Method for manufacturing a thermal interface material
View Patent ↗A method for manufacturing a thermal interface material comprising the steps of: providing a carbon nanotube array comprising a plurality of carbon nanotubes each having two opposite ends; forming a composite phase change material by filling clearances in the carbon nanotube array with a phase change material; forming a section with predetermined thickness by cutting the composite phase change material along a direction cross to an alignment direction of the carbon nanotubes; and heating up the section to a temperature higher than a phase change temperature of the phase change material and cooling down after the two opposite ends of the carbon nanotubes protruding out of the section.
1. A method for manufacturing a thermal interface material comprising the steps of:
providing a carbon nanotube array comprising a plurality of carbon nanotubes each having two opposite ends;
forming a composite phase change material by filling clearances in the carbon nanotube array with a paraffin;
cutting the composite phase change material to form a section and bending the ends of the carbon nanotubes, wherein the cutting of the composite phase change material is done along a direction that is at an angle to an alignment direction of the carbon nanotubes and bends the ends of the carbon nanotubes; and
heating the section to a temperature of 60 degrees Celsius until the ends of the carbon nanotubes become unbent and protrude out of the section.
2. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein the step of forming the composite phase change material comprising steps of:
immersing the carbon nanotube array into xylene;
putting paraffin into the xylene at 60 degrees Celsius;
evaporating the xylene; and
cooling the paraffin down.
3. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein the carbon nanotubes are formed by a chemical vapor deposition method or a deposition method.
4. The method for manufacturing a thermal interface material in accordance with claim 3 , wherein a catalyst used in the chemical vapor deposition method is made from a material selected from the group comprising of iron, cobalt, nickel, and palladium.
5. The method for manufacturing a thermal interface material in accordance with claim 3 , wherein a carbon source gas used in the chemical vapor deposition method is selected from the group comprising of methane, ethylene, propylene, acetylene, methanol, and ethanol.
6. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein the carbon nanotubes are substantially parallel to each other.
7. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein a thickness of the section is in a range from about 1 μm to about 100 μm.
8. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein a content of the carbon nanotubes array in the thermal interface material is in a range from about 0.2% to about 10% by volume.
9. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein a content of the carbon nanotubes array in the thermal interface material is about 10% by volume.
10. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein a content of the carbon nanotubes array in the thermal interface material is about 0.2% by volume.
11. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein the angle is approximately ninety degrees.
12. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein after cutting the composite phase change material, the carbon nanotubes in the section are in the shape of a “U”.
13. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein after cutting the composite phase change material, the carbon nanotubes in the section are formed in the shape of a “Z”.
14. The method for manufacturing a thermal interface material in accordance with claim 1 , wherein bending directions of the ends of the carbon nanotubes varies according to the direction of the cutting of the composite phase change material.
15. A method for manufacturing a thermal interface material comprising the steps of:
providing a composite phase change material comprising of carbon nanotube array comprising a plurality of carbon nanotubes each having two opposite ends and a paraffin filling clearances within the carbon nanotube array;
cutting the composite phase change material to form a section and bending the ends of the carbon nanotubes, wherein the cutting of the composite phase change material bends the ends of the carbon nanotubes and is done along a direction that is at an angle to an alignment direction of the carbon nanotubes; and
heating the section until the ends of the carbon nanotubes become unbent and protrude out of the section.