IP Library Granted Patent US 7,732,048
Granted Patent B2
US 7,732,048 · App. 11/886,298 · Granted Jun 8, 2010

Cellulose multi-filament

Assignee: Hyosung Corporation
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Quick Facts
Patent No.
US 7,732,048
App. No.
11/886,298
Granted
Jun 8, 2010
Kind
B2
Abstract

The present invention relates to cellulose fiber containing 500 to 2000 of filaments and having homogeneous physical properties and the multi-filaments according to the present invention is characterized in that the strength and the breaking elongation of the multi-filaments are 4 to 9 g/d and 4 to 15%, respectively. In particular, the present invention is characterized in that each mono-filament selected 100 strands from every three part divided from multi-filaments has properties as following: (a) 3 to 9 g/d in average strength, 7 to 15% in average breaking elongation and 0.035 to 0.055 in by birefringence, (b) the differences of the above three parts are below 1.0 g/d in average strength, 1.5% in breaking elongation and 0.7 denier in denier, (c) the CV (%) (coefficient of variation) of the above three parts are below 10%, and (d) the birefringence differences of the above three parts are below 0.004.

Claims (14)

1. Cellulose multi-filament yarn produced by a method comprising the steps of:

(a) preparing a cellulose solution by swelling and homogenizing a cellulose powder into an aqueous concentrated N-methyl morpholine N-oxide (NMMO) solution;

(b) obtaining a multi-filaments by spinning said cellulose solution with a spinning nozzle having 500 to 2000 orifices and a distributing plate having 50 to 300 holes and subsequently precipitating the cellulose solution into a coagulating bath at a temperature of 0 to 35° C. through an air gap wherein the air is 5 to 30° C. in temperature and 10 to 60% in humidity is blown into the air gap at 0.5 to 10 mm/sec air speed; and

(c) water-washing, drying with a drying roller maintained at a temperature of 80 to 170° C., treating the multi-filaments with a finishing oil and winding said multi-filaments,

wherein the multi-filament yarn is characterized by the following physical properties:

700 to 3000 in denier of original strands;

4 to 9 g/d and 4 to 15% in strength and breaking elongation of the multi-filaments, respectively;

a specific breaking time of 3 to 33 sec/denier;

and when said multi-filaments are divided into three parts and 100 mono-filaments selected from each part of said three parts have following physical properties:

3 to 9 g/d in strength, 7 to 15% in breaking elongation and 0.035 and 0.055 birefringence, respectively;

the differences of average strength, average breaking elongation and average denier are less than 1.0 g/d, 1.5% and 0.7 denier, respectively;

CV (coefficient of variation) of average strength, average breaking elongation and denier of said three parts less an 10%; and

the differences of average birefringence of said three parts are less than 0.004.

2. A tire cord comprising the cellulose fiber according to claim 1 .

Assignments (3)
CHANGE OF NAME Recorded Feb 27, 2025
From: HYOSUNG ADVANCED MATERIALS CORPORATION
To: HS HYOSUNG ADVANCED MATERIALS CORPORATION
Reel/Frame 070355/0207 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 21, 2018
From: HYOSUNG CORPORATION
To: HYOSUNG ADVANCED MATERIALS CORPORATION
Reel/Frame 048963/0092 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 14, 2007
From: KWON, IK-HYUN; CHOI, SOO-MYUNG; LEE, TAE-JUNG; CHOI, JAE-SHIK
To: HYOSUNG CORPORATION
Reel/Frame 019859/0561 →
Priority Claims (1)
KR 10-2005-0021205 · Mar 15, 2005 · national
Continuity (1)
Related Publication 20090011234A1 · Jan 8, 2009