IP Library › Granted Patent US 12,649,806
Granted Patent B2
US 12,649,806 · App. 18/538,072 · Granted Jun 9, 2026

Surface-treated, transportable ISO tanks and methods of reducing deposition of a friction reducer on a surface

Inventors: Eric L. Hanson (Carlsbad, CA); Eric L Bruner (La Jolla, CA); Majid Monji (San Diego, CA); Elizabeth Cambre (Texas City, TX); Edward Hughes (San Diego, CA)
Assignee: ACULON INC.
C08F120/56C08G65/007C08G65/226C08J7/042C09D5/1662C09D5/1693C09D171/00C09D171/02C09K8/52C09K8/882C10M105/74C23F11/173E21B43/08F17C13/004B01F25/31243C09K2208/34C10M2223/0603C10N2040/00F17C2201/0109F17C2221/01F17C2270/01
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Quick Facts
Patent No.
US 12,649,806
App. No.
18/538,072
Granted
Jun 9, 2026
Kind
B2
Abstract

Treated, transportable ISO tanks include an interior metal surface and a hydrophobic surface layer applied thereto, directly or through an intermediate layer. The surface layer comprises a self-assembled monolayer prepared from a fluorinated material having the structure: wherein A is an oxygen radical or a chemical bond; n is 1 to 20; Y is H, F, C n H 2n+1 or C n F 2n+1 ; X is H or F; b is at least 1, m is 0 to 50, p is 1 to 20, and Z is an acid group or an acid derivative. Also, a method of reducing deposition of a friction reducer on a surface of an apparatus that stores or transports the same, includes contacting the surface with the above fluorinated material in a diluent, directly or through an intermediate layer; forming a film on the surface; and introducing the friction reducer therein.

Claims (18)

1 . A method of reducing deposition of a friction reducer on a metal surface of an apparatus that stores or transports the friction reducer, the method comprising:

(a) contacting a metal surface of an apparatus that stores or transports the friction reducer, either directly or through an intermediate organometallic layer, with a fluorinated material in a diluent, wherein the fluorinated material has the following structure:

wherein A is an oxygen radical or a chemical bond, n is 1 to 20, Y is H, F, C n H 2n+1 or C n F 2n+1 , X is H or F, b is at least 1, m is 0 to 50, p is 1 to 20, and Z is an acid group or an acid derivative;

(b) forming a hydrophobic surface layer on the metal surface to reduce deposition of the friction reducer thereon; and (c) introducing the friction reducer into the apparatus.

2 . The method of claim 1 wherein the friction reducer comprises a polyacrylamide polymer.

3 . The method of claim 2 wherein the friction reducer is suspended in a carrier comprising mineral oil.

4 . The method of claim 1 wherein the apparatus comprises an ISO tank.

5 . The method of claim 1 wherein the surface comprises stainless steel.

6 . The method of claim 1 wherein the fluorinated material is dissolved or dispersed in a diluent to form a solution or dispersion, and the solution or dispersion is coalesced on the surface to form the hydrophobic surface layer.

7 . The method of claim 1 wherein Z is selected from:

where R″ is a hydrocarbon or substituted hydrocarbon radical having up to 200 carbons, and R and R′ are each independently H, a metal or an amine or an aliphatic or substituted aliphatic radical having 1 to 50 carbons or an aryl or substituted aryl radical having 6 to 50 carbons.

8 . The method of claim 7 wherein Z is

9 . The method of claim 1 wherein n is 1 to 6; b is 5 to 12, m is 1 to 6, and p is 2 to 4.

10 . The method of claim 1 wherein the fluorinated material in the hydrophobic surface layer is adhered to an intermediate organometallic layer.

11 . The method of claim 10 wherein the intermediate organometallic layer is a polymeric metal oxide with alkoxide and hydroxyl groups.

12 . The method of claim 1 , wherein the diluent comprises at least one of a glycol, a glycol ether, 1,1,1,2,2,3,3,4,4-nonafluoro-4-methoxybutane, 1,1,1,2,2,3,3,4,4-nonafluoro-4-ethoxybutane, 3-ethoxyperfluoro(2-methylhexane), 1H,1H,5H-Octafluoropentyl-1,1,2,2-tetrafluoroethyl ether, and 1,1,1,2,3,4,4,5,5,5-Decafluoropentane.

13 . The method of claim 12 wherein Z is selected from:

where R″ is a hydrocarbon or substituted hydrocarbon radical having up to 200 carbons, and R and R′ are each independently H, a metal or an amine or an aliphatic or substituted aliphatic radical having 1 to 50 carbons or an aryl or substituted aryl radical having 6 to 50 carbons.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 26, 2024
From: HANSON, ERIC L; BRUNER, ERIC L.; MONJI, MAJID; CAMBRE, ELIZABETH; HUGHES, EDWARD
To: ACULON INC.
Reel/Frame 066564/0266 →
Continuity (2)
Provisional Application 63432215 · Dec 13, 2022
Related Publication 20240200726A1 · Jun 20, 2024
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