Process of preparing continuous filament composed of nano fiber
View Patent ↗The present invention relates to a process of preparing a continuous filament composed of a nano fiber, wherein nano fibers are prepared by spinning a polymer spinning dope in a spinning dope main tank ( 20 ) onto the surface of water or organic solvent ( 4 a ) of a collector ( 4 ), which contains water or inorganic solvent ( 4 a ) and has a conductive material ( 5 ) with a high voltage applied sunken in the water or organic solvent ( 4 a ), through nozzles ( 2 ) with a high voltage applied, and the nano fibers are pressed, drawn, dried and wound while being pulled by a rotary roller ( 6 ) rotating at a constant linear velocity from the location spaced more than 1 cm from one end of a dropping spot. The present invention can prepare a continuous filament composed of a nano fiber by an electrospinning method and a continuous process.
1. A process of preparing a continuous filament composed of
nano fibers, which comprises
spinning a polymer spinning dope through nozzles onto a collector surface of water or an organic solvent and which has a conductive material disposed below the collector surface of said water or organic solvent,
applying a high voltage to said nozzles and said conductive material, and
the nano fibers spun onto the surface of said water or organic solvent are pressed, drawn, dried and wound while being pulled by a rotary roller rotating at a constant linear velocity at a location spaced more than 1 cm from one end of a dropping spot where the spun polymer contacts the collector surface.
2. The process of claim 1 , wherein the conductive material is a metal plate or a metal powder.
3. The process of claim 1 , wherein the distance from the surface of the water or organic solvent to the top surface of the conductive material is 0.01 to 200 mm.
4. The process of claim 1 , wherein the distance from the surface of the water or organic solvent to the top surface of the conductive material is 5 to 50 mm.
5. The process of claim 1 , wherein the angel (θ) between the nano fibers collected on the surface of the water or organic solvent and the undrawn filament (aggregate of nano fibers) pulled by a rotary roller is 0 to 180°.
6. The process of claim 1 , wherein the angle (θ) between the nano fibers collected on the surface of the water or organic solvent and the undrawn filament (aggregated of nano fibers) pulled by a rotary is 10 to 90°.
7. The process of claim 1 , wherein the drawn filament (yarn) is twisted before being wound.
8. The process of claim 1 , wherein the diameter of the nano fibers is less than 1,000 nm.
9. The process of claim 1 , wherein the polymer spinning dope is selected from the group consisting of polyester resins, nylon resins, polysulfon resins, poly lactic acid and a copolymer thereof or a mixture thereof.
10. The process of claim 1 , wherein more than two kinds of polymer spinning dope are spun onto the surface of the water or organic solvent to form two kinds of nano fibers, said two kinds of nano fibers being combined together.