facts
Patent No.
US 12,486,481
App. No.
18/410,960
Granted
Dec 2, 2025
Kind
B2
Abstract

Systems and methods for fractionating whole stillage from an ethanol production facility are provided. Whole stillage undergoes a separation of its liquid portion (thin stillage) from the solid portion (fiber cake). In some embodiments, the solids and liquids in whole stillage may be separated utilizing a screening centrifuge. The fiber cake may be dried to generate a high fiber animal feed. The thin stillage may be provided to a three-phase separator for separation into an oil emulsion, an aqueous clarified stillage, and a protein paste. The protein paste may be dried to generate a high protein animal feed with greater than about 45% protein content. The clarified thin stillage is condensed to yield a syrup with greater than around 60% solids. The oil emulsion is subjected to a pH adjustment to liberate the oil from the emulsion, which is then separated.

Claims (27)

1 . A method for processing whole stillage in an ethanol plant, comprising:

separating thin stillage liquid from the whole stillage;

separating protein paste and clarified liquid stillage output from the thin stillage liquid; and

sending at least a portion of the clarified liquid stillage output to an evaporation system to concentrate the clarified liquid stillage output into a concentrated, clarified liquid stillage product having at least 60% solids, wherein the concentrated, clarified liquid stillage product is used as an animal feed supplement, wherein the concentrated, clarified liquid stillage product comprises:

from 30% to 40% moisture; and

greater than 10% protein.

2 . The method of claim 1 , wherein separating the thin stillage liquid from the whole stillage produces a fiber cake.

3 . The method of claim 2 , further comprising drying the fiber cake to provide a high fiber animal feed product.

4 . The method of claim 2 , further comprising combining at least a portion of the protein paste and at least a portion of the fiber cake to form an animal feed product.

5 . The method of claim 1 , further comprising drying protein paste to provide an animal feed product.

6 . The method of claim 5 , wherein the animal feed product has at least 45% protein.

7 . The method of claim 1 , further comprising recycling a portion of the clarified liquid stillage output upstream for utilization as fermentation backset.

8 . The method of claim 1 , wherein separating thin stillage liquid from the whole stillage comprises separating thin stillage liquid from the whole stillage via filtration, centrifugation, pressing, and combinations thereof.

9 . The method of claim 1 , wherein separating thin stillage liquid from the whole stillage comprises separating thin stillage liquid from the whole stillage via one or more membranes, one or more screw presses, one or more decanters, one or more centrifuges, one or more filters, and combinations thereof.

10 . The method of claim 1 , wherein separating thin stillage liquid from the whole stillage comprises separating thin stillage liquid from the whole stillage via one or more filtration centrifuges.

11 . The method of claim 1 , wherein the thin stillage liquid is not subjected to an evaporator prior to separating protein paste and clarified liquid stillage output from the thin stillage liquid.

12 . The method of claim 1 , wherein separating protein paste and clarified liquid stillage output from the thin stillage liquid comprises separating protein paste and clarified liquid stillage output from the thin stillage liquid via filtration, centrifugation, and combinations thereof.

13 . The method of claim 1 , wherein separating protein paste and clarified liquid stillage output from the thin stillage liquid comprises separating protein paste and clarified liquid stillage output from the thin stillage liquid via a separation system comprising one or more separators, wherein the one or more separators are chosen from chosen from a three phase separator, a disk nozzle type centrifuge, a decanter centrifuge, and combinations thereof.

14 . The method of claim 1 , wherein separating protein paste and clarified liquid stillage output from the thin stillage liquid comprises separating protein paste and clarified liquid stillage output from the thin stillage liquid via one or more disk nozzle type centrifuges.

15 . The method of claim 1 , wherein the concentrated, clarified liquid stillage further comprises:

less than 1% fiber;

from 6% to 10% fat; and

from 5% to 7% ash.

16 . The method of claim 1 , wherein separating protein paste and clarified liquid stillage output from the thin stillage liquid comprises separating the thin stillage liquid into the clarified liquid stillage output, the protein paste, and an oil emulsion.

17 . The method of claim 16 , further comprising separating oil from the oil emulsion.

18 . The method of claim 17 , wherein separating oil from the oil emulsion forms a residual aqueous layer, wherein the residual aqueous layer comprises protein; and further comprising forming an animal feed product with at least a portion of the residual aqueous layer.

19 . The method of claim 1 , wherein the concentrated, clarified liquid stillage has a yield of at least 2 pounds per bushel of corn.

Assignments (3)
SECURITY INTEREST Recorded Aug 19, 2025
From: POET RESEARCH, INC.
To: COBANK, ACB
Reel/Frame 072062/0409 →
SECURITY INTEREST Recorded Aug 15, 2025
From: POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 072489/0295 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 23, 2024
From: BOOTSMA, JASON ALAN
To: POET RESEARCH, INC.
Reel/Frame 066210/0611 →
Continuity (6)
Continuation 17218508 · Mar 31, 2021
Continuation 16534165 · Aug 7, 2019
Division 15015355 · Feb 4, 2016
Division 14112897
Provisional Application 61476702 · Apr 18, 2011
Related Publication 20240263110A1 · Aug 8, 2024
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